Exportação concluída — 

Uso do pó das folhas do melão de São Caetano (Momordica charantia l.), obtido por secagem em camada de espuma, em formulações cosméticas capilares

Detalhes bibliográficos
Ano de defesa: 2022
Autor(a) principal: Almeida, Elaine Cristina Castro
Orientador(a): Não Informado pela instituição
Banca de defesa: Não Informado pela instituição
Tipo de documento: Dissertação
Tipo de acesso: Acesso aberto
Idioma: por
Instituição de defesa: Universidade Federal da Paraíba
Brasil
Engenharia Química
Programa de Pós-Graduação em Engenharia Química
UFPB
Programa de Pós-Graduação: Não Informado pela instituição
Departamento: Não Informado pela instituição
País: Não Informado pela instituição
Palavras-chave em Português:
Link de acesso: https://repositorio.ufpb.br/jspui/handle/123456789/25145
Resumo: The São Caetano melon (Momordica charantia L.) is a plant belonging to the cucurbitaceae family. It originated in Asia and is currently considered an invasive plant in tropical and subtropical countries, due to its rapid adaptation in these regions. Leaves, flowers and fruits have significant chemical and nutritional composition and activities such as antioxidant, antimicrobial and anti-inflammatory have already been proven in several parts of this plant. Global demand for natural cosmetics has been growing considerably in recent years, driven by sustainability and wellness trends. Consumers become interested in raw materials of natural origin that add value to the final product. The drying process is of great importance to ensure the quality and stability of plant species, reducing the risk of proliferation of microorganisms, since there is a reduction in water present in the material. Among the various drying techniques, the foam layer has been widely studied due to its low cost and high efficiency in removing moisture. The objective of this work was to obtain powder from the leaves of São Caetano melon, from drying in a foam layer, for later use in hair cosmetic formulations. For physicochemical characterization of the obtained powder, analyzes of pH, ash, moisture, solubility, total titratable acidity, measurement of brix and lipids, in addition to determinations of ascorbic acid, phenolic compounds and granulometry were performed. Adsorption isotherms were developed following an adaptation of the method proposed by Spiess and Wolf (1987). Samples were weighed with 0.5 g and taken for water activity reading, at the initial time and at regular time intervals. The temperatures in this study were 15; 30 and 45°C. For the development of shampoo and conditioner, concentrations of 0.5; 1.5 and 2.0% of the powder. The isotherms showed statistically significant values and were adjusted for the linear, Oswin and Peleg BET models, when analyzed individually and in groups. The obtained powder presented an average of 10.15% of humidity and a very low solubility rate, when compared with other materials. The content of lipids, vitamin C and phenolic compounds showed better results than some found in the literature for other studies. To compare the effects of the foaming agent used, a lyophilization drying was performed. The efficiency of the formulations was evaluated by means of foam and surface tension tests, for shampoos, and by combability tests and strands of different hair types. The foams and surface tensions of the formulations developed were equivalent to market products. For combing, concentrations of 1.5 and 2.0% obtained the best results. When analyzing the brightness, all the concentrations used proved to be efficient. In the accelerated stability study, the shampoo proved to be unstable over the weeks, requiring a formula adjustment. The conditioner was stable, with no change in viscosity, just a slight change in pH. From what has been observed, the powder of São Caetano melon leaves can be an alternative for use as an active in cosmetic formulations.
id UFPB-2_00a181de01735d4165d9181ada49df28
oai_identifier_str oai:repositorio.ufpb.br:123456789/25145
network_acronym_str UFPB-2
network_name_str Repositório Institucional da UFPB
repository_id_str
spelling Uso do pó das folhas do melão de São Caetano (Momordica charantia l.), obtido por secagem em camada de espuma, em formulações cosméticas capilaresIsotermasXampuCondicionadorCosméticosIsothermsShampooConditionerCosmeticsCNPQ::ENGENHARIAS::ENGENHARIA QUIMICAThe São Caetano melon (Momordica charantia L.) is a plant belonging to the cucurbitaceae family. It originated in Asia and is currently considered an invasive plant in tropical and subtropical countries, due to its rapid adaptation in these regions. Leaves, flowers and fruits have significant chemical and nutritional composition and activities such as antioxidant, antimicrobial and anti-inflammatory have already been proven in several parts of this plant. Global demand for natural cosmetics has been growing considerably in recent years, driven by sustainability and wellness trends. Consumers become interested in raw materials of natural origin that add value to the final product. The drying process is of great importance to ensure the quality and stability of plant species, reducing the risk of proliferation of microorganisms, since there is a reduction in water present in the material. Among the various drying techniques, the foam layer has been widely studied due to its low cost and high efficiency in removing moisture. The objective of this work was to obtain powder from the leaves of São Caetano melon, from drying in a foam layer, for later use in hair cosmetic formulations. For physicochemical characterization of the obtained powder, analyzes of pH, ash, moisture, solubility, total titratable acidity, measurement of brix and lipids, in addition to determinations of ascorbic