Caracterização microestrutural e mecânica da liga AA2024 conformada por spray e processada termomecanicamente

Detalhes bibliográficos
Ano de defesa: 2019
Autor(a) principal: Asato, Gabriel Hitoshi
Orientador(a): Jorge Júnior, Alberto Moreira lattes
Banca de defesa: Não Informado pela instituição
Tipo de documento: Tese
Tipo de acesso: Acesso aberto
Idioma: por
Instituição de defesa: Universidade Federal de São Carlos
Câmpus São Carlos
Programa de Pós-Graduação: Programa de Pós-Graduação em Ciência e Engenharia de Materiais - PPGCEM
Departamento: Não Informado pela instituição
País: Não Informado pela instituição
Palavras-chave em Português:
Palavras-chave em Inglês:
Área do conhecimento CNPq:
Link de acesso: https://repositorio.ufscar.br/handle/20.500.14289/11247
Resumo: This work aimed to evaluate the possibility of combining spray forming processing with mechanical processing techniques (for instance, extrusion, rotary forging, and equal-channel angular pressing (ECAP)) to be used as processing routes for reuse of aluminum alloys. In the specific case of the AA2024 alloy, in applications nobler than the intended for production of casting alloys. For such an aiming, the final alloy must have a refined microstructure, solubilized alloying elements, be entirely homogeneous, absent of porosity that can affect mechanical properties, and chemical composition similar to the as received alloy. Our results have shown that, after spray forming, the microstructure presented equiaxed grains with an average size of 50 μm, alloying elements more solubilized than the as received alloy and a significant fraction of porosity. Chemical analysis of the deposit showed chemical composition with a small variation in composition, but still inside the allowed values imposed by the ASTM standard. The deposit was machined into cylindrical samples to be processed by extrusion and rotary forging and square-like samples to be processed by ECAP. The combination of rotary forging and ECAP were also performed. After processing, microstructural characterizations were accomplished to verify porosity closing and microstructure refinement. Mechanical compression tests were conducted to evaluate the mechanical strength of the processed alloys compared to the as received one. Results obtained from mechanical tests for the alloys processed by extrusion and rotary forging presented higher values than for the initial alloy. However, ECAP presented a decrease in mechanical resistance. Concerning the microstructure, the grains remained elongated, characteristic of mechanically processed alloys without recrystallization, secondary phases were sufficiently solubilized, no coring effect was observed in grains, and the porosity was significantly reduced.
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spelling Asato, Gabriel HitoshiJorge Júnior, Alberto Moreirahttp://lattes.cnpq.br/6360362248108490Bolfarini, Claudemirohttp://lattes.cnpq.br/9231627080617037http://lattes.cnpq.br/0739042399340119fcba0843-8c9b-40ec-bf9a-46a95f2a59cb2019-04-17T13:31:04Z2019-04-17T13:31:04Z2019-03-22ASATO, Gabriel Hitoshi. Caracterização microestrutural e mecânica da liga AA2024 conformada por spray e processada termomecanicamente. 2019. Tese (Doutorado em Ciência e Engenharia de Materiais) – Universidade Federal de São Carlos, São Carlos, 2019. Disponível em: https://repositorio.ufscar.br/handle/20.500.14289/11247.https://repositorio.ufscar.br/handle/20.500.14289/11247This work aimed to evaluate the possibility of combining spray forming processing with mechanical processing techniques (for instance, extrusion, rotary forging, and equal-channel angular pressing (ECAP)) to be used as processing routes for reuse of aluminum alloys. In the specific case of the AA2024 alloy, in applications nobler than the intended for production of casting alloys. For such an aiming, the final alloy must have a refined microstructure, solubilized alloying elements, be entirely homogeneous, absent of porosity that can affect mechanical properties, and chemical composition similar to the as received alloy. Our results have shown that, after spray forming, the microstructure presented equiaxed grains with an average size of 50 μm, alloying elements more solubilized than the as received alloy and a significant fraction of porosity. Chemical analysis of the deposit showed chemical composition with a small variation in composition, but still inside the allowed values imposed by the ASTM standard. The deposit was machined into cylindrical samples to be processed by extrusion and rotary forging and square-like samples to be processed by ECAP. The combination of rotary forging and ECAP were also performed. After processing, microstructural characterizations were accomplished to verify porosity closing and microstructure refinement. Mechanical compression tests were conducted to evaluate the mechanical strength of the processed alloys compared to the as received one. Results obtained from mechanical tests for the alloys processed by extrusion and rotary forging presented higher values than for the initial