Influência das temperaturas de recozimento contínuo na microestrutura e nas propriedades mecânicas de aço bifásico galvanizado da classe de resistência de 980 MPa

Detalhes bibliográficos
Ano de defesa: 2014
Autor(a) principal: Edney Amaral Moraes
Orientador(a): Não Informado pela instituição
Banca de defesa: Não Informado pela instituição
Tipo de documento: Dissertação
Tipo de acesso: Acesso aberto
Idioma: por
Instituição de defesa: Universidade Federal de Minas Gerais
Programa de Pós-Graduação: Não Informado pela instituição
Departamento: Não Informado pela instituição
País: Não Informado pela instituição
Palavras-chave em Português:
Link de acesso: https://hdl.handle.net/1843/BUBD-9ZRGQZ
Resumo: Dual phase steels constitutes a family of high strength steels characterized by comprising a hard second phase, generally martensite dispersed in a ferrite matrix. Dual phase steels are strongly dependent on the microstructure obtained to meet the needs in its application and ultimately the required mechanical properties. Besides the parameters associated with hot rolling and cold rolling, together with the chemical composition, the process of continuous intercritical annealing directly affects the microstructure formation and consequently the mechanical properties. In this study, was evaluated via Gleeble thermo-mechanical simulator, the effect of varying two parameters intercritical annealing on the microstructure and mechanical properties of a dual phase steel of 980 MPa class (DP980) as follows: soaking temperature and slow cooling temperature. Five soaking temperatures, 720°C, 750°C, 780°C, 810°C and 840°C were evaluated by setting the slow cooling temperature at 670°C. Subsequently, using soaking temperature of 780°C five slow cooling temperatures, 610°C, 640°C, 670°C, 700°C and 730°C were tested. Aiming to evaluate the microstructural evolution during the stages of heating, soaking and slow cooling, interrupted tests were performed by the use of high cooling rates of the specimens. The temperatures tested were in the region of heating 500°C, 600°C, 620°C, 640°C, 660°C, 680°C and 700°C. For soaking temperatures of 750°C, 780°C and 810°C, the tests were stopped at the beginning and at the end of the soaking for microstructural evaluation. Analyzes by optical and scanning electron microscopy (SEM) revealed that the first microstructural variation in the region of heating was the spheroidization of carbides and later recrystallization of ferrite, which began approximately at the temperature of 660°C. At the temperature of 720°C throughout the ferrite was already recrystallized and the first nucleus of the austenite were observed on the boundaries of ferritic grains. Was observed increase in yield strength and tensile strength with increasing soaking temperature. The total elongation, uniform elongation and strain hardening exponent tended to decrease with increasing soaking temperature. The increased mechanical resistance and reduced ductility were due to the increased fraction of the constituents of the second phase (bainite, martensite and MA), ranging from 14% to 54% for soaking temperatures of 720°C and 840°C, respectively. The various slow cooling temperatures showed no great influence on the microstructure and mechanical properties, fixing the soaking temperature at 780°C. The microstructure obtained is basically composed of ferrite, bainite, martensite and MA constituent, as in other tests. At all slow cooling temperatures tested the tensile strength was over 980 MPa and the volume fraction of the second phase was 44% on average.
