Tailoring the composition of the AA2017 to reduce its hot cracking susceptibility during LPBF

Detalhes bibliográficos
Ano de defesa: 2024
Autor(a) principal: Rojas Arias, Nicolas
Orientador(a): Gargarella, Piter lattes
Banca de defesa: Não Informado pela instituição
Tipo de documento: Tese
Tipo de acesso: Acesso aberto
Idioma: eng
Instituição de defesa: Universidade Federal de São Carlos
Câmpus São Carlos
Programa de Pós-Graduação: Programa de Pós-Graduação em Ciência e Engenharia de Materiais - PPGCEM
Departamento: Não Informado pela instituição
País: Não Informado pela instituição
Palavras-chave em Português:
Palavras-chave em Inglês:
Área do conhecimento CNPq:
Link de acesso: https://repositorio.ufscar.br/handle/20.500.14289/20516
Resumo: Laser Powder Bed Fusion (LPBF) holds significant importance and research interest because of its capability to fabricate metallic components with intricate geometries that are challenging to replicate using traditional manufacturing methods. However, only a limited number of alloys are commercially viable for LPBF due to the processing conditions and characteristics of the alloys. This issue is particularly critical for alloys with wide solidification ranges such as wrought aluminum alloys, which may exhibit poor LPBF processability. For instance, previous experiments with the AA2017 alloy revealed its unsuitability for LPBF due to susceptibility to hot cracking. This study aimed to alter this alloy composition by incorporating additional elements that reduce the solidification range, facilitate grain refinement, and prevent crack formation during LPBF. The impact of different alloy element additions on the solidification range and phase formation was assessed via thermodynamic calculations. Compositions based on AA2017 were designed using the CALPHAD method and subsequently produced via gas atomization. The Design of Experiments methodology guided the selection of appropriate processing parameters to achieve crack-free parts with optimal structural integrity. Various characterization techniques were employed to examine the microstructural and mechanical properties. A new composition based on AA2017 was produced, enabling the construction of high-density, crack-free LPBF parts. X-ray diffraction analysis and microscopy techniques revealed that the improved processability of the new composition is attributed to its shorter solidification interval and a more fraction of liquid in the final stage of solidification with the presence of eutectic Al+Al3CeCu regions, which not only help to prevent crack formation but also enhanced the material's mechanical strength, as confirmed by the mechanical tests.
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spelling Rojas Arias, NicolasGargarella, Piterhttp://lattes.cnpq.br/4641435644243916Gil Coury, Franciscohttp://lattes.cnpq.br/8609825406277730http://lattes.cnpq.br/12504213956535492024-09-11T13:23:26Z2024-09-11T13:23:26Z2024-09-06ROJAS ARIAS, Nicolas. Tailoring the composition of the AA2017 to reduce its hot cracking susceptibility during LPBF. 2024. Tese (Doutorado em Ciência e Engenharia de Materiais) – Universidade Federal de São Carlos, São Carlos, 2024. Disponível em: https://repositorio.ufscar.br/handle/20.500.14289/20516.https://repositorio.ufscar.br/handle/20.500.14289/20516Laser Powder Bed Fusion (LPBF) holds significant importance and research interest because of its capability to fabricate metallic components with intricate geometries that are challenging to replicate using traditional manufacturing methods. However, only a limited number of alloys are commercially viable for LPBF due to the processing conditions and characteristics of the alloys. This issue is particularly critical for alloys with wide solidification ranges such as wrought aluminum alloys, which may exhibit poor LPBF processability. For instance, previous experiments with the AA2017 alloy revealed its unsuitability for LPBF due to susceptibility to hot cracking. This study aimed to alter this alloy composition by incorporating additional elements that reduce the solidification range, facilitate grain refinement, and prevent crack formation during LPBF. The impact of different alloy element additions on the solidification range and phase formation was assessed via thermodynamic calculations. Compositions based on AA2017 were designed using the CALPHAD method and subsequently produced via gas atomization. The Design of Experiments methodology guided the selection of appropriate processing parameters to achieve crack-free parts with optimal structural integrity. Various characterization techniques were employed to examine the microstructural and mechanical properties. A new composition based on AA2017 was produced, enabling the construction of high-density, crack-free LPBF parts. X-ray diffraction analysis and microscopy techniques revealed that the improved processability of the new composition is attributed to its shorter solidification interval and a more fraction of liquid in the final stage of solidification with the presence of eutectic Al+Al3CeCu regions, which