Avaliação das propriedades mecânicas e microestrutura de concreto de ultra alto desempenho com adições minerais e resíduos industriais

Detalhes bibliográficos
Ano de defesa: 2020
Autor(a) principal: Sokolovicz, Bóris Casanova lattes
Orientador(a): Isaia, Geraldo Cechella lattes
Banca de defesa: Tutikian, Bernardo Fonseca lattes, Hoppe Filho, Juarez lattes, Vargas, Alexandre Silva de lattes, Lübeck, André lattes
Tipo de documento: Tese
Tipo de acesso: Acesso aberto
Idioma: por
Instituição de defesa: Universidade Federal de Santa Maria
Centro de Tecnologia
Programa de Pós-Graduação: Programa de Pós-Graduação em Engenharia Civil
Departamento: Engenharia Civil
País: Brasil
Palavras-chave em Português:
Palavras-chave em Inglês:
Área do conhecimento CNPq:
Link de acesso: http://repositorio.ufsm.br/handle/1/19866
Resumo: With the increase in the world population, civil construction is the largest consumer of resources, with great environmental impact. One of the ways to reduce this impact is to increase the mechanical strength of the concrete, reducing the resistant sections of the structural parts, dematerializing them from the emanation of greenhouse gases. The use of industrial and pozzolan waste in concrete, in addition to the packaging of particles, are concrete actions that reduce environmental impacts, increasing sustainability. Thus, the general objective of this research was to analyze the microstructure and physical-mechanical properties of ultra high performance concrete (UHPC) with hydrated lime, foundry sand, pozzolanic and inert mineral additions, through the packaging effects of the particles. The specific objectives were: to evaluate the workability of UHPC with rice husk ash (RHA), fly ash (FA), lime CH I, limestone filler (LF), quartz powder and foundry sand, in relation to the reference concrete, with structural white cement, silica fume (SF), quartz powder and sand industrial; study the packaging of particles by the modified Andreassen method; analyze the performance of variables related to the mechanical strength of concrete in wet and thermal cures: axial compression, modulus of elasticity and instrumented breaks; and analyze the microstructure of UHPC mixtures by: X-Ray Diffraction (XRD), Thermogravimetric Analysis (TG/DTG), Fourier Transform Infrared (FTIR) and Scanning Electron Microscopy (SEM/EDS). The greatest resistance for all ages was the REF mixture. The efficiency of thermal curing was verified, mainly in early ages, with emphasis on the mixture with 15% partial replacement of cement with rice husk ash (RHA15). For mixtures with mineral additions, the similar behavior was noticeable. This performance confirms that the physical effect was representative, because, even with changes in levels and types of mineral additions, the average clinker intensity did not vary significantly. The elasticity modules showed the same trend of resistance behavior. In instrumented breaks, the stresses were proportional to the specific deformations in almost the entire test. In mixtures with mineral additions (RHA15, FA15, RHA10-FA5 and RHA10-LF5), the deformations were greater, attesting to the less fragile behavior. In XRD, the presence of non-hydrated compounds (alite and belite) was observed due to the low a / mc ratio. In mixtures with the addition of lime there was an increase in the peaks of portlandite and calcite, showing that a portion of the lime did not react with the pozzolana. In TG-DTG, mixtures with mineral additions had higher levels of combined water, calcium hydroxide (CH) and carbonates than REF, attesting that the lime partially reacted with the pozzolan. In FTIR, the REF mixture showed low peaks of portlandite, the opposite behavior of mixtures with mineral additions. In SEM, it was found that mixtures with mineral additions showed higher levels of Ca / Si ratio when compared to the reference concrete.
