Modificação microestrutural da liga Al-Si 380 conformada por spray com a co-injeção de partículas contendo fases intermetálicas

Detalhes bibliográficos
Ano de defesa: 2007
Autor(a) principal: Bereta, Luiz Antonio
Orientador(a): Bolfarini, Claudemiro lattes
Banca de defesa: Não Informado pela instituição
Tipo de documento: Tese
Tipo de acesso: Acesso aberto
Idioma: por
Instituição de defesa: Universidade Federal de São Carlos
Programa de Pós-Graduação: Programa de Pós-Graduação em Ciência e Engenharia de Materiais - PPGCEM
Departamento: Não Informado pela instituição
País: BR
Palavras-chave em Português:
Área do conhecimento CNPq:
Link de acesso: https://repositorio.ufscar.br/handle/ufscar/698
Resumo: The aim of this work was to determine the microstructure and the mechanical properties of a spray formed Al-Si 380 alloy in different conditions as follow: co-injection of particles containing intermetallic phases, extrusion and heat treatment in the deposits. The wear resistance was also evaluated. The microstructure was determined as a function of two different composition applied in the co-injection, two processing routes (spray formed with or without extrusion) and two heat treatment condition (present or not). The composition of the co-injection particles was selected aiming to improve the formation of α-Al(Fe,Mn)Si instead of β-Al(Fe,Mn)Si intermetallic, with Thermocalc program. The microstructure of the deposit was characterized by scanning electron microscopy (SEM) coupled with microanalysis (EDS) and the length of the needle-like phases (-Al(Fe,Mn)Si) was measured. The processing condition that formed the smallest average length of the -Al(Fe,Mn)Si was extruded and heat treated. An extra heat was processed with Mg addition in order to improve the precipitation hardening. The samples were tested in tension at room temperature, 100 oC, 200 oC e 300 oC. The wear tests were carried out at a sliding speed of 0,48 m/s and at the load of 500g, 800g and 1000g, in a 2,5 mm diameter samples. The co-injection of the particles containing the α-Al(Fe,Mn)Si phase was effective in decreasing the β-Al(Fe,Mn)Si phase length and promote the increase of the elongation values. The artificial aging heat treatment was effective in increase the yield and ultimate tensile strengths without decrease significantly the elongation. The Mg addition promoted an additional increase of the yield and ultimate tensile strengths. The wear tests show that no statistical difference was observed among the evaluated samples, according to test parameters selected.
id SCAR_6ee423584fab4098755b40a4c3d9ca9e
oai_identifier_str oai:repositorio.ufscar.br:ufscar/698
network_acronym_str SCAR
network_name_str Repositório Institucional da UFSCAR
repository_id_str
spelling Bereta, Luiz AntonioBolfarini, Claudemirohttp://lattes.cnpq.br/9231627080617037http://lattes.cnpq.br/87068339952438162016-06-02T19:10:11Z2012-10-302016-06-02T19:10:11Z2007-12-19BERETA, Luiz Antonio. Microstructure modification of spray formed al-si 380 alloy with the CO-injection of particles containning intermetallic phases. 2007. 132 f. Tese (Doutorado em Ciências Exatas e da Terra) - Universidade Federal de São Carlos, São Carlos, 2007.https://repositorio.ufscar.br/handle/ufscar/698The aim of this work was to determine the microstructure and the mechanical properties of a spray formed Al-Si 380 alloy in different conditions as follow: co-injection of particles containing intermetallic phases, extrusion and heat treatment in the deposits. The wear resistance was also evaluated. The microstructure was determined as a function of two different composition applied in the co-injection, two processing routes (spray formed with or without extrusion) and two heat treatment condition (present or not). The composition of the co-injection particles was selected aiming to improve the formation of α-Al(Fe,Mn)Si instead of β-Al(Fe,Mn)Si intermetallic, with Thermocalc program. The microstructure of the deposit was characterized by scanning electron microscopy (SEM) coupled with microanalysis (EDS) and the length of the needle-like phases (-Al(Fe,Mn)Si) was measured. The processing condition that formed the smallest average length of the -Al(Fe,Mn)Si was