Secagem de materiais pastosos e granulares no leito de jorro mecânico e convencional

Detalhes bibliográficos
Ano de defesa: 2017
Autor(a) principal: Sousa, Robson Costa de
Orientador(a): Freire, José Teixeira lattes
Banca de defesa: Não Informado pela instituição
Tipo de documento: Tese
Tipo de acesso: Acesso aberto
Idioma: por
Instituição de defesa: Universidade Federal de São Carlos
Câmpus São Carlos
Programa de Pós-Graduação: Programa de Pós-Graduação em Engenharia Química - PPGEQ
Departamento: Não Informado pela instituição
País: Não Informado pela instituição
Palavras-chave em Português:
Área do conhecimento CNPq:
Link de acesso: https://repositorio.ufscar.br/handle/ufscar/9487
Resumo: This study had the objective to assess the behavior of a mechanically spouted bed compared to a conventional spouted bed through attrition of particulate matter, thermal and mass analysis during water evaporation and through the drying of pastes and granular materials. Based on the obtained results, two mathematical models were applied to represent attrition, the CST model and the two-parameter diffusive model to describe the drying of the paste and grains, respectively. Therefore, a stainless steel spouted bed with cylindrical column of 0.95 m of height, 0.30 m of diameter, inferior and superior conical base (60° angle) with 0.30 m of diameter and 0.20 m of height. For the mechanically spouted bed dryer, a helical screw with the following measures was used: outside diameter of 0.01 m, length of 1 m, 0.70 m of spiral with diameter, and pitch of 0.0508 m. The attrition experiments were conducted with dolomite particles, and glass and alumina spheres. With the exception of the glass beads, there was attrition for the other particulate materials in both spouted beds; however, at larger proportions when the conventional set was used. It was also observed that attrition influenced the fluid dynamics of the conventional spouted bed. Of the models used, the one proposed by Gwyn (1969) provided acceptable predictions regarding the results observed in this study. For water evaporation, glass beads of 3.2 mm of diameter were used as inert particles. It was verified that operational variables (velocity, temperature and water flow) had direct influence on temperature and relative and absolute humidity of air at the outlet of the spouted bed. For the drying of pastes, skimmed milk and the glass beads employed in the water evaporation trials were used. The skimmed milk interfered in the circulation of inert particles, causing changes in the dimensionless pressure drop and air humidity at the outlet of the mechanically spouted bed dryer. Relative and absolute humidity as well as the moisture of the powder collected at the outlet of the cyclone were influenced by the operational variables. The results predicted by the CST model presented satisfactory agreement with the majority of results obtained in the skimmed milk drying experiments. When it comes to the drying of alumina spheres, the dimensionless data of grain moisture and of temperature and relative humidity of the fluid phase as a function of time were influenced by the operational conditions. The results predicted by the two-parameter mathematical model reached satisfactory accuracy regarding the observed data and allowed for a qualitative analysis of the drying operation. In general, all results obtained in this study showed behavior which is consistent with what has been observed in the literature.