alloy. However, ECAP presented a decrease in mechanical resistance. Concerning the microstructure, the grains remained elongated, characteristic of mechanically processed alloys without recrystallization, secondary phases were sufficiently solubilized, no coring effect was observed in grains, and the porosity was significantly reduced.Este trabalho teve como objetivo avaliar a possibilidade de combinar o processamento por conformação por spray com técnicas de processamentomecânico (por exemplo, extrusão, forjamento rotatório e extrusão por canalangular (ECA)) para serem utilizadas como rotas de processamento para reutilização de ligas de alumínio. No caso específico da liga AA2024, em aplicações mais nobres do que as destinadas à produção de ligas de fundição. Para atingir o objetivo, a liga final deve ter uma microestrutura refinada, fases secundárias solubilizadas, ser totalmente homogênea, sem porosidade e composição química similar à liga como recebida. Nossos resultados mostraram que, após a conformação por spray, a microestrutura apresentou grãos equiaxiais com tamanho médio de 50 μm, elementos de liga mais solubilizados que a liga como recebida e uma fração significativa de porosidade. A análise química do depósito mostrou composição química com pequena variação na composição, mas ainda dentro dos valores permitidos pelo padrão ASTM. O depósito foi usinado em amostras cilíndricas para serem processadas por extrusão e forjamento rotativo e amostras quadradas para serem processadas pelo ECAP. A combinação de forjamento rotativo e ECAP também foi realizada. Após o processamento, caracterizações microestruturais foram realizadas para verificar o fechamento da porosidade e o refinamento da microestrutura. Testes mecânicos de compressão foram realizados para avaliar a resistência mecânica das ligas processadas em relação à como recebida. Os resultados obtidos nos ensaios mecânicos das ligas processadas por extrusão e forjamento rotativo apresentaram valores superiores aos da liga inicial. No entanto, o ECAP apresentou uma diminuição na resistência mecânica. Em relação à microestrutura, os grãos permaneceram alongados, característicos das ligas processadas mecanicamente a frio sem recristalização, as fases secundárias foram suficientemente solubilizadas, não foi observado efeito de microssegregação (coring) nos grãos e a porosidade foi significativamente reduzida.Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)CAPES: Código de Financiamento 001porUniversidade Federal de São CarlosCâmpus São CarlosPrograma de Pós-Graduação em Ciência e Engenharia de Materiais - PPGCEMUFSCarConformação por sprayAA2024ExtrusãoForjamento rotativoECAPSpray formingExtrusionRotary forgingENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA::METALURGIA FISICAENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICAENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA::METALURGIA FISICA::PROPRIEDADES MECANICAS DOS METAIS E LIGASCaracterização microestrutural e mecânica da liga AA2024 conformada por spray e processada termomecanicamenteMicrostructural and mechanical characterization of the spray formed AA2024 alloy thermomechanically processedinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/doctoralThesisOnline6002b508166-b635-4fb0-a91b-419736667f7finfo:eu-repo/semantics/openAccessreponame:Repositório Institucional da UFSCARinstname:Universidade Federal de São Carlos (UFSCAR)instacron:UFSCARORIGINALGabriel Hitoshi Asato - Tese.pdfGabriel Hitoshi Asato - Tese.pdfTese versão finalapplication/pdf10530159https://repositorio.ufscar.br/bitstreams/13060bb1-eee3-4397-840b-94a9013da182/download81d4b037bfc93e5d2164842a06e1d816MD51trueAnonymousREADLICENSElicense.txtlicense.txttext/plain; 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dc.title.por.fl_str_mv Caracterização microestrutural e mecânica da liga AA2024 conformada por spray e processada termomecanicamente
dc.title.alternative.eng.fl_str_mv Microstructural and mechanical characterization of the spray formed AA2024 alloy thermomechanically processed
title Caracterização microestrutural e mecânica da liga AA2024 conformada por spray e processada termomecanicamente
spellingShingle Caracterização microestrutural e mecânica da liga AA2024 conformada por spray e processada termomecanicamente
Asato, Gabriel Hitoshi
Conformação por spray
AA2024
Extrusão
Forjamento rotativo
ECAP
Spray forming
Extrusion
Rotary forging
ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA::METALURGIA FISICA
ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA
ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA::METALURGIA FISICA::PROPRIEDADES MECANICAS DOS METAIS E LIGAS
title_short Caracterização microestrutural e mecânica da liga AA2024 conformada por spray e processada termomecanicamente
title_full Caracterização microestrutural e mecânica da liga AA2024 conformada por spray e processada termomecanicamente
title_fullStr Caracterização microestrutural e mecânica da liga AA2024 conformada por spray e processada termomecanicamente