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spelling 2020-05-15T16:18:15Z2020-05-15T16:18:15Z2020-01-07http://repositorio.ufsm.br/handle/1/19866With the increase in the world population, civil construction is the largest consumer of resources, with great environmental impact. One of the ways to reduce this impact is to increase the mechanical strength of the concrete, reducing the resistant sections of the structural parts, dematerializing them from the emanation of greenhouse gases. The use of industrial and pozzolan waste in concrete, in addition to the packaging of particles, are concrete actions that reduce environmental impacts, increasing sustainability. Thus, the general objective of this research was to analyze the microstructure and physical-mechanical properties of ultra high performance concrete (UHPC) with hydrated lime, foundry sand, pozzolanic and inert mineral additions, through the packaging effects of the particles. The specific objectives were: to evaluate the workability of UHPC with rice husk ash (RHA), fly ash (FA), lime CH I, limestone filler (LF), quartz powder and foundry sand, in relation to the reference concrete, with structural white cement, silica fume (SF), quartz powder and sand industrial; study the packaging of particles by the modified Andreassen method; analyze the performance of variables related to the mechanical strength of concrete in wet and thermal cures: axial compression, modulus of elasticity and instrumented breaks; and analyze the microstructure of UHPC mixtures by: X-Ray Diffraction (XRD), Thermogravimetric Analysis (TG/DTG), Fourier Transform Infrared (FTIR) and Scanning Electron Microscopy (SEM/EDS). The greatest resistance for all ages was the REF mixture. The efficiency of thermal curing was verified, mainly in early ages, with emphasis on the mixture with 15% partial replacement of cement with rice husk ash (RHA15). For mixtures with mineral additions, the similar behavior was noticeable. This performance confirms that the physical effect was representative, because, even with changes in levels and types of mineral additions, the average clinker intensity did not vary significantly. The elasticity modules showed the same trend of resistance behavior. In instrumented breaks, the stresses were proportional to the specific deformations in almost the entire test. In mixtures with mineral additions (RHA15, FA15, RHA10-FA5 and RHA10-LF5), the deformations were greater, attesting to the less fragile behavior. In XRD, the presence of non-hydrated compounds (alite and belite) was observed due to the low a / mc ratio. In mixtures with the addition of lime there was an increase in the peaks of portlandite and calcite, showing that a portion of the lime did not react with the pozzolana. In TG-DTG, mixtures with mineral additions had higher levels of combined water, calcium hydroxide (CH) and carbonates than REF, attesting that the lime partially reacted with the pozzolan. In FTIR, the REF mixture showed low peaks of portlandite, the opposite behavior of mixtures with mineral additions. In SEM, it was found that mixtures with mineral additions showed higher levels of Ca / Si ratio when compared to the reference concrete.Com o aumento da população mundial, a construção civil é a maior consumidora de recursos, com grande impacto ambiental. Uma das maneiras de diminuir esse impacto é aumentar a resistência mecânica do concreto, reduzindo as seções resistentes das peças estruturais, desmaterializando-as da emanação dos gases do efeito estufa. A utilização no concreto de resíduos industriais e pozolana, além do empacotamento das partículas, são ações concretas que diminuem os impactos ambientais, aumentando a sustentabilidade. Assim, o objetivo geral desta pesquisa foi analisar a microestrutura e propriedades físico-mecânicas de concreto de ultra alto desempenho (CUAD) com cal hidratada, areia de fundição, adições minerais pozolânicas e inerte, através dos efeitos de empacotamento das partículas. Os objetivos específicos foram: avaliar a