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spelling Sousa, Robson Costa deFreire, José Teixeirahttp://lattes.cnpq.br/2270677706718167Freire, Fábio Benteshttp://lattes.cnpq.br/8937961078558996http://lattes.cnpq.br/73205860551420132018-02-26T19:50:47Z2018-02-26T19:50:47Z2017-06-02SOUSA, Robson Costa de. Secagem de materiais pastosos e granulares no leito de jorro mecânico e convencional. 2017. Tese (Doutorado em Engenharia Química) – Universidade Federal de São Carlos, São Carlos, 2017. Disponível em: https://repositorio.ufscar.br/handle/ufscar/9487.https://repositorio.ufscar.br/handle/ufscar/9487This study had the objective to assess the behavior of a mechanically spouted bed compared to a conventional spouted bed through attrition of particulate matter, thermal and mass analysis during water evaporation and through the drying of pastes and granular materials. Based on the obtained results, two mathematical models were applied to represent attrition, the CST model and the two-parameter diffusive model to describe the drying of the paste and grains, respectively. Therefore, a stainless steel spouted bed with cylindrical column of 0.95 m of height, 0.30 m of diameter, inferior and superior conical base (60° angle) with 0.30 m of diameter and 0.20 m of height. For the mechanically spouted bed dryer, a helical screw with the following measures was used: outside diameter of 0.01 m, length of 1 m, 0.70 m of spiral with diameter, and pitch of 0.0508 m. The attrition experiments were conducted with dolomite particles, and glass and alumina spheres. With the exception of the glass beads, there was attrition for the other particulate materials in both spouted beds; however, at larger proportions when the conventional set was used. It was also observed that attrition influenced the fluid dynamics of the conventional spouted bed. Of the models used, the one proposed by Gwyn (1969) provided acceptable predictions regarding the results observed in this study. For water evaporation, glass beads of 3.2 mm of diameter were used as inert particles. It was verified that operational variables (velocity, temperature and water flow) had direct influence on temperature and relative and absolute humidity of air at the outlet of the spouted bed. For the drying of pastes, skimmed milk and the glass beads employed in the water evaporation trials were used. The skimmed milk interfered in the circulation of inert particles, causing changes in the dimensionless pressure drop and air humidity at the outlet of the mechanically spouted bed dryer. Relative and absolute humidity as well as the moisture of the powder collected at the outlet of the cyclone were influenced by the operational variables. The results predicted by the CST model presented satisfactory agreement with the majority of results obtained in the skimmed milk drying experiments. When it comes to the drying of alumina spheres, the dimensionless data of grain moisture and of temperature and relative humidity of the fluid phase as a function of time were influenced by the operational conditions. The results predicted by the two-parameter mathematical model reached satisfactory accuracy regarding the observed data and allowed for a qualitative analysis of the drying operation. In general, all results obtained in this study showed behavior which is consistent with what has been observed in the literature.Este trabalho teve como objetivo verificar o comportamento do leito de jorro mecânico em relação ao leito de jorro convencional através da atrição de materiais particulados, da análise térmica e de massa durante a evaporação de água e da secagem de materiais pastosos e granulares. Com base nos dados obtidos, foram aplicados dois modelos matemáticos para representar a atrição, o modelo CST e o difusivo a dois parâmetros para descrever a secagem da pasta e dos grãos, respectivamente. Desta forma, foi utilizado um leito de jorro com coluna cilíndrica de aço inox de 0,87 m de altura, 0,30 m de diâmetro, base cônica inferior e superior (angulo de 60°) com diâmetro 0,30 m e altura de 0,20 m. Para o leito de jorro mecânico utilizou-se um parafuso helicoidal de dimensões: eixo de 0,01 m de diâmetro, 1,3 m de comprimento, 0,70 m de espiral com diâmetro e passe de 0,0508 m. Para a atrição, os experimentos foram conduzidos com partículas de dolomita, esferas de vidro e alumina. Com exceção das esferas de vidro, houve atrição para os demais materiais particulados em ambos os leitos de jorro, porém em maiores proporções quando utilizou-se a configuração