Estudo da secagem da polpa do abacate (Persea americana)

Detalhes bibliográficos
Ano de defesa: 2021
Autor(a) principal: Dal-Bó, Vanessa
Orientador(a): Freire, José Teixeira lattes
Banca de defesa: Não Informado pela instituição
Tipo de documento: Tese
Tipo de acesso: Acesso aberto
Idioma: por
Instituição de defesa: Universidade Federal de São Carlos
Câmpus São Carlos
Programa de Pós-Graduação: Programa de Pós-Graduação em Engenharia Química - PPGEQ
Departamento: Não Informado pela instituição
País: Não Informado pela instituição
Palavras-chave em Português:
Palavras-chave em Inglês:
Área do conhecimento CNPq:
Link de acesso: https://repositorio.ufscar.br/handle/ufscar/14435
Resumo: The drying process can be carried out by different methods, but the choice directly influences the quality of the final product, which can obviously be affected by operational conditions. This work aims to study the drying of the avocado pulp, through process optimization and experimental analysis. To achieve the proposed objective, this study was divided into two stages. Initially, the equipment to be used for drying the fruit pulp was defined. For this, the process synthesis techniques were applied, such as making the branch-and-bound trees, heuristic rules and determination the base flowchart, using the fuzzy logic method. From the application of the process synthesis, the lyophilization equipment proved to be promising for the drying process of the fruit pulp. After, considering that the knowledge of the drying rate is essential in the choice of suitable conditions for the lyophilization process, and the experimental data obtained to determine the drying kinetics, in the simplest lyophilizer, are measured in a discontinuous way, through destructive analysis, a simplest and low-cost setup for a laboratory-scale lyophilizer was developed, with an automated data acquisition system. The setup made it possible to obtain the drying kinetics curves, the temperature of the material as a function of time and the pressure difference, in addition to controlling different temperatures of the heating tray. The study was evaluated for the drying of the avocado pulp with heating temperature of 30, 40, 50 ° C and also without the supplying controlled of heat. The data acquisition system implemented proved to be satisfactory for the conditions evaluated. As expected, the load cell was influenced by the operating conditions, but the data was reproducible, so it was possible to minimize errors in the measurement of mass. The controlled supply of heat during lyophilization accelerated the process and, consequently, had a direct influence on the drying rate. In addition to the tests related to lyophilization of the avocado pulp, the influence of drying on the morphology, thermal decomposition, rehydration capacity, color, phenolic compounds and antioxidant activity of the fruit pulp was verified. It was observed that the heating temperature had an influence on the evaluated parameters, with temperatures of 40 and 50 ° C being the most appropriate for the process of dehydration of the fruit pulp. This study proved to be important for the analysis of the steps that occur during the lyophilization process.
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spelling Dal-Bó, VanessaFreire, José Teixeirahttp://lattes.cnpq.br/2270677706718167http://lattes.cnpq.br/73036356070731762021-06-25T21:40:28Z2021-06-25T21:40:28Z2021-04-26DAL-BÓ, Vanessa. Estudo da secagem da polpa do abacate (Persea americana). 2021. Tese (Doutorado em Engenharia Química) – Universidade Federal de São Carlos, São Carlos, 2021. Disponível em: https://repositorio.ufscar.br/handle/ufscar/14435.https://repositorio.ufscar.br/handle/ufscar/14435The drying process can be carried out by different methods, but the choice directly influences the quality of the final product, which can obviously be affected by operational conditions. This work aims to study the drying of the avocado pulp, through process optimization and experimental analysis. To achieve the proposed objective, this study was divided into two stages. Initially, the equipment to be used for drying the fruit pulp was defined. For this, the process synthesis techniques were applied, such as making the branch-and-bound trees, heuristic rules and determination the base flowchart, using the fuzzy logic method. From the application of the process synthesis, the