id UFMG_e5232e5dce0240fcbfd7b4f775da1096
oai_identifier_str oai:repositorio.ufmg.br:1843/BUBD-9ZRGQZ
network_acronym_str UFMG
network_name_str Repositório Institucional da UFMG
repository_id_str
spelling 2019-08-11T23:11:52Z2025-09-08T22:51:36Z2019-08-11T23:11:52Z2014-12-05https://hdl.handle.net/1843/BUBD-9ZRGQZDual phase steels constitutes a family of high strength steels characterized by comprising a hard second phase, generally martensite dispersed in a ferrite matrix. Dual phase steels are strongly dependent on the microstructure obtained to meet the needs in its application and ultimately the required mechanical properties. Besides the parameters associated with hot rolling and cold rolling, together with the chemical composition, the process of continuous intercritical annealing directly affects the microstructure formation and consequently the mechanical properties. In this study, was evaluated via Gleeble thermo-mechanical simulator, the effect of varying two parameters intercritical annealing on the microstructure and mechanical properties of a dual phase steel of 980 MPa class (DP980) as follows: soaking temperature and slow cooling temperature. Five soaking temperatures, 720°C, 750°C, 780°C, 810°C and 840°C were evaluated by setting the slow cooling temperature at 670°C. Subsequently, using soaking temperature of 780°C five slow cooling temperatures, 610°C, 640°C, 670°C, 700°C and 730°C were tested. Aiming to evaluate the microstructural evolution during the stages of heating, soaking and slow cooling, interrupted tests were performed by the use of high cooling rates of the specimens. The temperatures tested were in the region of heating 500°C, 600°C, 620°C, 640°C, 660°C, 680°C and 700°C. For soaking temperatures of 750°C, 780°C and 810°C, the tests were stopped at the beginning and at the end of the soaking for microstructural evaluation. Analyzes by optical and scanning electron microscopy (SEM) revealed that the first microstructural variation in the region of heating was the spheroidization of carbides and later recrystallization of ferrite, which began approximately at the temperature of 660°C. At the temperature of 720°C throughout the ferrite was already recrystallized and the first nucleus of the austenite were observed on the boundaries of ferritic grains. Was observed increase in yield strength and tensile strength with increasing soaking temperature. The total elongation, uniform elongation and strain hardening exponent tended to decrease with increasing soaking temperature. The increased mechanical resistance and reduced ductility were due to the increased fraction of the constituents of the second phase (bainite, martensite and MA), ranging from 14% to 54% for soaking temperatures of 720°C and 840°C, respectively. The various slow cooling temperatures showed no great influence on the microstructure and mechanical properties, fixing the soaking temperature at 780°C. The microstructure obtained is basically composed of ferrite, bainite, martensite and MA constituent, as in other tests. At all slow cooling temperatures tested the tensile strength was over 980 MPa and the volume fraction of the second phase was 44% on average.Universidade Federal de Minas GeraisMateriais e de MinasEngenharia MetalúrgicaEngenharia metalúrgicaInfluência das temperaturas de recozimento contínuo na microestrutura e nas propriedades mecânicas de aço bifásico galvanizado da classe de resistência de 980 MPainfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/masterThesisEdney Amaral Moraesinfo:eu-repo/semantics/openAccessporreponame:Repositório Institucional da UFMGinstname:Universidade Federal de Minas Gerais (UFMG)instacron:UFMGDagoberto Brandao SantosVicente Tadeu Lopes BuonoRoberta de Oliveira RochaAços bifásicos ou dual phase constituem uma família de aços de alta resistência caracterizados pela microestrutura composta por um segundo constituinte duro, geralmente martensita, dispersa na matriz ferrítica. Os aços bifásicos são fortemente dependentes da microestrutura para atender às necessidades na sua aplicação, e fundamentalmente as propriedades mecânicas requeridas. Além dos parâmetros associados à laminação a quente e laminação a frio, em conjunto com a composição química, o processo de recozimento contínuo intercrítico afeta diretamente a formação microestrutural e por consequência as propriedades mecânicas. Nesse trabalho foi avaliado, via simulador termomecânico Gleeble, o efeito da variação de dois parâmetros de recozimento intercrítico na microestrutura e propriedades mecânicas de um aço bifásico da classe de 980 MPa (DP980), a saber: temperatura de