convencional. Foi visto também que a atrição influenciou na fluidodinâmica do leito de jorro convencional. Dos modelos aplicados, o proposto por Gwyn (1969) forneceu previsões aceitáveis em relação aos resultados observados. Para a evaporação de água, utilizou-se esferas de vidro de 3,2 mm de diâmetro como inertes. Verificou-se que as variáveis operacionais (velocidade, temperatura e vazão de água) influenciaram diretamente na temperatura, umidades relativa e absoluta do ar na saída do leito de jorro. Para a secagem de pastas, utilizou-se o leite desnatado e esferas de vidro usadas nos experimentos de evaporação de água. O leite desnatado interferiu na circulação das partículas inertes, causando modificações no adimensional de queda de pressão e na umidade do ar na saída do leito de jorro mecânico. As umidades relativa e absoluta, bem como a umidade do pó recolhido na saída do ciclone foram influenciadas pelas variáveis operacionais. Os resultados preditos do modelo CST apresentaram concordância satisfatória com a grande maioria dos resultados obtidos nos experimentos de secagem do leite desnatado. Quanto à secagem das esferas de alumina, os dados do adimensional de umidade dos grãos, como também da temperatura e da umidade relativa da fase fluida em função do tempo foram influenciados pelas condições operacionais. Os resultados preditos pelo modelo matemático a dois parâmetros alcançaram precisão satisfatória com relação aos dados observados e permitiu uma análise qualitativa da operação de secagem. No geral, todos os resultados obtidos nesse trabalho apresentaram comportamentos que concordam com o que foi observado na literatura.Não recebi financiamentoporUniversidade Federal de São CarlosCâmpus São CarlosPrograma de Pós-Graduação em Engenharia Química - PPGEQUFSCarLeito de jorro mecânicoLeito de jorro convencionalSecagemENGENHARIAS::ENGENHARIA QUIMICASecagem de materiais pastosos e granulares no leito de jorro mecânico e convencionalinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/doctoralThesisOnlineinfo:eu-repo/semantics/openAccessreponame:Repositório Institucional da UFSCARinstname:Universidade Federal de São Carlos (UFSCAR)instacron:UFSCARORIGINALTeseRCS.pdfTeseRCS.pdfapplication/pdf3385950https://{{ getenv "DSPACE_HOST" "repositorio.ufscar.br" }}/bitstream/ufscar/9487/1/TeseRCS.pdfedf97ef71dc454069e6129f86e111ac7MD51LICENSElicense.txtlicense.txttext/plain; charset=utf-81957https://{{ getenv "DSPACE_HOST" "repositorio.ufscar.br" }}/bitstream/ufscar/9487/2/license.txtae0398b6f8b235e40ad82cba6c50031dMD52TEXTTeseRCS.pdf.txtTeseRCS.pdf.txtExtracted texttext/plain288521https://{{ getenv "DSPACE_HOST" "repositorio.ufscar.br" }}/bitstream/ufscar/9487/3/TeseRCS.pdf.txt2741b1ce5b364852b40c5e895a97a06eMD53THUMBNAILTeseRCS.pdf.jpgTeseRCS.pdf.jpgIM Thumbnailimage/jpeg5751https://{{ getenv "DSPACE_HOST" "repositorio.ufscar.br" }}/bitstream/ufscar/9487/4/TeseRCS.pdf.jpg4eb0e32a71e6a46f354e79b38b177212MD54ufscar/94872019-09-11 03:03:35.319oai:repositorio.ufscar.br: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Repositório InstitucionalPUBhttps://repositorio.ufscar.br/oai/requestopendoar:43222023-05-25T12:55:27.485082Repositório Institucional da UFSCAR - Universidade Federal de São Carlos (UFSCAR)false
dc.title.por.fl_str_mv Secagem de materiais pastosos e granulares no leito de jorro mecânico e convencional
title Secagem de materiais pastosos e granulares no leito de jorro mecânico e convencional
spellingShingle Secagem de materiais pastosos e granulares no leito de jorro mecânico e convencional
Sousa, Robson Costa de
Leito de jorro mecânico
Leito de jorro convencional
Secagem
ENGENHARIAS::ENGENHARIA QUIMICA
title_short Secagem de materiais pastosos e granulares no leito de jorro mecânico e convencional
title_full Secagem de materiais pastosos e granulares no leito de jorro mecânico e convencional
title_fullStr Secagem de materiais pastosos e granulares no leito de jorro mecânico e convencional
title_full_unstemmed Secagem de materiais pastosos e granulares no leito de jorro mecânico e convencional
title_sort Secagem de materiais pastosos e granulares no leito de jorro mecânico e convencional
author Sousa, Robson Costa de
author_facet Sousa, Robson Costa de
author_role author
dc.contributor.authorlattes.por.fl_str_mv http://lattes.cnpq.br/7320586055142013
dc.contributor.author.fl_str_mv Sousa, Robson Costa de
dc.contributor.advisor1.fl_str_mv Freire, José Teixeira
dc.contributor.advisor1Lattes.fl_str_mv http://lattes.cnpq.br/2270677706718167