extruded and heat treated. An extra heat was processed with Mg addition in order to improve the precipitation hardening. The samples were tested in tension at room temperature, 100 oC, 200 oC e 300 oC. The wear tests were carried out at a sliding speed of 0,48 m/s and at the load of 500g, 800g and 1000g, in a 2,5 mm diameter samples. The co-injection of the particles containing the α-Al(Fe,Mn)Si phase was effective in decreasing the β-Al(Fe,Mn)Si phase length and promote the increase of the elongation values. The artificial aging heat treatment was effective in increase the yield and ultimate tensile strengths without decrease significantly the elongation. The Mg addition promoted an additional increase of the yield and ultimate tensile strengths. The wear tests show that no statistical difference was observed among the evaluated samples, according to test parameters selected.Este trabalho teve por objetivo determinar a microestrutura e as propriedades mecânicas da liga Al-Si 380 processada via conformação por spray, em diferentes condições, a saber: co-injeção de partículas contendo fases intermetálicas, extrusão dos depósitos e tratamento térmico. Foi avaliada também a resistência ao desgaste. A microestrutura foi determinada em função de duas composições diferentes que foram empregadas para co-injeção, duas condições de processamento (conformado por spray com e sem extrusão) e duas condições de tratamento térmico (presente/ausente). A composição das partículas co-injetadas foi projetada objetivando a formação da fase intermetálica α-Al(Fe,Mn)Si em detrimento a β-Al(Fe,Mn)Si, com emprego do programa Thermocalc. Os depósitos da liga Al-Si 380 foram caracterizados por MEV/EDS e as fases com morfologia de agulha (β-Al(Fe,Mn)Si) foram mensuradas. A condição com menor comprimento médio das partículas da fase β-Al(Fe,Mn)Si foi extrudada e tratada termicamente, além de sofrer adição de Mg em uma das condições. O ensaio de tração foi realizado à temperatura ambiente, 100 oC, 200 oC e 300 oC. O ensaio de desgaste foi realizado a uma velocidade de 0,48m/s, sendo aplicadas três cargas diferentes: 500g, 800g e 1000g, em um corpo de prova de 2,5 mm de diâmetro. A co-injeção das partículas da fase α-Al(Fe,Mn)Si foi efetiva em diminuir o comprimento da fase β-Al(Fe,Mn)Si no depósito e levou ao aumento do alongamento até a fratura do material obtido. O tratamento térmico de envelhecimento artificial aplicado foi efetivo em aumentar os limites de resistência e escoamento sem, entretanto, implicar em diminuição significativa do alongamento até a fratura. A adição de Mg aumentou ainda mais os limites de resistência e escoamento. Os ensaios de desgastes evidenciaram que não existem, estatisticamente, diferenças significativas dentre as amostras avaliadas, segundo os parâmetros do ensaio empregado.Universidade Federal de Sao Carlosapplication/pdfporUniversidade Federal de São CarlosPrograma de Pós-Graduação em Ciência e Engenharia de Materiais - PPGCEMUFSCarBRLigas de alumínioConformação por sprayCoinjeçãoMicroestruturaCompostos intermetálicosENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICAModificação microestrutural da liga Al-Si 380 conformada por spray com a co-injeção de partículas contendo fases intermetálicasMicrostructure modification of spray formed al-si 380 alloy with the CO-injection of particles containning intermetallic phasesinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/doctoralThesisinfo:eu-repo/semantics/openAccessreponame:Repositório Institucional da UFSCARinstname:Universidade Federal de São Carlos (UFSCAR)instacron:UFSCARORIGINAL4636.pdfapplication/pdf4081013https://{{ getenv "DSPACE_HOST" "repositorio.ufscar.br" }}/bitstream/ufscar/698/1/4636.pdf43647aa9920214a912b94ee9ef6ce97aMD51TEXT4636.pdf.txt4636.pdf.txtExtracted texttext/plain0https://{{ getenv "DSPACE_HOST" "repositorio.ufscar.br" }}/bitstream/ufscar/698/2/4636.pdf.txtd41d8cd98f00b204e9800998ecf8427eMD52THUMBNAIL4636.pdf.jpg4636.pdf.jpgIM Thumbnailimage/jpeg6518https://{{ getenv "DSPACE_HOST" "repositorio.ufscar.br" }}/bitstream/ufscar/698/3/4636.pdf.jpg894fa5c709f7cda0c35d9c134857a0a6MD53ufscar/6982019-09-11 04:04:12.217oai:repositorio.ufscar.br:ufscar/698Repositório InstitucionalPUBhttps://repositorio.ufscar.br/oai/requestopendoar:43222023-05-25T12:43:36.838798Repositório Institucional da UFSCAR - Universidade Federal de São Carlos (UFSCAR)false