lyophilization equipment proved to be promising for the drying process of the fruit pulp. After, considering that the knowledge of the drying rate is essential in the choice of suitable conditions for the lyophilization process, and the experimental data obtained to determine the drying kinetics, in the simplest lyophilizer, are measured in a discontinuous way, through destructive analysis, a simplest and low-cost setup for a laboratory-scale lyophilizer was developed, with an automated data acquisition system. The setup made it possible to obtain the drying kinetics curves, the temperature of the material as a function of time and the pressure difference, in addition to controlling different temperatures of the heating tray. The study was evaluated for the drying of the avocado pulp with heating temperature of 30, 40, 50 ° C and also without the supplying controlled of heat. The data acquisition system implemented proved to be satisfactory for the conditions evaluated. As expected, the load cell was influenced by the operating conditions, but the data was reproducible, so it was possible to minimize errors in the measurement of mass. The controlled supply of heat during lyophilization accelerated the process and, consequently, had a direct influence on the drying rate. In addition to the tests related to lyophilization of the avocado pulp, the influence of drying on the morphology, thermal decomposition, rehydration capacity, color, phenolic compounds and antioxidant activity of the fruit pulp was verified. It was observed that the heating temperature had an influence on the evaluated parameters, with temperatures of 40 and 50 ° C being the most appropriate for the process of dehydration of the fruit pulp. This study proved to be important for the analysis of the steps that occur during the lyophilization process.O processo de secagem pode ser realizado por diferentes métodos, porém a escolha influencia diretamente a qualidade do produto final, a qual pode ser evidentemente afetada pelas condições operacionais. Este trabalho tem como objetivo estudar a secagem da polpa do abacate, por meio da otimização de processos e análise experimental. Para atingir o objetivo proposto, este estudo foi dividido em duas etapas. Na primeira etapa definiu-se o equipamento a ser utilizado para a secagem da polpa do fruto. Para isso, foram aplicadas as técnicas de síntese de processo, como confecção de árvore de estados, regras heurísticas e determinação do fluxograma-base, por meio do método de lógica fuzzy. A partir da aplicação da síntese de processos, o equipamento de liofilização mostrou-se promissor para o processo de secagem da polpa do fruto. Na segunda etapa, tendo em vista que o conhecimento da taxa de secagem é essencial na escolha de condições adequadas para o processo de liofilização, e os dados experimentais obtidos para determinar a cinética de secagem, em liofilizadores mais básicos, são medidos de forma descontínua, por meio de análises destrutivas, foi desenvolvido um projeto de adaptação, simples e de baixo custo, de um liofilizador em escala laboratorial, com um sistema de aquisição de dados automatizado. O projeto permitiu obter as curvas de cinética de secagem, a temperatura do material em função do tempo e a diferença de pressão, além de controlar diferentes temperaturas da bandeja de aquecimento. O estudo foi avaliado para a secagem da polpa do abacate com temperatura de aquecimento de 30, 40, 50 °C e também sem o fornecimento controlado de calor. O sistema de aquisição de dados implementado mostrou-se satisfatório para as condições avaliadas. Como esperado, a célula de carga foi influenciada pelas condições operacionais, porém os dados foram reprodutíveis, com isso foi possível minimizar os erros na medida da massa. O fornecimento controlado de calor durante a liofilização acelerou o processo e, consequentemente teve influência direta na taxa de secagem. Além dos ensaios referentes a liofilização da polpa do abacate, verificou-se a influência da secagem na morfologia, decomposição térmica, capacidade de reidratação, cor, compostos fenólicos e atividade antioxidante da polpa do fruto. Observou-se que a temperatura de aquecimento exerceu influência nos parâmetros avaliados, sendo as temperaturas de 40 e 50°C as mais apropriadas para o processo de desidratação da polpa do fruto. Este estudo mostrou-se importante para a análise das etapas que ocorrem durante o processo de liofilização.Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)CNPq: 140907/2017-3porUniversidade Federal de São CarlosCâmpus São CarlosPrograma de Pós-Graduação em Engenharia Química - PPGEQUFSCarAttribution-NonCommercial-NoDerivs 3.0 Brazilhttp://creativecommons.org/licenses/by-nc-nd/3.0/br/info:eu-repo/semantics/openAccessSecagemCongelamentoReidrataçãoCompostos fenólicosSíntese de ProcessosFreeze-dryingDryingFreezeRehydrationPhenolic compoundsProcess synthesisENGENHARIAS::ENGENHARIA QUIMICA::PROCESSOS INDUSTRIAIS DE ENGENHARIA QUIMICAENGENHARIASEstudo da secagem da polpa do abacate (Persea americana)Study of the drying of avocado pulp (Persea americana)info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/doctoralThesisreponame:Repositório Institucional da UFSCARinstname:Universidade Federal de São Carlos (UFSCAR)instacron:UFSCARCC-LICENSElicense_rdflicense_rdfapplication/rdf+xml; charset=utf-8811https://{{ getenv "DSPACE_HOST" "repositorio.ufscar.br" }}/bitstream/ufscar/14435/4/license_rdfe39d27027a6cc9cb039ad269a5db8e34MD54ORIGINAL[2021] Tese - Vanessa Dal-Bó - UFSCar - PPGEQ.pdf[2021] Tese - Vanessa Dal-Bó - UFSCar - PPGEQ.pdf[2021] Tese - Vanessa Dal-Bó - UFSCar - PPGEQapplication/pdf3464796https://{{ getenv "DSPACE_HOST" "repositorio.ufscar.br" }}/bitstream/ufscar/14435/1/%5b2021%5d%20Tese%20-%20Vanessa%20Dal-B%c3%b3%20-%20UFSCar%20-%20PPGEQ.pdf6836fcdad2479c778f7f352501e3a180MD51[2021] Carta comprovante - Vanessa Dal-Bó - UFSCar - PPGEQ.pdf[2021] Carta comprovante - Vanessa Dal-Bó - UFSCar - PPGEQ.pdf[2021] Carta comprovante - Vanessa Dal-Bó - UFSCar - PPGEQapplication/pdf68316https://{{ getenv "DSPACE_HOST" "repositorio.ufscar.br" }}/bitstream/ufscar/14435/3/%5b2021%5d%20Carta%20comprovante%20-%20Vanessa%20Dal-B%c3%b3%20-%20UFSCar%20-%20PPGEQ.pdf120044d55458e1dc2d63ee706bf7befbMD53TEXT[2021] Tese - Vanessa Dal-Bó - UFSCar - PPGEQ.pdf.txt[2021] Tese - Vanessa Dal-Bó - UFSCar - PPGEQ.pdf.txtExtracted texttext/plain340060https://{{ getenv "DSPACE_HOST" "repositorio.ufscar.br" }}/bitstream/ufscar/14435/5/%5b2021%5d%20Tese%20-%20Vanessa%20Dal-B%c3%b3%20-%20UFSCar%20-%20PPGEQ.pdf.txt370d17df453de8580435f92936c4e4feMD55[2021] Carta comprovante - Vanessa Dal-Bó - UFSCar - PPGEQ.pdf.txt[2021] Carta comprovante - Vanessa Dal-Bó - UFSCar - PPGEQ.pdf.txtExtracted texttext/plain1073https://{{ getenv "DSPACE_HOST" "repositorio.ufscar.br" }}/bitstream/ufscar/14435/7/%5b2021%5d%20Carta%20comprovante%20-%20Vanessa%20Dal-B%c3%b3%20-%20UFSCar%20-%20PPGEQ.pdf.txt0d267b4a72c71369d93ce954345711a5MD57THUMBNAIL[2021] Tese - Vanessa Dal-Bó - UFSCar - PPGEQ.pdf.jpg[2021] Tese - Vanessa Dal-Bó - UFSCar - PPGEQ.pdf.jpgIM Thumbnailimage/jpeg5719https://{{ getenv "DSPACE_HOST" "repositorio.ufscar.br" }}/bitstream/ufscar/14435/6/%5b2021%5d%20Tese%20-%20Vanessa%20Dal-B%c3%b3%20-%20UFSCar%20-%20PPGEQ.pdf.jpg2c445ad916e8a71f7e9458663a4a7935MD56[2021] Carta comprovante - Vanessa Dal-Bó - UFSCar - PPGEQ.pdf.jpg[2021] Carta comprovante - Vanessa Dal-Bó - UFSCar - PPGEQ.pdf.jpgIM Thumbnailimage/jpeg12181https://{{ getenv "DSPACE_HOST" "repositorio.ufscar.br" }}/bitstream/ufscar/14435/8/%5b2021%5d%20Carta%20comprovante%20-%20Vanessa%20Dal-B%c3%b3%20-%20UFSCar%20-%20PPGEQ.pdf.jpga9749eb8f2d534c48eb6c2aec125c828MD58ufscar/144352021-06-28 03:20:58.085oai:repositorio.ufscar.br:ufscar/14435Repositório InstitucionalPUBhttps://repositorio.ufscar.br/oai/requestopendoar:43222023-05-25T13:01:32.166375Repositório Institucional da UFSCAR - Universidade Federal de São Carlos (UFSCAR)false
dc.title.por.fl_str_mv Estudo da secagem da polpa do abacate (Persea americana)
dc.title.alternative.eng.fl_str_mv Study of the drying of avocado pulp (Persea americana)
title Estudo da secagem da polpa do abacate (Persea americana)
spellingShingle Estudo da secagem da polpa do abacate (Persea americana)
Dal-Bó, Vanessa
Secagem
Congelamento
Reidratação
Compostos fenólicos
Síntese de Processos
Freeze-drying
Drying
Freeze
Rehydration
Phenolic compounds
Process synthesis
ENGENHARIAS::ENGENHARIA QUIMICA::PROCESSOS INDUSTRIAIS DE ENGENHARIA QUIMICA
ENGENHARIAS
title_short Estudo da secagem da polpa do abacate (Persea americana)
title_full Estudo da secagem da polpa do abacate (Persea americana)
title_fullStr Estudo da secagem da polpa do abacate (Persea americana)
title_full_unstemmed Estudo da secagem da polpa do abacate (Persea americana)
