Comportamento mecânico da liga Ti-6Al-4V com superfície modificada por laser de femtosegundo para uso biomédico

Detalhes bibliográficos
Ano de defesa: 2012
Autor(a) principal: Santos, Alan dos
Orientador(a): Bolfarini, Claudemiro lattes
Banca de defesa: Não Informado pela instituição
Tipo de documento: Dissertação
Tipo de acesso: Acesso aberto
Idioma: por
Instituição de defesa: Universidade Federal de São Carlos
Câmpus São Carlos
Programa de Pós-Graduação: Programa de Pós-Graduação em Ciência e Engenharia de Materiais - PPGCEM
Departamento: Não Informado pela instituição
País: Não Informado pela instituição
Palavras-chave em Português:
Palavras-chave em Inglês:
Área do conhecimento CNPq:
Link de acesso: https://repositorio.ufscar.br/handle/20.500.14289/7106
Resumo: Stainless steel orthopedic implants are still the most widely used in Brazil due to their lower cost. There is, however, a tendency to expand the use of special alloys such as titanium-based, due to clinical advantages that they present, notably the low modulus of elasticity and the best biocompatibility among the metallic biomaterials. The surface treatments aim to develop substrates suitable for bone growth, thus preventing the implantation of the prosthesis with PMMA cement, which results in an efficient mechanical fixing, but there is no biological interaction between implant and bone. There are several surface modification techniques, all of them improving at some level the process of osseointegration. However, researches have focused on biological aspects of the process and, despite the durability of the implant, there is currently no objective information in the literature about the influence of surface treatments on the mechanical behavior under cyclic stresses. The laser surface modification emerges as a promising alternative, since it permits precise control of parameters, regular surface development, induces reduced mechanical and thermal damage, and is known to promote osseointegration. The femtosecond laser, in particular, allows pulses of short duration (10-15s), reducing even more the damage caused by heat input. This study evaluated the influence of surface modification by femtosecond LASER in the fatigue resistance of Ti-6Al-4V alloy samples. S-N curves were determined for the reference samples and for the samples with modified surface. The topography developed and the fracture surfaces were analyzed by scanning electron microscopy. The femtosecond LASER has developed a regular surface with a bimodal distribution of microcolumns and ripples, and did not cause severe damage adjacent to the modified surface, however, has significantly reduced fatigue resistance.
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spelling Santos, Alan dosBolfarini, Claudemirohttp://lattes.cnpq.br/9231627080617037http://lattes.cnpq.br/6009157017178581cf14889f-2fd5-47cb-9949-07eac1b1a5ed2016-09-13T18:03:48Z2016-09-13T18:03:48Z2012-02-10SANTOS, Alan dos. Comportamento mecânico da liga Ti-6Al-4V com superfície modificada por laser de femtosegundo para uso biomédico. 2012. Dissertação (Mestrado em Ciência e Engenharia de Materiais) – Universidade Federal de São Carlos, São Carlos, 2012. Disponível em: https://repositorio.ufscar.br/handle/20.500.14289/7106.https://repositorio.ufscar.br/handle/20.500.14289/7106Stainless steel orthopedic implants are still the most widely used in Brazil due to their lower cost. There is, however, a tendency to expand the use of special alloys such as titanium-based, due to clinical advantages that they present, notably the low modulus of elasticity and the best biocompatibility among the metallic biomaterials. The surface treatments aim to develop substrates suitable for bone growth, thus preventing the implantation of the prosthesis with PMMA cement, which results in an efficient mechanical fixing, but there is no biological interaction between implant and bone. There are several surface modification techniques, all of them improving at some level the process of osseointegration. However, researches have focused on biological aspects of the process and, despite the durability of the implant, there is currently no objective information in the literature about the influence of surface treatments on the mechanical behavior under cyclic stresses. The laser surface modification emerges as a promising alternative, since it permits precise control of parameters, regular surface development, induces reduced mechanical and thermal damage, and is known to promote osseointegration. The femtosecond laser, in particular, allows pulses of short duration (10-15s), reducing even more the damage caused by heat input. This study evaluated the influence of surface modification by femtosecond LASER in the fatigue resistance of Ti-6Al-4V alloy samples. S-N curves were determined for the reference samples