trabalhabilidade do CUAD com cinza de casca de arroz (CCA), cinza volante (CV), cal CH I, fíler calcário, pó de quartzo e areia de fundição, em relação ao concreto de referência, com cimento branco estrutural, sílica ativa, pó de quartzo e areia industrial; estudar o empacotamento das partículas pelo método de Andreassen modificado; analisar o desempenho das variáveis relacionadas com a resistência mecânica do concreto em curas úmida e térmica: compressão axial, módulo de elasticidade e rompimentos instrumentados; analisar a microestrutura das misturas do CUAD por: Difração de Raios X (DRX), Análise termogravimétrica (TG/DTG), Infravermelho com transformada de Fourier (FTIR) e Microscopia Eletrônica de Varredura MEV/EDS. As maiores resistências para todas as idades foram da mistura REF. Verificou-se a eficiência da cura térmica, principalmente em idades iniciais, com destaque para a mistura com 15% de substituição parcial de cimento por cinza de casca de arroz (CCA15). Para as misturas com adições minerais, ficou perceptível o comportamento semelhante. Esse desempenho ratifica que o efeito físico foi representativo, pois, mesmo com alterações de teores e de tipos de adições minerais, a intensidade de clínquer média não variou significativamente. Os módulos de elasticidade apresentaram a mesma tendência de comportamento da resistência. Nos rompimentos instrumentados as tensões foram proporcionais às deformações específicas em quase todo o ensaio. Nas misturas com adições minerais (CCA15, CV15, CCA10-CV5 e CCA10-FC5), as deformações foram maiores, atestando o comportamento menos frágil. No DRX, observou-se presença de compostos não hidratados (alita e belita) devido à baixa relação a/mc. Nas misturas com adição de cal houve acréscimo nos picos de portlandita e calcita, evidenciando que uma parcela da cal não reagiu com a pozolana. No TG-DTG as misturas com adições minerais tiveram maiores níveis de água combinada, hidróxido de cálcio (CH) e carbonatos que a REF, atestando que a cal reagiu parcialmente com a pozolana. No FTIR a mistura REF apresentou baixos picos de portlandita, comportamento oposto das misturas com adições minerais. No MEV, verificou-se que as misturas com adições minerais apresentaram níveis mais elevados de relação Ca/Si quando comparados ao concreto referência.porUniversidade Federal de Santa MariaCentro de TecnologiaPrograma de Pós-Graduação em Engenharia CivilUFSMBrasilEngenharia CivilAttribution-NonCommercial-NoDerivatives 4.0 Internationalhttp://creativecommons.org/licenses/by-nc-nd/4.0/info:eu-repo/semantics/openAccessConcreto de ultra alto desempenhoPropriedades mecânicasMicroestruturaSustentabilidadePozolanasEmpacotamento de partículasMicrostructureUltra high performance concreteMechanical propertiesSustainabilityPozzolansParticles packingCNPQ::ENGENHARIAS::ENGENHARIA CIVILAvaliação das propriedades mecânicas e microestrutura de concreto de ultra alto desempenho com adições minerais e resíduos industriaisEvaluation of mechanical properties and microstructure of ultra high performance concrete with mineral additions and industrial wasteinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/doctoralThesisIsaia, Geraldo Cechellahttp://lattes.cnpq.br/8260652949733370Tutikian, Bernardo Fonsecahttp://lattes.cnpq.br/9916860252080305Hoppe Filho, Juarezhttp://lattes.cnpq.br/8692521256968834Vargas, Alexandre Silva dehttp://lattes.cnpq.br/6501148372644975Lübeck, Andréhttp://lattes.cnpq.br/7511022637484145http://lattes.cnpq.br/8038983210001144Sokolovicz, Bóris Casanova3001000000036006005d5ff349-6e1b-45f0-a3fc-dfb31b446decc5c762b4-ae1d-451d-b3c8-3433bb3acd5bf18993ee-de36-4b05-b08c-ecae584ce62aa11aafd1-61d8-4a76-adf1-858f7f7146efe6a60716-9532-480b-817e-af617f323759ef9b6201-2cb1-40a2-80fa-d9652b40742areponame:Biblioteca Digital de Teses e Dissertações do UFSMinstname:Universidade Federal de Santa Maria (UFSM)instacron:UFSMORIGINALTES_PPGEC_2020_SOKOLOVICZ _BORIS_CASANOVA.pdfTES_PPGEC_2020_SOKOLOVICZ _BORIS_CASANOVA.pdfTese de