title_full_unstemmed Caracterização microestrutural e mecânica da liga AA2024 conformada por spray e processada termomecanicamente
title_sort Caracterização microestrutural e mecânica da liga AA2024 conformada por spray e processada termomecanicamente
author Asato, Gabriel Hitoshi
author_facet Asato, Gabriel Hitoshi
author_role author
dc.contributor.authorlattes.por.fl_str_mv http://lattes.cnpq.br/0739042399340119
dc.contributor.author.fl_str_mv Asato, Gabriel Hitoshi
dc.contributor.advisor1.fl_str_mv Jorge Júnior, Alberto Moreira
dc.contributor.advisor1Lattes.fl_str_mv http://lattes.cnpq.br/6360362248108490
dc.contributor.advisor-co1.fl_str_mv Bolfarini, Claudemiro
dc.contributor.advisor-co1Lattes.fl_str_mv http://lattes.cnpq.br/9231627080617037
dc.contributor.authorID.fl_str_mv fcba0843-8c9b-40ec-bf9a-46a95f2a59cb
contributor_str_mv Jorge Júnior, Alberto Moreira
Bolfarini, Claudemiro
dc.subject.por.fl_str_mv Conformação por spray
AA2024
Extrusão
Forjamento rotativo
ECAP
topic Conformação por spray
AA2024
Extrusão
Forjamento rotativo
ECAP
Spray forming
Extrusion
Rotary forging
ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA::METALURGIA FISICA
ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA
ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA::METALURGIA FISICA::PROPRIEDADES MECANICAS DOS METAIS E LIGAS
dc.subject.eng.fl_str_mv Spray forming
Extrusion
Rotary forging
dc.subject.cnpq.fl_str_mv ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA::METALURGIA FISICA
ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA
ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA::METALURGIA FISICA::PROPRIEDADES MECANICAS DOS METAIS E LIGAS
description This work aimed to evaluate the possibility of combining spray forming processing with mechanical processing techniques (for instance, extrusion, rotary forging, and equal-channel angular pressing (ECAP)) to be used as processing routes for reuse of aluminum alloys. In the specific case of the AA2024 alloy, in applications nobler than the intended for production of casting alloys. For such an aiming, the final alloy must have a refined microstructure, solubilized alloying elements, be entirely homogeneous, absent of porosity that can affect mechanical properties, and chemical composition similar to the as received alloy. Our results have shown that, after spray forming, the microstructure presented equiaxed grains with an average size of 50 μm, alloying elements more solubilized than the as received alloy and a significant fraction of porosity. Chemical analysis of the deposit showed chemical composition with a small variation in composition, but still inside the allowed values imposed by the ASTM standard. The deposit was machined into cylindrical samples to be processed by extrusion and rotary forging and square-like samples to be processed by ECAP. The combination of rotary forging and ECAP were also performed. After processing, microstructural characterizations were accomplished to verify porosity closing and microstructure refinement. Mechanical compression tests were conducted to evaluate the mechanical strength of the processed alloys compared to the as received one. Results obtained from mechanical tests for the alloys processed by extrusion and rotary forging presented higher values than for the initial alloy. However, ECAP presented a decrease in mechanical resistance. Concerning the microstructure, the grains remained elongated, characteristic of mechanically processed alloys without recrystallization, secondary phases were sufficiently solubilized, no coring effect was observed in grains, and the porosity was significantly reduced.
publishDate 2019
dc.date.accessioned.fl_str_mv 2019-04-17T13:31:04Z
dc.date.available.fl_str_mv 2019-04-17T13:31:04Z
dc.date.issued.fl_str_mv 2019-03-22
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/doctoralThesis
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status_str publishedVersion
dc.identifier.citation.fl_str_mv ASATO, Gabriel Hitoshi. Caracterização microestrutural e mecânica da liga AA2024 conformada por spray e processada termomecanicamente. 2019. Tese (Doutorado em Ciência e Engenharia de Materiais) – Universidade Federal de São Carlos, São Carlos, 2019. Disponível em: https://repositorio.ufscar.br/handle/20.500.14289/11247.
dc.identifier.uri.fl_str_mv https://repositorio.ufscar.br/handle/20.500.14289/11247
identifier_str_mv ASATO, Gabriel Hitoshi. Caracterização microestrutural e mecânica da liga AA2024 conformada por spray e processada termomecanicamente. 2019. Tese (Doutorado em Ciência e Engenharia de Materiais) – Universidade Federal de São Carlos, São Carlos, 2019. Disponível em: https://repositorio.ufscar.br/handle/20.500.14289/11247.
url https://repositorio.ufscar.br/handle/20.500.14289/11247
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dc.publisher.none.fl_str_mv Universidade Federal de São Carlos
Câmpus São Carlos
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dc.publisher.initials.fl_str_mv UFSCar
publisher.none.fl_str_mv Universidade Federal de São Carlos
Câmpus São Carlos
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