title_sort Estudo da secagem da polpa do abacate (Persea americana)
author Dal-Bó, Vanessa
author_facet Dal-Bó, Vanessa
author_role author
dc.contributor.authorlattes.por.fl_str_mv http://lattes.cnpq.br/7303635607073176
dc.contributor.author.fl_str_mv Dal-Bó, Vanessa
dc.contributor.advisor1.fl_str_mv Freire, José Teixeira
dc.contributor.advisor1Lattes.fl_str_mv http://lattes.cnpq.br/2270677706718167
contributor_str_mv Freire, José Teixeira
dc.subject.por.fl_str_mv Secagem
Congelamento
Reidratação
Compostos fenólicos
Síntese de Processos
topic Secagem
Congelamento
Reidratação
Compostos fenólicos
Síntese de Processos
Freeze-drying
Drying
Freeze
Rehydration
Phenolic compounds
Process synthesis
ENGENHARIAS::ENGENHARIA QUIMICA::PROCESSOS INDUSTRIAIS DE ENGENHARIA QUIMICA
ENGENHARIAS
dc.subject.eng.fl_str_mv Freeze-drying
Drying
Freeze
Rehydration
Phenolic compounds
Process synthesis
dc.subject.cnpq.fl_str_mv ENGENHARIAS::ENGENHARIA QUIMICA::PROCESSOS INDUSTRIAIS DE ENGENHARIA QUIMICA
ENGENHARIAS
description The drying process can be carried out by different methods, but the choice directly influences the quality of the final product, which can obviously be affected by operational conditions. This work aims to study the drying of the avocado pulp, through process optimization and experimental analysis. To achieve the proposed objective, this study was divided into two stages. Initially, the equipment to be used for drying the fruit pulp was defined. For this, the process synthesis techniques were applied, such as making the branch-and-bound trees, heuristic rules and determination the base flowchart, using the fuzzy logic method. From the application of the process synthesis, the lyophilization equipment proved to be promising for the drying process of the fruit pulp. After, considering that the knowledge of the drying rate is essential in the choice of suitable conditions for the lyophilization process, and the experimental data obtained to determine the drying kinetics, in the simplest lyophilizer, are measured in a discontinuous way, through destructive analysis, a simplest and low-cost setup for a laboratory-scale lyophilizer was developed, with an automated data acquisition system. The setup made it possible to obtain the drying kinetics curves, the temperature of the material as a function of time and the pressure difference, in addition to controlling different temperatures of the heating tray. The study was evaluated for the drying of the avocado pulp with heating temperature of 30, 40, 50 ° C and also without the supplying controlled of heat. The data acquisition system implemented proved to be satisfactory for the conditions evaluated. As expected, the load cell was influenced by the operating conditions, but the data was reproducible, so it was possible to minimize errors in the measurement of mass. The controlled supply of heat during lyophilization accelerated the process and, consequently, had a direct influence on the drying rate. In addition to the tests related to lyophilization of the avocado pulp, the influence of drying on the morphology, thermal decomposition, rehydration capacity, color, phenolic compounds and antioxidant activity of the fruit pulp was verified. It was observed that the heating temperature had an influence on the evaluated parameters, with temperatures of 40 and 50 ° C being the most appropriate for the process of dehydration of the fruit pulp. This study proved to be important for the analysis of the steps that occur during the lyophilization process.
publishDate 2021
dc.date.accessioned.fl_str_mv 2021-06-25T21:40:28Z
dc.date.available.fl_str_mv 2021-06-25T21:40:28Z
dc.date.issued.fl_str_mv 2021-04-26
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dc.identifier.citation.fl_str_mv DAL-BÓ, Vanessa. Estudo da secagem da polpa do abacate (Persea americana). 2021. Tese (Doutorado em Engenharia Química) – Universidade Federal de São Carlos, São Carlos, 2021. Disponível em: https://repositorio.ufscar.br/handle/ufscar/14435.
dc.identifier.uri.fl_str_mv https://repositorio.ufscar.br/handle/ufscar/14435
identifier_str_mv DAL-BÓ, Vanessa. Estudo da secagem da polpa do abacate (Persea americana). 2021. Tese (Doutorado em Engenharia Química) – Universidade Federal de São Carlos, São Carlos, 2021. Disponível em: https://repositorio.ufscar.br/handle/ufscar/14435.
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