encharque (TE) e temperatura de fim de resfriamento lento (TRL). Foram avaliadas cinco temperaturas de encharque, 720°C, 750°C, 780°C, 810°C, e 840°C, fixando a temperatura de fim de resfriamento lento em 670°C. Posteriormente, para a temperatura de encharque de 780°C foram testadas cinco temperaturas de fim de resfriamento lento, 610°C, 640°C, 670°C, 700°C e 730°C. Com o objetivo de avaliar a evolução da microestrutura durante as etapas de aquecimento, encharque e resfriamento lento foram realizados ensaios interrompidos, mediante o emprego de altas taxas de resfriamento dos corpos de prova. As temperaturas testadas na região de aquecimento foram de 500°C, 600°C, 620°C, 640°C, 660°C, 680°C e 700°C. Para as temperaturas de encharque de 750°C, 780°C e 810°C os ensaios foram interrompidos no início e no fim do encharque para avaliação microestrutural. Análises via microscopia óptica e eletrônica de varredura (MEV) revelaram que a primeira variação microestrutural na região de aquecimento foi a esferoidização de carbonetos e, posteriormente, a recristalização da ferrita, que se iniciou aproximadamente na temperatura de 660°C. Na temperatura de 720°C toda a ferrita já se encontrava recristalizada e os primeiros núcleos da austenita foram observados nos contornos de grãos ferríticos. Na região de encharque foi observado que quanto maior o tempo e a temperatura, maior a fração de austenita formada. Observou-se aumento do limite de escoamento e limite de resistência com o aumento da temperatura de encharque. O alongamento total, alongamento uniforme e expoente de encruamento apresentaram tendência de queda com o aumento da temperatura de encharque. O aumento da resistência mecânica e redução da ductilidade foram devidos ao aumento da fração do segundo constituinte (considerando a soma de bainita, martensita e MA), variando de 14% a 54% para as temperaturas de encharque de 720°C e 840°C, respectivamente. As diferentes temperaturas de fim de resfriamento lento não apresentaram grande influência na microestrutura e nas propriedades mecânicas, fixando a TE em 780°C. A microestrutura obtida é composta basicamente por ferrita, bainita, martensita e constituinte MA, assim como nos demais testes. Em todas as temperaturas testadas de fim de resfriamento lento o limite de resistência ficou acima de 980 MPa e a fração volumétrica da segunda fase foi em média 44%.UFMGORIGINALdisserta__o_mestrado_edney_moraes_v3.pdfapplication/pdf9105301https://repositorio.ufmg.br//bitstreams/ea593e72-27be-4e41-8fc1-14fadafb920e/downloadea9945ac983476ff4b8c874575cc79a4MD51trueAnonymousREADTEXTdisserta__o_mestrado_edney_moraes_v3.pdf.txttext/plain145116https://repositorio.ufmg.br//bitstreams/fe9f1e02-88b7-4110-83b3-c7c946fc1557/download695fc5e867b3df04ca05d7f614ad7e0fMD52falseAnonymousREAD1843/BUBD-9ZRGQZ2025-09-08 19:51:36.534open.accessoai:repositorio.ufmg.br:1843/BUBD-9ZRGQZhttps://repositorio.ufmg.br/Repositório InstitucionalPUBhttps://repositorio.ufmg.br/oairepositorio@ufmg.bropendoar:2025-09-08T22:51:36Repositório Institucional da UFMG - Universidade Federal de Minas Gerais (UFMG)false
dc.title.none.fl_str_mv Influência das temperaturas de recozimento contínuo na microestrutura e nas propriedades mecânicas de aço bifásico galvanizado da classe de resistência de 980 MPa
title Influência das temperaturas de recozimento contínuo na microestrutura e nas propriedades mecânicas de aço bifásico galvanizado da classe de resistência de 980 MPa
spellingShingle Influência das temperaturas de recozimento contínuo na microestrutura e nas propriedades mecânicas de aço bifásico galvanizado da classe de resistência de 980 MPa
Edney Amaral Moraes
Engenharia metalúrgica
Materiais e de Minas
Engenharia Metalúrgica
title_short Influência das temperaturas de recozimento contínuo na microestrutura e nas propriedades mecânicas de aço bifásico galvanizado da classe de resistência de 980 MPa
title_full Influência das temperaturas de recozimento contínuo na microestrutura e nas propriedades mecânicas de aço bifásico galvanizado da classe de resistência de 980 MPa
title_fullStr Influência das temperaturas de recozimento contínuo na microestrutura e nas propriedades mecânicas de aço bifásico galvanizado da classe de resistência de 980 MPa
title_full_unstemmed Influência das temperaturas de recozimento contínuo na microestrutura e nas propriedades mecânicas de aço bifásico galvanizado da classe de resistência de 980 MPa
title_sort Influência das temperaturas de recozimento contínuo na microestrutura e nas propriedades mecânicas de aço bifásico galvanizado da classe de resistência de 980 MPa
author Edney Amaral Moraes
