Clarifica??o de ?leo de milho em coluna de leito fixo usando sabugo de milho como adsorvente

Detalhes bibliográficos
Ano de defesa: 2012
Autor(a) principal: Freitas, Mayra Gomes Nicolau de lattes
Orientador(a): Meleiro, Luiz Augusto da Cruz lattes
Banca de defesa: Rojas, Edwin Elard Garcia, Pagani, M?nica Marques
Tipo de documento: Dissertação
Tipo de acesso: Acesso aberto
Idioma: por
Instituição de defesa: Universidade Federal Rural do Rio de Janeiro
Programa de Pós-Graduação: Programa de P?s-Gradua??o em Ci?ncia e Tecnologia de Alimentos
Departamento: Instituto de Tecnologia
País: Brasil
Palavras-chave em Português:
Palavras-chave em Inglês:
Área do conhecimento CNPq:
Link de acesso: https://tede.ufrrj.br/jspui/handle/jspui/3688
Resumo: Bleaching is one of the most important stages in the processing of vegetable oils. This processing step is currently carried out in discontinuous mode through adsorption of the oil pigments on appropriates bleaching clays. Brazilian food companies employ large amounts of imported clays that are difficult to regenerate, increase the bleaching costs, and generate a great quantity of industrial waste. This work proposes changes in the operation mode and in the adsorbent for the bleaching process. With this purpose, a column packed with triturated corncob operated in continuous mode was used for bleaching corn oil. Corncob was proposed as an alternative adsorbent because it is described in the literature as a material with great adsorption power, besides it is part of the corn oil production chain. Bleaching process was carried out in continuous mode in a packed-bed column with 0,5m length and 0,0508m diameter. The proposed process lead to clarification levels comparable to those using industrial bleaching clays, while decreasing around 30% the oil?s acidity without alkali addition.
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spelling Meleiro, Luiz Augusto da Cruz814.559.417-00http://lattes.cnpq.br/0883486364645272Mendes, Marisa Fernandeshttp://lattes.cnpq.br/3233683706295801Rojas, Edwin Elard GarciaPagani, M?nica Marques116.541.057-59http://lattes.cnpq.br/3379300361967119Freitas, Mayra Gomes Nicolau de2020-06-26T16:12:13Z2012-07-31FREITAS, Mayra Gomes Nicolau de. Clarifica??o de ?leo de milho em coluna de leito fixo usando sabugo de milho como adsorvente. 2012. 56 f. Disserta??o (Programa de P?s-Gradua??o em Ci?ncia e Tecnologia de Alimentos) - Universidade Federal Rural do Rio de Janeiro, Serop?dica.https://tede.ufrrj.br/jspui/handle/jspui/3688Bleaching is one of the most important stages in the processing of vegetable oils. This processing step is currently carried out in discontinuous mode through adsorption of the oil pigments on appropriates bleaching clays. Brazilian food companies employ large amounts of imported clays that are difficult to regenerate, increase the bleaching costs, and generate a great quantity of industrial waste. This work proposes changes in the operation mode and in the adsorbent for the bleaching process. With this purpose, a column packed with triturated corncob operated in continuous mode was used for bleaching corn oil. Corncob was proposed as an alternative adsorbent because it is described in the literature as a material with great adsorption power, besides it is part of the corn oil production chain. Bleaching process was carried out in continuous mode in a packed-bed column with 0,5m length and 0,0508m diameter. The proposed process lead to clarification levels comparable to those using industrial bleaching clays, while decreasing around 30% the oil?s acidity without alkali addition.A clarifica??o ? uma das etapas mais importantes no processamento de ?leos vegetais. Esta etapa geralmente ? conduzida em um processo descont?nuo atrav?s da adsor??o dos pigmentos que conferem cor aos ?leos em argilas adequadas para este fim. Nesta etapa, a ind?stria de alimentos faz uso de grandes quantidades de argilas importadas que, por serem de dif?cil recupera??o, encarecem o processo e geram grande quantidade de res?duo industrial. Devido a isso, este trabalho prop?e um estudo da viabilidade de uma mudan?a nesse processo, quanto ao modo de opera??o, e ao adsorvente utilizado na clarifica??o do ?leo de milho. Ensaios de clarifica??o foram conduzidos em modo cont?nuo e como adsorvente, a proposta foi de utilizar o sabugo de milho. Tal material ? descrito na literatura como de consider?vel poder adsortivo, faz parte da cadeia de produ??o do ?leo de milho, e a escolha do mesmo, oferece a vantagem da reutiliza??o de um res?duo agroindustrial. O processo de clarifica??o conduzido em modo cont?nuo foi realizado em uma coluna de leito fixo de 0,5 m de altura e 0,0508 m de di?metro, acoplada ? uma bomba dosadora e man?metros na entrada e na sa?da da coluna, para o acompanhamento da perda de carga causada pelo recheio. O ?leo de milho cru foi bombeado atrav?s do topo da coluna preenchida com leitos, constitu?dos de sabugo de milho triturado, argila comercial, e uma mistura dos dois. As amostras de ?leo clarificado foram coletadas no fundo da coluna. O processo teve seu desempenho avaliado com o monitoramento da despigmenta??o do ?leo cru, feito atrav?s de medidas da absorv?ncia do ?leo em faixa de comprimento de onda pr?