not only help to prevent crack formation but also enhanced the material's mechanical strength, as confirmed by the mechanical tests.A Fusão a Laser em Leito de Pó (LPBF) tem uma importância significativa e desperta interesse de pesquisa devido à sua capacidade de fabricar componentes metálicos com geometrias complexas que são desafiadoras de replicar usando métodos de fabricação tradicionais. No entanto, apenas um número limitado de ligas é comercialmente viável para LPBF devido às condições de processamento e características das ligas. Esse problema é particularmente crítico para ligas com amplas faixas de solidificação, como as ligas de alumínio forjado, que podem apresentar uma baixa processabilidade no LPBF. Por exemplo, experimentos anteriores com a liga AA2017 revelaram sua inadequação para LPBF devido à susceptibilidade à fissuração a quente. Este estudo teve como objetivo alterar a composição desta liga incorporando elementos adicionais que reduzem a faixa de solidificação, facilitam o refinamento de grãos e previnem a formação de fissuras durante o LPBF. O impacto de diferentes adições de elementos de liga na faixa de solidificação e na formação de fases foi avaliado por meio de cálculos termodinâmicos. Composições baseadas em AA2017 foram projetadas usando o método CALPHAD e subsequentemente produzidas por atomização de gás. A metodologia de Design de Experimentos guiou a seleção de parâmetros de processamento adequados para alcançar peças livres de fissuras com integridade estrutural ótima. Várias técnicas de caracterização foram empregadas para examinar as propriedades microestruturais e mecânicas. Uma nova composição baseada em AA2017 foi produzida, possibilitando a construção de peças LPBF de alta densidade e livres de fissuras. Análises de difração de raios X e técnicas de microscopia revelaram que a melhor processabilidade da nova composição é atribuída ao seu intervalo de solidificação mais curto e fração de líquido maior na etapa final de solidificação com a presença de regiões eutéticas Al+Al3CeCu, que não apenas ajudam a prevenir a formação de fissuras, mas também melhoram a resistência mecânica do material, conforme confirmado pelos testes mecânicos.Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)2022/00896-3, Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)2020/01426-5, Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)engUniversidade Federal de São CarlosCâmpus São CarlosPrograma de Pós-Graduação em Ciência e Engenharia de Materiais - PPGCEMUFSCarAttribution-NonCommercial-NoDerivs 3.0 Brazilhttp://creativecommons.org/licenses/by-nc-nd/3.0/br/info:eu-repo/semantics/openAccessFusão a laser em leito de póAA2017Suscetibilidade ao trincamento a quenteRegiões eutéticasLaser powder bed fusionHot cracking susceptibilityAdditive manufacturingWrought aluminum alloysComposition designENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA::METALURGIA FISICATailoring the composition of the AA2017 to reduce its hot cracking susceptibility during LPBFAdaptação da composição do AA2017 para reduzir sua suscetibilidade a trincas a quente durante a LPBFinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/doctoralThesisreponame:Repositório Institucional da UFSCARinstname:Universidade Federal de São Carlos (UFSCAR)instacron:UFSCARTEXTNicolas Rojas Arias - Tese.pdf.txtNicolas Rojas Arias - Tese.pdf.txtExtracted texttext/plain100806https://repositorio.ufscar.br/bitstreams/6520e0d8-be54-4e65-8a45-3acdf5d3fe33/downloadf0ea477174993c0752d0844f73527d08MD53falseAnonymousREADTHUMBNAILNicolas Rojas Arias - Tese.pdf.jpgNicolas Rojas Arias - Tese.pdf.jpgGenerated Thumbnailimage/jpeg3708https://repositorio.ufscar.br/bitstreams/675707a4-8b03-4cc3-bbfd-42c7a079da77/download13ccec33b9a178ed0faccc6bb73446e9MD54falseAnonymousREADORIGINALNicolas Rojas Arias - Tese.pdfNicolas Rojas Arias - Tese.pdfTeseapplication/pdf12815720https://repositorio.ufscar.br/bitstreams/d184a573-c7f5-4da0-ace4-6001d658b506/downloade615bc19a9b0d29aa9f9788d8b5a7aeeMD51trueAnonymousREADCC-LICENSElicense_rdflicense_rdfapplication/rdf+xml; charset=utf-8810https://repositorio.ufscar.br/bitstreams/2c320feb-9627-4bf1-8ee4-1244bf9e4e55/downloadf337d95da1fce0a22c77480e5e9a7aecMD52falseAnonymousREAD20.500.14289/205162025-02-06 03:12:28.033http://creativecommons.org/licenses/by-nc-nd/3.0/br/Attribution-NonCommercial-NoDerivs 3.0 Brazilopen.accessoai:repositorio.ufscar.br:20.500.14289/20516https://repositorio.ufscar.brRepositório InstitucionalPUBhttps://repositorio.ufscar.br/oai/requestrepositorio.sibi@ufscar.bropendoar:43222025-02-06T06:12:28Repositório Institucional da UFSCAR - Universidade Federal de São Carlos (UFSCAR)false
dc.title.eng.fl_str_mv Tailoring the composition of the AA2017 to reduce its hot cracking susceptibility during LPBF
dc.title.alternative.por.fl_str_mv Adaptação da composição do AA2017 para reduzir sua suscetibilidade a trincas a quente durante a LPBF
title Tailoring the composition of the AA2017 to reduce its hot cracking susceptibility during LPBF
spellingShingle Tailoring the composition of the AA2017 to reduce its hot cracking susceptibility during LPBF