author_facet Edney Amaral Moraes
author_role author
dc.contributor.author.fl_str_mv Edney Amaral Moraes
dc.subject.por.fl_str_mv Engenharia metalúrgica
topic Engenharia metalúrgica
Materiais e de Minas
Engenharia Metalúrgica
dc.subject.other.none.fl_str_mv Materiais e de Minas
Engenharia Metalúrgica
description Dual phase steels constitutes a family of high strength steels characterized by comprising a hard second phase, generally martensite dispersed in a ferrite matrix. Dual phase steels are strongly dependent on the microstructure obtained to meet the needs in its application and ultimately the required mechanical properties. Besides the parameters associated with hot rolling and cold rolling, together with the chemical composition, the process of continuous intercritical annealing directly affects the microstructure formation and consequently the mechanical properties. In this study, was evaluated via Gleeble thermo-mechanical simulator, the effect of varying two parameters intercritical annealing on the microstructure and mechanical properties of a dual phase steel of 980 MPa class (DP980) as follows: soaking temperature and slow cooling temperature. Five soaking temperatures, 720°C, 750°C, 780°C, 810°C and 840°C were evaluated by setting the slow cooling temperature at 670°C. Subsequently, using soaking temperature of 780°C five slow cooling temperatures, 610°C, 640°C, 670°C, 700°C and 730°C were tested. Aiming to evaluate the microstructural evolution during the stages of heating, soaking and slow cooling, interrupted tests were performed by the use of high cooling rates of the specimens. The temperatures tested were in the region of heating 500°C, 600°C, 620°C, 640°C, 660°C, 680°C and 700°C. For soaking temperatures of 750°C, 780°C and 810°C, the tests were stopped at the beginning and at the end of the soaking for microstructural evaluation. Analyzes by optical and scanning electron microscopy (SEM) revealed that the first microstructural variation in the region of heating was the spheroidization of carbides and later recrystallization of ferrite, which began approximately at the temperature of 660°C. At the temperature of 720°C throughout the ferrite was already recrystallized and the first nucleus of the austenite were observed on the boundaries of ferritic grains. Was observed increase in yield strength and tensile strength with increasing soaking temperature. The total elongation, uniform elongation and strain hardening exponent tended to decrease with increasing soaking temperature. The increased mechanical resistance and reduced ductility were due to the increased fraction of the constituents of the second phase (bainite, martensite and MA), ranging from 14% to 54% for soaking temperatures of 720°C and 840°C, respectively. The various slow cooling temperatures showed no great influence on the microstructure and mechanical properties, fixing the soaking temperature at 780°C. The microstructure obtained is basically composed of ferrite, bainite, martensite and MA constituent, as in other tests. At all slow cooling temperatures tested the tensile strength was over 980 MPa and the volume fraction of the second phase was 44% on average.
publishDate 2014
dc.date.issued.fl_str_mv 2014-12-05
dc.date.accessioned.fl_str_mv 2019-08-11T23:11:52Z
2025-09-08T22:51:36Z
dc.date.available.fl_str_mv 2019-08-11T23:11:52Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/masterThesis
format masterThesis
status_str publishedVersion
dc.identifier.uri.fl_str_mv https://hdl.handle.net/1843/BUBD-9ZRGQZ
url https://hdl.handle.net/1843/BUBD-9ZRGQZ
dc.language.iso.fl_str_mv por
language por
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.publisher.none.fl_str_mv Universidade Federal de Minas Gerais
publisher.none.fl_str_mv Universidade Federal de Minas Gerais
dc.source.none.fl_str_mv reponame:Repositório Institucional da UFMG
instname:Universidade Federal de Minas Gerais (UFMG)
instacron:UFMG
instname_str Universidade Federal de Minas Gerais (UFMG)
instacron_str UFMG
institution UFMG
reponame_str Repositório Institucional da UFMG
collection Repositório Institucional da UFMG
bitstream.url.fl_str_mv https://repositorio.ufmg.br//bitstreams/ea593e72-27be-4e41-8fc1-14fadafb920e/download
https://repositorio.ufmg.br//bitstreams/fe9f1e02-88b7-4110-83b3-c7c946fc1557/download
bitstream.checksum.fl_str_mv ea9945ac983476ff4b8c874575cc79a4
695fc5e867b3df04ca05d7f614ad7e0f
bitstream.checksumAlgorithm.fl_str_mv MD5
MD5
repository.name.fl_str_mv Repositório Institucional da UFMG - Universidade Federal de Minas Gerais (UFMG)
repository.mail.fl_str_mv repositorio@ufmg.br
_version_ 1862105858124546048