- determinada, e do monitoramento do ?ndice de acidez livre das amostras. Os resultados obtidos permitem afirmar que o sabugo apresentou poder clarificante compar?vel ao das terras clarificantes; e poder neutralizante, capaz de reduzir a acidez livre das amostras em cerca de 30% no processo cont?nuo, sem a adi??o de ?lcali.Submitted by Celso Magalhaes (celsomagalhaes@ufrrj.br) on 2020-06-26T16:12:13Z No. of bitstreams: 1 2012 - Mayra Gomes Nicolau de Freitas.pdf: 1050748 bytes, checksum: edfec4cecf46ccc6469d0058050d8aad (MD5)Made available in DSpace on 2020-06-26T16:12:13Z (GMT). No. of bitstreams: 1 2012 - Mayra Gomes Nicolau de Freitas.pdf: 1050748 bytes, checksum: edfec4cecf46ccc6469d0058050d8aad (MD5) Previous issue date: 2012-07-31Coordena??o de Aperfei?oamento de Pessoal de n?vel Superior - CAPESapplication/pdfhttps://tede.ufrrj.br/retrieve/60986/2012%20-%20Mayra%20Gomes%20Nicolau%20de%20Freitas.pdf.jpgporUniversidade Federal Rural do Rio de JaneiroPrograma de P?s-Gradua??o em Ci?ncia e Tecnologia de AlimentosUFRRJBrasilInstituto de TecnologiaABOISSA ?LEOS VEGETAIS ?LEOS VEGETAIS. Soft Oils. ABOISSA News pdf. S?o Paulo, 2012 AHMAD, A.L.; CHAN, C.Y.; ABD SHUKOR, S.R.; MASHITAH, M.D. Adsorption kinetics and thermodynamics of ?-carotene on silica-based adsorbent. Chemical Engineering Journal, Mal?sia, v.148, p. 378-384, 2009 AMERICAN OIL CHEMISTS? SOCIETY. Official methods and recommended practices of the American Oil Chemistis? Society. USA: AOCS, (AOCS Official Method, Cd 8-53; Ca 5a-40; Cd 3-25), 1990 AMERICAN OIL CHEMISTS? SOCIETY. 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Journal of Environmental Management, Taiwan, v.92, p. 708- 713, 2011Adsor??oBranqueamento?leo vegetalBleaching. .AdsorptionVegetable OilCi?ncia e Tecnologia de AlimentosClarifica??o de ?leo de milho em coluna de leito fixo usando sabugo de milho como adsorventeBleaching corn oil in a fixed-bed column using agricultural waste as an adsorbentinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/masterThesisinfo:eu-repo/semantics/openAccessreponame:Biblioteca Digital de Teses e Dissertações da UFRRJinstname:Universidade Federal Rural do Rio de Janeiro (UFRRJ)instacron:UFRRJTHUMBNAIL2012 - Mayra Gomes Nicolau de Freitas.pdf.jpg2012 - Mayra Gomes Nicolau de Freitas.pdf.jpgimage/jpeg1943http://localhost:8080/tede/bitstream/jspui/3688/4/2012+-+Mayra+Gomes+Nicolau+de+Freitas.pdf.jpgcc73c4c239a4c332d642ba1e7c7a9fb2MD54TEXT2012 - Mayra Gomes Nicolau de Freitas.pdf.txt2012 - Mayra Gomes Nicolau de Freitas.pdf.txttext/plain161498http://localhost:8080/tede/bitstream/jspui/3688/3/2012+-+Mayra+Gomes+Nicolau+de+Freitas.pdf.txt1a0cc5250a12ecad1684c4b7fad97072MD53ORIGINAL2012 - Mayra Gomes Nicolau de Freitas.pdf2012 - Mayra Gomes Nicolau de Freitas.pdfapplication/pdf1050748http://localhost:8080/tede/bitstream/jspui/3688/2/2012+-+Mayra+Gomes+Nicolau+de+Freitas.pdfedfec4cecf46ccc6469d0058050d8aadMD52LICENSElicense.txtlicense.txttext/plain; charset=utf-82089http://localhost:8080/tede/bitstream/jspui/3688/1/license.txt7b5ba3d2445355f386edab96125d42b7MD51jspui/36882022-08-11 15:13:36.447oai:localhost: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Biblioteca Digital de Teses e Dissertaçõeshttps://tede.ufrrj.br/PUBhttps://tede.ufrrj.br/oai/requestbibliot@ufrrj.br||bibliot@ufrrj.bropendoar:2022-08-11T18:13:36Biblioteca Digital de Teses e Dissertações da UFRRJ - Universidade Federal Rural do Rio de Janeiro (UFRRJ)false
dc.title.por.fl_str_mv Clarifica??o de ?leo de milho em coluna de leito fixo usando sabugo de milho como adsorvente
dc.title.alternative.eng.fl_str_mv Bleaching corn oil in a fixed-bed column using agricultural waste as an adsorbent
title Clarifica??o de ?leo de milho em coluna de leito fixo usando sabugo de milho como adsorvente
spellingShingle Clarifica??o de ?leo de milho em coluna de leito fixo usando sabugo de milho como adsorvente
Freitas, Mayra Gomes Nicolau de
Adsor??o
Branqueamento
?leo vegetal
Bleaching. .