Rojas Arias, Nicolas
Fusão a laser em leito de pó
AA2017
Suscetibilidade ao trincamento a quente
Regiões eutéticas
Laser powder bed fusion
Hot cracking susceptibility
Additive manufacturing
Wrought aluminum alloys
Composition design
ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA::METALURGIA FISICA
title_short Tailoring the composition of the AA2017 to reduce its hot cracking susceptibility during LPBF
title_full Tailoring the composition of the AA2017 to reduce its hot cracking susceptibility during LPBF
title_fullStr Tailoring the composition of the AA2017 to reduce its hot cracking susceptibility during LPBF
title_full_unstemmed Tailoring the composition of the AA2017 to reduce its hot cracking susceptibility during LPBF
title_sort Tailoring the composition of the AA2017 to reduce its hot cracking susceptibility during LPBF
author Rojas Arias, Nicolas
author_facet Rojas Arias, Nicolas
author_role author
dc.contributor.authorlattes.por.fl_str_mv http://lattes.cnpq.br/1250421395653549
dc.contributor.author.fl_str_mv Rojas Arias, Nicolas
dc.contributor.advisor1.fl_str_mv Gargarella, Piter
dc.contributor.advisor1Lattes.fl_str_mv http://lattes.cnpq.br/4641435644243916
dc.contributor.advisor-co1.fl_str_mv Gil Coury, Francisco
dc.contributor.advisor-co1Lattes.fl_str_mv http://lattes.cnpq.br/8609825406277730
contributor_str_mv Gargarella, Piter
Gil Coury, Francisco
dc.subject.por.fl_str_mv Fusão a laser em leito de pó
AA2017
Suscetibilidade ao trincamento a quente
Regiões eutéticas
topic Fusão a laser em leito de pó
AA2017
Suscetibilidade ao trincamento a quente
Regiões eutéticas
Laser powder bed fusion
Hot cracking susceptibility
Additive manufacturing
Wrought aluminum alloys
Composition design
ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA::METALURGIA FISICA
dc.subject.eng.fl_str_mv Laser powder bed fusion
Hot cracking susceptibility
Additive manufacturing
Wrought aluminum alloys
Composition design
dc.subject.cnpq.fl_str_mv ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA::METALURGIA FISICA
description Laser Powder Bed Fusion (LPBF) holds significant importance and research interest because of its capability to fabricate metallic components with intricate geometries that are challenging to replicate using traditional manufacturing methods. However, only a limited number of alloys are commercially viable for LPBF due to the processing conditions and characteristics of the alloys. This issue is particularly critical for alloys with wide solidification ranges such as wrought aluminum alloys, which may exhibit poor LPBF processability. For instance, previous experiments with the AA2017 alloy revealed its unsuitability for LPBF due to susceptibility to hot cracking. This study aimed to alter this alloy composition by incorporating additional elements that reduce the solidification range, facilitate grain refinement, and prevent crack formation during LPBF. The impact of different alloy element additions on the solidification range and phase formation was assessed via thermodynamic calculations. Compositions based on AA2017 were designed using the CALPHAD method and subsequently produced via gas atomization. The Design of Experiments methodology guided the selection of appropriate processing parameters to achieve crack-free parts with optimal structural integrity. Various characterization techniques were employed to examine the microstructural and mechanical properties. A new composition based on AA2017 was produced, enabling the construction of high-density, crack-free LPBF parts. X-ray diffraction analysis and microscopy techniques revealed that the improved processability of the new composition is attributed to its shorter solidification interval and a more fraction of liquid in the final stage of solidification with the presence of eutectic Al+Al3CeCu regions, which not only help to prevent crack formation but also enhanced the material's mechanical strength, as confirmed by the mechanical tests.
publishDate 2024
dc.date.accessioned.fl_str_mv 2024-09-11T13:23:26Z
dc.date.available.fl_str_mv 2024-09-11T13:23:26Z
dc.date.issued.fl_str_mv 2024-09-06
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dc.identifier.citation.fl_str_mv ROJAS ARIAS, Nicolas. Tailoring the composition of the AA2017 to reduce its hot cracking susceptibility during LPBF. 2024. Tese (Doutorado em Ciência e Engenharia de Materiais) – Universidade Federal de São Carlos, São Carlos, 2024. Disponível em: https://repositorio.ufscar.br/handle/20.500.14289/20516.
dc.identifier.uri.fl_str_mv https://repositorio.ufscar.br/handle/20.500.14289/20516
identifier_str_mv ROJAS ARIAS, Nicolas. Tailoring the composition of the AA2017 to reduce its hot cracking susceptibility during LPBF. 2024. Tese (Doutorado em Ciência e Engenharia de Materiais) – Universidade Federal de São Carlos, São Carlos, 2024. Disponível em: https://repositorio.ufscar.br/handle/20.500.14289/20516.
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http://creativecommons.org/licenses/by-nc-nd/3.0/br/
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