and for the samples with modified surface. The topography developed and the fracture surfaces were analyzed by scanning electron microscopy. The femtosecond LASER has developed a regular surface with a bimodal distribution of microcolumns and ripples, and did not cause severe damage adjacent to the modified surface, however, has significantly reduced fatigue resistance.Os implantes ortopédicos de aço inoxidável ainda são – em razão do menor custo - os mais utilizados no Brasil, mas há uma tendência em se ampliar a utilização de ligas especiais, como as de titânio, devido às vantagens clínicas que apresentam, destacando-se o baixo módulo de elasticidade e a melhor biocompatibilidade dentre os biomateriais metálicos. Os tratamentos de superfície buscam desenvolver substratos adequados ao crescimento ósseo, evitando assim a implantação da prótese por cementação com PMMA, que resulta em uma eficiente fixação mecânica, porém não há interação biológica entre o implante e o osso. Existem diversas técnicas de modificação superficial, todas elas melhorando em algum nível o processo de osseointegração. Entretanto, as pesquisas têm se concentrado nos aspectos biológicos do processo e, a despeito da durabilidade do implante, não há atualmente na literatura informações objetivas sobre a influência destes tratamentos de superfície no comportamento mecânico sob esforços cíclicos. A modificação superficial por LASER surge como uma alternativa promissora, pois permite um controle preciso de parâmetros, oferece regularidade, induz reduzidos danos mecânicos e térmicos e conhecidamente promove a osseointegração. O LASER de femtosegundo, em especial, permite pulsos de curtíssima duração (10-15s), reduzindo ainda mais os danos decorrentes do aporte térmico. Este trabalho avaliou a influência da modificação superficial por LASER de femtosegundo na resistência à fadiga de corpos de prova da liga Ti-6Al-4V. Foram levantadas as curvas S-N para amostras de referência e com a superfície modificada. A topografia formada e as superfícies de fratura foram analisadas por microscopia eletrônica de varredura. O laser de femtosegundo desenvolveu uma superfície regular bimodal de microcolunas e ripples, não causou danos metalúrgicos severos nas adjacências da superfície, porém, reduziu significativamente a resistência à fadiga.Não recebi financiamentoporUniversidade Federal de São CarlosCâmpus São CarlosPrograma de Pós-Graduação em Ciência e Engenharia de Materiais - PPGCEMUFSCarAço inoxidávelLigas de titânioBiomateriaisPróteseLaserStainless steelTitanium alloysBiomaterialsProsthesisLaserENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICAComportamento mecânico da liga Ti-6Al-4V com superfície modificada por laser de femtosegundo para uso biomédicoMechanical behavior of ti-6al-4v titanium alloy with surface modified by femtosecond laser for biomedical useinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/masterThesisOnline600600ea2697dd-8d22-4c7a-8bdd-487c739e04c7info:eu-repo/semantics/openAccessreponame:Repositório Institucional da UFSCARinstname:Universidade Federal de São Carlos (UFSCAR)instacron:UFSCARLICENSElicense.txtlicense.txttext/plain; charset=utf-81957https://repositorio.ufscar.br/bitstreams/3d09b69c-9fb7-435e-9a69-35db1646f9ae/downloadae0398b6f8b235e40ad82cba6c50031dMD52falseAnonymousREADORIGINALDissAS.pdfDissAS.pdfapplication/pdf3683315https://repositorio.ufscar.br/bitstreams/06f91b98-8146-440b-b058-b4f4388439d8/download5ae06ee0ca42268d4a03bfff70047e6cMD51trueAnonymousREADTEXTDissAS.pdf.txtDissAS.pdf.txtExtracted texttext/plain125591https://repositorio.ufscar.br/bitstreams/7d192cd1-b5b2-486d-91fc-34ee4ffc0600/download84f3b6a374b2489498a14d535b5106d6MD55falseAnonymousREADTHUMBNAILDissAS.pdf.jpgDissAS.pdf.jpgIM Thumbnailimage/jpeg3790https://repositorio.ufscar.br/bitstreams/40e918e5-8261-48ed-86ab-210815b9f1a1/download41aebb6a6bef8783d0e4c53a4cd90e9bMD56falseAnonymousREAD20.500.14289/71062025-02-05 17:09:00.206Acesso abertoopen.accessoai:repositorio.ufscar.br:20.500.14289/7106https://repositorio.ufscar.brRepositório InstitucionalPUBhttps://repositorio.ufscar.br/oai/requestrepositorio.sibi@ufscar.bropendoar:43222025-02-05T20:09Repositório Institucional da UFSCAR - Universidade Federal de São Carlos (UFSCAR)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
dc.title.por.fl_str_mv Comportamento mecânico da liga Ti-6Al-4V com superfície modificada por laser de femtosegundo para uso biomédico
dc.title.alternative.eng.fl_str_mv Mechanical behavior of ti-6al-4v titanium alloy with surface modified by femtosecond laser for biomedical use
title Comportamento mecânico da liga Ti-6Al-4V com superfície modificada por laser de femtosegundo para uso biomédico
spellingShingle Comportamento mecânico da liga Ti-6Al-4V com superfície modificada por laser de femtosegundo para uso biomédico