dc.title.por.fl_str_mv Modificação microestrutural da liga Al-Si 380 conformada por spray com a co-injeção de partículas contendo fases intermetálicas
dc.title.alternative.eng.fl_str_mv Microstructure modification of spray formed al-si 380 alloy with the CO-injection of particles containning intermetallic phases
title Modificação microestrutural da liga Al-Si 380 conformada por spray com a co-injeção de partículas contendo fases intermetálicas
spellingShingle Modificação microestrutural da liga Al-Si 380 conformada por spray com a co-injeção de partículas contendo fases intermetálicas
Bereta, Luiz Antonio
Ligas de alumínio
Conformação por spray
Coinjeção
Microestrutura
Compostos intermetálicos
ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA
title_short Modificação microestrutural da liga Al-Si 380 conformada por spray com a co-injeção de partículas contendo fases intermetálicas
title_full Modificação microestrutural da liga Al-Si 380 conformada por spray com a co-injeção de partículas contendo fases intermetálicas
title_fullStr Modificação microestrutural da liga Al-Si 380 conformada por spray com a co-injeção de partículas contendo fases intermetálicas
title_full_unstemmed Modificação microestrutural da liga Al-Si 380 conformada por spray com a co-injeção de partículas contendo fases intermetálicas
title_sort Modificação microestrutural da liga Al-Si 380 conformada por spray com a co-injeção de partículas contendo fases intermetálicas
author Bereta, Luiz Antonio
author_facet Bereta, Luiz Antonio
author_role author
dc.contributor.authorlattes.por.fl_str_mv http://lattes.cnpq.br/8706833995243816
dc.contributor.author.fl_str_mv Bereta, Luiz Antonio
dc.contributor.advisor1.fl_str_mv Bolfarini, Claudemiro
dc.contributor.advisor1Lattes.fl_str_mv http://lattes.cnpq.br/9231627080617037
contributor_str_mv Bolfarini, Claudemiro
dc.subject.por.fl_str_mv Ligas de alumínio
Conformação por spray
Coinjeção
Microestrutura
Compostos intermetálicos
topic Ligas de alumínio
Conformação por spray
Coinjeção
Microestrutura
Compostos intermetálicos
ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA
dc.subject.cnpq.fl_str_mv ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA
description The aim of this work was to determine the microstructure and the mechanical properties of a spray formed Al-Si 380 alloy in different conditions as follow: co-injection of particles containing intermetallic phases, extrusion and heat treatment in the deposits. The wear resistance was also evaluated. The microstructure was determined as a function of two different composition applied in the co-injection, two processing routes (spray formed with or without extrusion) and two heat treatment condition (present or not). The composition of the co-injection particles was selected aiming to improve the formation of α-Al(Fe,Mn)Si instead of β-Al(Fe,Mn)Si intermetallic, with Thermocalc program. The microstructure of the deposit was characterized by scanning electron microscopy (SEM) coupled with microanalysis (EDS) and the length of the needle-like phases (-Al(Fe,Mn)Si) was measured. The processing condition that formed the smallest average length of the -Al(Fe,Mn)Si was extruded and heat treated. An extra heat was processed with Mg addition in order to improve the precipitation hardening. The samples were tested in tension at room temperature, 100 oC, 200 oC e 300 oC. The wear tests were carried out at a sliding speed of 0,48 m/s and at the load of 500g, 800g and 1000g, in a 2,5 mm diameter samples. The co-injection of the particles containing the α-Al(Fe,Mn)Si phase was effective in decreasing the β-Al(Fe,Mn)Si phase length and promote the increase of the elongation values. The artificial aging heat treatment was effective in increase the yield and ultimate tensile strengths without decrease significantly the elongation. The Mg addition promoted an additional increase of the yield and ultimate tensile strengths. The wear tests show that no statistical difference was observed among the evaluated samples, according to test parameters selected.