dc.contributor.advisor-co1.fl_str_mv Freire, Fábio Bentes
dc.contributor.advisor-co1Lattes.fl_str_mv http://lattes.cnpq.br/8937961078558996
contributor_str_mv Freire, José Teixeira
Freire, Fábio Bentes
dc.subject.por.fl_str_mv Leito de jorro mecânico
Leito de jorro convencional
Secagem
topic Leito de jorro mecânico
Leito de jorro convencional
Secagem
ENGENHARIAS::ENGENHARIA QUIMICA
dc.subject.cnpq.fl_str_mv ENGENHARIAS::ENGENHARIA QUIMICA
description This study had the objective to assess the behavior of a mechanically spouted bed compared to a conventional spouted bed through attrition of particulate matter, thermal and mass analysis during water evaporation and through the drying of pastes and granular materials. Based on the obtained results, two mathematical models were applied to represent attrition, the CST model and the two-parameter diffusive model to describe the drying of the paste and grains, respectively. Therefore, a stainless steel spouted bed with cylindrical column of 0.95 m of height, 0.30 m of diameter, inferior and superior conical base (60° angle) with 0.30 m of diameter and 0.20 m of height. For the mechanically spouted bed dryer, a helical screw with the following measures was used: outside diameter of 0.01 m, length of 1 m, 0.70 m of spiral with diameter, and pitch of 0.0508 m. The attrition experiments were conducted with dolomite particles, and glass and alumina spheres. With the exception of the glass beads, there was attrition for the other particulate materials in both spouted beds; however, at larger proportions when the conventional set was used. It was also observed that attrition influenced the fluid dynamics of the conventional spouted bed. Of the models used, the one proposed by Gwyn (1969) provided acceptable predictions regarding the results observed in this study. For water evaporation, glass beads of 3.2 mm of diameter were used as inert particles. It was verified that operational variables (velocity, temperature and water flow) had direct influence on temperature and relative and absolute humidity of air at the outlet of the spouted bed. For the drying of pastes, skimmed milk and the glass beads employed in the water evaporation trials were used. The skimmed milk interfered in the circulation of inert particles, causing changes in the dimensionless pressure drop and air humidity at the outlet of the mechanically spouted bed dryer. Relative and absolute humidity as well as the moisture of the powder collected at the outlet of the cyclone were influenced by the operational variables. The results predicted by the CST model presented satisfactory agreement with the majority of results obtained in the skimmed milk drying experiments. When it comes to the drying of alumina spheres, the dimensionless data of grain moisture and of temperature and relative humidity of the fluid phase as a function of time were influenced by the operational conditions. The results predicted by the two-parameter mathematical model reached satisfactory accuracy regarding the observed data and allowed for a qualitative analysis of the drying operation. In general, all results obtained in this study showed behavior which is consistent with what has been observed in the literature.
publishDate 2017
dc.date.issued.fl_str_mv 2017-06-02
dc.date.accessioned.fl_str_mv 2018-02-26T19:50:47Z
dc.date.available.fl_str_mv 2018-02-26T19:50:47Z
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dc.identifier.citation.fl_str_mv SOUSA, Robson Costa de. Secagem de materiais pastosos e granulares no leito de jorro mecânico e convencional. 2017. Tese (Doutorado em Engenharia Química) – Universidade Federal de São Carlos, São Carlos, 2017. Disponível em: https://repositorio.ufscar.br/handle/ufscar/9487.
dc.identifier.uri.fl_str_mv https://repositorio.ufscar.br/handle/ufscar/9487
identifier_str_mv SOUSA, Robson Costa de. Secagem de materiais pastosos e granulares no leito de jorro mecânico e convencional. 2017. Tese (Doutorado em Engenharia Química) – Universidade Federal de São Carlos, São Carlos, 2017. Disponível em: https://repositorio.ufscar.br/handle/ufscar/9487.
url https://repositorio.ufscar.br/handle/ufscar/9487
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dc.publisher.none.fl_str_mv Universidade Federal de São Carlos
Câmpus São Carlos
dc.publisher.program.fl_str_mv Programa de Pós-Graduação em Engenharia Química - PPGEQ
dc.publisher.initials.fl_str_mv UFSCar
publisher.none.fl_str_mv Universidade Federal de São Carlos
Câmpus São Carlos
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