Santos, Alan dos
Aço inoxidável
Ligas de titânio
Biomateriais
Prótese
Laser
Stainless steel
Titanium alloys
Biomaterials
Prosthesis
Laser
ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA
title_short Comportamento mecânico da liga Ti-6Al-4V com superfície modificada por laser de femtosegundo para uso biomédico
title_full Comportamento mecânico da liga Ti-6Al-4V com superfície modificada por laser de femtosegundo para uso biomédico
title_fullStr Comportamento mecânico da liga Ti-6Al-4V com superfície modificada por laser de femtosegundo para uso biomédico
title_full_unstemmed Comportamento mecânico da liga Ti-6Al-4V com superfície modificada por laser de femtosegundo para uso biomédico
title_sort Comportamento mecânico da liga Ti-6Al-4V com superfície modificada por laser de femtosegundo para uso biomédico
author Santos, Alan dos
author_facet Santos, Alan dos
author_role author
dc.contributor.authorlattes.por.fl_str_mv http://lattes.cnpq.br/6009157017178581
dc.contributor.author.fl_str_mv Santos, Alan dos
dc.contributor.advisor1.fl_str_mv Bolfarini, Claudemiro
dc.contributor.advisor1Lattes.fl_str_mv http://lattes.cnpq.br/9231627080617037
dc.contributor.authorID.fl_str_mv cf14889f-2fd5-47cb-9949-07eac1b1a5ed
contributor_str_mv Bolfarini, Claudemiro
dc.subject.por.fl_str_mv Aço inoxidável
Ligas de titânio
Biomateriais
Prótese
Laser
topic Aço inoxidável
Ligas de titânio
Biomateriais
Prótese
Laser
Stainless steel
Titanium alloys
Biomaterials
Prosthesis
Laser
ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA
dc.subject.eng.fl_str_mv Stainless steel
Titanium alloys
Biomaterials
Prosthesis
Laser
dc.subject.cnpq.fl_str_mv ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA
description Stainless steel orthopedic implants are still the most widely used in Brazil due to their lower cost. There is, however, a tendency to expand the use of special alloys such as titanium-based, due to clinical advantages that they present, notably the low modulus of elasticity and the best biocompatibility among the metallic biomaterials. The surface treatments aim to develop substrates suitable for bone growth, thus preventing the implantation of the prosthesis with PMMA cement, which results in an efficient mechanical fixing, but there is no biological interaction between implant and bone. There are several surface modification techniques, all of them improving at some level the process of osseointegration. However, researches have focused on biological aspects of the process and, despite the durability of the implant, there is currently no objective information in the literature about the influence of surface treatments on the mechanical behavior under cyclic stresses. The laser surface modification emerges as a promising alternative, since it permits precise control of parameters, regular surface development, induces reduced mechanical and thermal damage, and is known to promote osseointegration. The femtosecond laser, in particular, allows pulses of short duration (10-15s), reducing even more the damage caused by heat input. This study evaluated the influence of surface modification by femtosecond LASER in the fatigue resistance of Ti-6Al-4V alloy samples. S-N curves were determined for the reference samples and for the samples with modified surface. The topography developed and the fracture surfaces were analyzed by scanning electron microscopy. The femtosecond LASER has developed a regular surface with a bimodal distribution of microcolumns and ripples, and did not cause severe damage adjacent to the modified surface, however, has significantly reduced fatigue resistance.
publishDate 2012
dc.date.issued.fl_str_mv 2012-02-10
dc.date.accessioned.fl_str_mv 2016-09-13T18:03:48Z
dc.date.available.fl_str_mv 2016-09-13T18:03:48Z
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dc.identifier.citation.fl_str_mv SANTOS, Alan dos. Comportamento mecânico da liga Ti-6Al-4V com superfície modificada por laser de femtosegundo para uso biomédico. 2012. Dissertação (Mestrado em Ciência e Engenharia de Materiais) – Universidade Federal de São Carlos, São Carlos, 2012. Disponível em: https://repositorio.ufscar.br/handle/20.500.14289/7106.
dc.identifier.uri.fl_str_mv https://repositorio.ufscar.br/handle/20.500.14289/7106
identifier_str_mv SANTOS, Alan dos. Comportamento mecânico da liga Ti-6Al-4V com superfície modificada por laser de femtosegundo para uso biomédico. 2012. Dissertação (Mestrado em Ciência e Engenharia de Materiais) – Universidade Federal de São Carlos, São Carlos, 2012. Disponível em: https://repositorio.ufscar.br/handle/20.500.14289/7106.
url https://repositorio.ufscar.br/handle/20.500.14289/7106
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dc.publisher.none.fl_str_mv Universidade Federal de São Carlos
Câmpus São Carlos
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