publishDate 2007
dc.date.issued.fl_str_mv 2007-12-19
dc.date.available.fl_str_mv 2012-10-30
2016-06-02T19:10:11Z
dc.date.accessioned.fl_str_mv 2016-06-02T19:10:11Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/doctoralThesis
format doctoralThesis
status_str publishedVersion
dc.identifier.citation.fl_str_mv BERETA, Luiz Antonio. Microstructure modification of spray formed al-si 380 alloy with the CO-injection of particles containning intermetallic phases. 2007. 132 f. Tese (Doutorado em Ciências Exatas e da Terra) - Universidade Federal de São Carlos, São Carlos, 2007.
dc.identifier.uri.fl_str_mv https://repositorio.ufscar.br/handle/ufscar/698
identifier_str_mv BERETA, Luiz Antonio. Microstructure modification of spray formed al-si 380 alloy with the CO-injection of particles containning intermetallic phases. 2007. 132 f. Tese (Doutorado em Ciências Exatas e da Terra) - Universidade Federal de São Carlos, São Carlos, 2007.
url https://repositorio.ufscar.br/handle/ufscar/698
dc.language.iso.fl_str_mv por
language por
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.publisher.none.fl_str_mv Universidade Federal de São Carlos
dc.publisher.program.fl_str_mv Programa de Pós-Graduação em Ciência e Engenharia de Materiais - PPGCEM
dc.publisher.initials.fl_str_mv UFSCar
dc.publisher.country.fl_str_mv BR
publisher.none.fl_str_mv Universidade Federal de São Carlos
dc.source.none.fl_str_mv reponame:Repositório Institucional da UFSCAR
instname:Universidade Federal de São Carlos (UFSCAR)
instacron:UFSCAR
instname_str Universidade Federal de São Carlos (UFSCAR)
instacron_str UFSCAR
institution UFSCAR
reponame_str Repositório Institucional da UFSCAR
collection Repositório Institucional da UFSCAR
bitstream.url.fl_str_mv https://{{ getenv "DSPACE_HOST" "repositorio.ufscar.br" }}/bitstream/ufscar/698/1/4636.pdf
https://{{ getenv "DSPACE_HOST" "repositorio.ufscar.br" }}/bitstream/ufscar/698/2/4636.pdf.txt
https://{{ getenv "DSPACE_HOST" "repositorio.ufscar.br" }}/bitstream/ufscar/698/3/4636.pdf.jpg
bitstream.checksum.fl_str_mv 43647aa9920214a912b94ee9ef6ce97a
d41d8cd98f00b204e9800998ecf8427e
894fa5c709f7cda0c35d9c134857a0a6
bitstream.checksumAlgorithm.fl_str_mv MD5
MD5
MD5
repository.name.fl_str_mv Repositório Institucional da UFSCAR - Universidade Federal de São Carlos (UFSCAR)
repository.mail.fl_str_mv
_version_ 1767351055787491328