Doutoradoapplication/pdf22900659http://repositorio.ufsm.br/bitstream/1/19866/1/TES_PPGEC_2020_SOKOLOVICZ%20_BORIS_CASANOVA.pdf762d483296218a57f43aac00481d7345MD51CC-LICENSElicense_rdflicense_rdfapplication/rdf+xml; charset=utf-8805http://repositorio.ufsm.br/bitstream/1/19866/2/license_rdf4460e5956bc1d1639be9ae6146a50347MD52LICENSElicense.txtlicense.txttext/plain; charset=utf-816http://repositorio.ufsm.br/bitstream/1/19866/3/license.txt6eeec7985884eb94336b41cc5308bf0fMD53TEXTTES_PPGEC_2020_SOKOLOVICZ _BORIS_CASANOVA.pdf.txtTES_PPGEC_2020_SOKOLOVICZ _BORIS_CASANOVA.pdf.txtExtracted texttext/plain436411http://repositorio.ufsm.br/bitstream/1/19866/4/TES_PPGEC_2020_SOKOLOVICZ%20_BORIS_CASANOVA.pdf.txt69108f1a30df390ebcae403951dbbf57MD54THUMBNAILTES_PPGEC_2020_SOKOLOVICZ _BORIS_CASANOVA.pdf.jpgTES_PPGEC_2020_SOKOLOVICZ _BORIS_CASANOVA.pdf.jpgIM Thumbnailimage/jpeg4450http://repositorio.ufsm.br/bitstream/1/19866/5/TES_PPGEC_2020_SOKOLOVICZ%20_BORIS_CASANOVA.pdf.jpg1451edef4c7b6c1b4532b42a1bbb523aMD551/198662021-04-26 15:05:20.871oai:repositorio.ufsm.br:1/19866Q3JlYXRpdmUgQ29tbXVucw==Biblioteca Digital de Teses e Dissertaçõeshttps://repositorio.ufsm.br/ONGhttps://repositorio.ufsm.br/oai/requestatendimento.sib@ufsm.br||tedebc@gmail.comopendoar:2021-04-26T18:05:20Biblioteca Digital de Teses e Dissertações do UFSM - Universidade Federal de Santa Maria (UFSM)false
dc.title.por.fl_str_mv Avaliação das propriedades mecânicas e microestrutura de concreto de ultra alto desempenho com adições minerais e resíduos industriais
dc.title.alternative.eng.fl_str_mv Evaluation of mechanical properties and microstructure of ultra high performance concrete with mineral additions and industrial waste
title Avaliação das propriedades mecânicas e microestrutura de concreto de ultra alto desempenho com adições minerais e resíduos industriais
spellingShingle Avaliação das propriedades mecânicas e microestrutura de concreto de ultra alto desempenho com adições minerais e resíduos industriais
Sokolovicz, Bóris Casanova
Concreto de ultra alto desempenho
Propriedades mecânicas
Microestrutura
Sustentabilidade
Pozolanas
Empacotamento de partículas
Microstructure
Ultra high performance concrete
Mechanical properties
Sustainability
Pozzolans
Particles packing
CNPQ::ENGENHARIAS::ENGENHARIA CIVIL
title_short Avaliação das propriedades mecânicas e microestrutura de concreto de ultra alto desempenho com adições minerais e resíduos industriais
title_full Avaliação das propriedades mecânicas e microestrutura de concreto de ultra alto desempenho com adições minerais e resíduos industriais
title_fullStr Avaliação das propriedades mecânicas e microestrutura de concreto de ultra alto desempenho com adições minerais e resíduos industriais
title_full_unstemmed Avaliação das propriedades mecânicas e microestrutura de concreto de ultra alto desempenho com adições minerais e resíduos industriais
title_sort Avaliação das propriedades mecânicas e microestrutura de concreto de ultra alto desempenho com adições minerais e resíduos industriais
author Sokolovicz, Bóris Casanova
author_facet Sokolovicz, Bóris Casanova
author_role author
dc.contributor.advisor1.fl_str_mv Isaia, Geraldo Cechella
dc.contributor.advisor1Lattes.fl_str_mv http://lattes.cnpq.br/8260652949733370
dc.contributor.referee1.fl_str_mv Tutikian, Bernardo Fonseca
dc.contributor.referee1Lattes.fl_str_mv http://lattes.cnpq.br/9916860252080305
dc.contributor.referee2.fl_str_mv Hoppe Filho, Juarez
dc.contributor.referee2Lattes.fl_str_mv http://lattes.cnpq.br/8692521256968834
dc.contributor.referee3.fl_str_mv Vargas, Alexandre Silva de
dc.contributor.referee3Lattes.fl_str_mv http://lattes.cnpq.br/6501148372644975
dc.contributor.referee4.fl_str_mv Lübeck, André
dc.contributor.referee4Lattes.fl_str_mv http://lattes.cnpq.br/7511022637484145
dc.contributor.authorLattes.fl_str_mv http://lattes.cnpq.br/8038983210001144
dc.contributor.author.fl_str_mv Sokolovicz, Bóris Casanova
contributor_str_mv Isaia, Geraldo Cechella
Tutikian, Bernardo Fonseca
Hoppe Filho, Juarez
Vargas, Alexandre Silva de
Lübeck, André
dc.subject.por.fl_str_mv Concreto de ultra alto desempenho