Adsorption
Vegetable Oil
Ci?ncia e Tecnologia de Alimentos
title_short Clarifica??o de ?leo de milho em coluna de leito fixo usando sabugo de milho como adsorvente
title_full Clarifica??o de ?leo de milho em coluna de leito fixo usando sabugo de milho como adsorvente
title_fullStr Clarifica??o de ?leo de milho em coluna de leito fixo usando sabugo de milho como adsorvente
title_full_unstemmed Clarifica??o de ?leo de milho em coluna de leito fixo usando sabugo de milho como adsorvente
title_sort Clarifica??o de ?leo de milho em coluna de leito fixo usando sabugo de milho como adsorvente
author Freitas, Mayra Gomes Nicolau de
author_facet Freitas, Mayra Gomes Nicolau de
author_role author
dc.contributor.advisor1.fl_str_mv Meleiro, Luiz Augusto da Cruz
dc.contributor.advisor1ID.fl_str_mv 814.559.417-00
dc.contributor.advisor1Lattes.fl_str_mv http://lattes.cnpq.br/0883486364645272
dc.contributor.advisor-co1.fl_str_mv Mendes, Marisa Fernandes
dc.contributor.advisor-co1Lattes.fl_str_mv http://lattes.cnpq.br/3233683706295801
dc.contributor.referee1.fl_str_mv Rojas, Edwin Elard Garcia
dc.contributor.referee2.fl_str_mv Pagani, M?nica Marques
dc.contributor.authorID.fl_str_mv 116.541.057-59
dc.contributor.authorLattes.fl_str_mv http://lattes.cnpq.br/3379300361967119
dc.contributor.author.fl_str_mv Freitas, Mayra Gomes Nicolau de
contributor_str_mv Meleiro, Luiz Augusto da Cruz
Mendes, Marisa Fernandes
Rojas, Edwin Elard Garcia
Pagani, M?nica Marques
dc.subject.por.fl_str_mv Adsor??o
Branqueamento
?leo vegetal
topic Adsor??o
Branqueamento
?leo vegetal
Bleaching. .
Adsorption
Vegetable Oil
Ci?ncia e Tecnologia de Alimentos
dc.subject.eng.fl_str_mv Bleaching. .
Adsorption
Vegetable Oil
dc.subject.cnpq.fl_str_mv Ci?ncia e Tecnologia de Alimentos
description Bleaching is one of the most important stages in the processing of vegetable oils. This processing step is currently carried out in discontinuous mode through adsorption of the oil pigments on appropriates bleaching clays. Brazilian food companies employ large amounts of imported clays that are difficult to regenerate, increase the bleaching costs, and generate a great quantity of industrial waste. This work proposes changes in the operation mode and in the adsorbent for the bleaching process. With this purpose, a column packed with triturated corncob operated in continuous mode was used for bleaching corn oil. Corncob was proposed as an alternative adsorbent because it is described in the literature as a material with great adsorption power, besides it is part of the corn oil production chain. Bleaching process was carried out in continuous mode in a packed-bed column with 0,5m length and 0,0508m diameter. The proposed process lead to clarification levels comparable to those using industrial bleaching clays, while decreasing around 30% the oil?s acidity without alkali addition.
publishDate 2012
dc.date.issued.fl_str_mv 2012-07-31
dc.date.accessioned.fl_str_mv 2020-06-26T16:12:13Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/masterThesis
format masterThesis
status_str publishedVersion
dc.identifier.citation.fl_str_mv FREITAS, Mayra Gomes Nicolau de. Clarifica??o de ?leo de milho em coluna de leito fixo usando sabugo de milho como adsorvente. 2012. 56 f. Disserta??o (Programa de P?s-Gradua??o em Ci?ncia e Tecnologia de Alimentos) - Universidade Federal Rural do Rio de Janeiro, Serop?dica.
dc.identifier.uri.fl_str_mv https://tede.ufrrj.br/jspui/handle/jspui/3688
identifier_str_mv FREITAS, Mayra Gomes Nicolau de. Clarifica??o de ?leo de milho em coluna de leito fixo usando sabugo de milho como adsorvente. 2012. 56 f. Disserta??o (Programa de P?s-Gradua??o em Ci?ncia e Tecnologia de Alimentos) - Universidade Federal Rural do Rio de Janeiro, Serop?dica.
url https://tede.ufrrj.br/jspui/handle/jspui/3688
dc.language.iso.fl_str_mv por
language por
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