Propriedades mecânicas
Microestrutura
Sustentabilidade
Pozolanas
Empacotamento de partículas
Microstructure
topic Concreto de ultra alto desempenho
Propriedades mecânicas
Microestrutura
Sustentabilidade
Pozolanas
Empacotamento de partículas
Microstructure
Ultra high performance concrete
Mechanical properties
Sustainability
Pozzolans
Particles packing
CNPQ::ENGENHARIAS::ENGENHARIA CIVIL
dc.subject.eng.fl_str_mv Ultra high performance concrete
Mechanical properties
Sustainability
Pozzolans
Particles packing
dc.subject.cnpq.fl_str_mv CNPQ::ENGENHARIAS::ENGENHARIA CIVIL
description With the increase in the world population, civil construction is the largest consumer of resources, with great environmental impact. One of the ways to reduce this impact is to increase the mechanical strength of the concrete, reducing the resistant sections of the structural parts, dematerializing them from the emanation of greenhouse gases. The use of industrial and pozzolan waste in concrete, in addition to the packaging of particles, are concrete actions that reduce environmental impacts, increasing sustainability. Thus, the general objective of this research was to analyze the microstructure and physical-mechanical properties of ultra high performance concrete (UHPC) with hydrated lime, foundry sand, pozzolanic and inert mineral additions, through the packaging effects of the particles. The specific objectives were: to evaluate the workability of UHPC with rice husk ash (RHA), fly ash (FA), lime CH I, limestone filler (LF), quartz powder and foundry sand, in relation to the reference concrete, with structural white cement, silica fume (SF), quartz powder and sand industrial; study the packaging of particles by the modified Andreassen method; analyze the performance of variables related to the mechanical strength of concrete in wet and thermal cures: axial compression, modulus of elasticity and instrumented breaks; and analyze the microstructure of UHPC mixtures by: X-Ray Diffraction (XRD), Thermogravimetric Analysis (TG/DTG), Fourier Transform Infrared (FTIR) and Scanning Electron Microscopy (SEM/EDS). The greatest resistance for all ages was the REF mixture. The efficiency of thermal curing was verified, mainly in early ages, with emphasis on the mixture with 15% partial replacement of cement with rice husk ash (RHA15). For mixtures with mineral additions, the similar behavior was noticeable. This performance confirms that the physical effect was representative, because, even with changes in levels and types of mineral additions, the average clinker intensity did not vary significantly. The elasticity modules showed the same trend of resistance behavior. In instrumented breaks, the stresses were proportional to the specific deformations in almost the entire test. In mixtures with mineral additions (RHA15, FA15, RHA10-FA5 and RHA10-LF5), the deformations were greater, attesting to the less fragile behavior. In XRD, the presence of non-hydrated compounds (alite and belite) was observed due to the low a / mc ratio. In mixtures with the addition of lime there was an increase in the peaks of portlandite and calcite, showing that a portion of the lime did not react with the pozzolana. In TG-DTG, mixtures with mineral additions had higher levels of combined water, calcium hydroxide (CH) and carbonates than REF, attesting that the lime partially reacted with the pozzolan. In FTIR, the REF mixture showed low peaks of portlandite, the opposite behavior of mixtures with mineral additions. In SEM, it was found that mixtures with mineral additions showed higher levels of Ca / Si ratio when compared to the reference concrete.
publishDate 2020
dc.date.accessioned.fl_str_mv 2020-05-15T16:18:15Z
dc.date.available.fl_str_mv 2020-05-15T16:18:15Z
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Centro de Tecnologia
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publisher.none.fl_str_mv Universidade Federal de Santa Maria
Centro de Tecnologia
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