acid, phenolic compounds and granulometry were performed. Adsorption isotherms were developed following an adaptation of the method proposed by Spiess and Wolf (1987). Samples were weighed with 0.5 g and taken for water activity reading, at the initial time and at regular time intervals. The temperatures in this study were 15; 30 and 45°C. For the development of shampoo and conditioner, concentrations of 0.5; 1.5 and 2.0% of the powder. The isotherms showed statistically significant values and were adjusted for the linear, Oswin and Peleg BET models, when analyzed individually and in groups. The obtained powder presented an average of 10.15% of humidity and a very low solubility rate, when compared with other materials. The content of lipids, vitamin C and phenolic compounds showed better results than some found in the literature for other studies. To compare the effects of the foaming agent used, a lyophilization drying was performed. The efficiency of the formulations was evaluated by means of foam and surface tension tests, for shampoos, and by combability tests and strands of different hair types. The foams and surface tensions of the formulations developed were equivalent to market products. For combing, concentrations of 1.5 and 2.0% obtained the best results. When analyzing the brightness, all the concentrations used proved to be efficient. In the accelerated stability study, the shampoo proved to be unstable over the weeks, requiring a formula adjustment. The conditioner was stable, with no change in viscosity, just a slight change in pH. From what has been observed, the powder of São Caetano melon leaves can be an alternative for use as an active in cosmetic formulations.O melão de São Caetano (Momordica charantia L.) é uma planta pertencente à família cucurbitaceae. Teve sua origem na Asia e atualmente é considerada planta invasora de países tropicais e subtropicais, devido a rápida adaptação nessas regiões. Folhas, flores e frutos apresentam composição química e nutricional significativa e atividades como antioxidante, antimicrobiana e anti-inflamatória já foram comprovadas em diversas partes dessa planta. A demanda global por cosméticos naturais está crescendo consideravelmente nos últimos anos, impulsionada por tendências de sustentabilidade e bem-estar. Os consumidores passam a ter interesse em matérias-primas de origem natural que agreguem valor ao produto final. O processo de secagem é de grande importância para assegurar qualidade e estabilidade de espécies vegetais, diminuindo o risco de proliferação de microrganismos, uma vez que ocorre a redução de água, presente no material. Entre as diversas técnicas de secagem, a em camada de espuma vem sendo muito estudada devido ao seu baixo custo e alta eficiência na remoção da umidade. O presente trabalho teve como objetivo obter o pó das folhas do melão de São Caetano, a partir da secagem em camada de espuma, para posterior utilização em formulações cosméticas capilares. Para caraterização físico-química do pó obtido foram realizadas análises de pH, cinzas, umidade, solubilidade, acidez total titulável, medida de brix e lipídeos, além das determinações de ácido ascórbico, compostos fenólicos e granulometria. As isotermas de adsorção desenvolveram-se seguindo uma adaptação do método proposto por Spiess e Wolf (1987). Foram pesadas amostras com 0,5 g e levadas para leitura de atividade de água, no tempo inicial e em intervalos regulares de tempo. As temperaturas desse estudo foram de 15; 30 e 45 °C. Para o desenvolvimento do xampu e condicionador utilizaram-se as concentrações de 0,5; 1,5 e 2,0% do pó. As isotermas apresentaram valores estatisticamente significativos e se ajustaram para os modelos BET linear, Oswin e Peleg, quando analisados de forma individual e agrupadas. O pó obtido apresentou uma média de 10,15% de umidade e uma taxa de solubilidade muito baixa, quando comparado com outros materiais. O teor de lipídeos, vitamina C e compostos fenólicos apresentaram resultados superiores a alguns encontrados na literatura para outros estudos. Para comparar os efeitos do agente espumante utilizado, foi realizado uma secagem por liofilização. A eficiência das formulações foi avaliada por meio de testes de espuma e tensão superficial, para os xampus, e por testes de penteabilidade e mechas de diferentes tipos de cabelo. As espumas e tensões superficiais das formulações desenvolvidas se equipararam a produtos de mercado. Para a penteabilidade, as concentrações de 1,5 e 2,0% obtiveram os melhores resultados. Ao analisar o brilho, todas as concentrações utilizadas se mostraram eficientes. No estudo de estabilidade acelerada, o xampu se mostrou instável ao longo das semanas, sendo necessário um ajuste de fórmula. O condicionador se apresentou estável, sem nenhuma alteração na viscosidade, apenas uma leve mudança no pH. A partir do que foi observado, o pó das folhas do melão de São Caetano pode ser uma alternativa para a utilização como ativo em formulações cosméticas.Universidade Federal da ParaíbaBrasilEngenharia QuímicaPrograma de Pós-Graduação em Engenharia QuímicaUFPBCavalcante, Josilene de Assishttp://lattes.cnpq.br/5620795941510888Cornélio, Melânia Lopeshttp://lattes.cnpq.br/9470334173934601Almeida, Elaine Cristina Castro2022-10-19T18:33:46Z2022-06-132022-10-19T18:33:46Z2022-03-28info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/masterThesishttps://repositorio.ufpb.br/jspui/handle/123456789/25145porhttp://creativecommons.org/licenses/by-nd/3.0/br/info:eu-repo/semantics/openAccessreponame:Repositório Institucional da UFPBinstname:Universidade Federal da Paraíba (UFPB)instacron:UFPB2022-10-25T12:21:07Zoai:repositorio.ufpb.br:123456789/25145Repositório InstitucionalPUBhttps://repositorio.ufpb.br/oai/requestdiretoria@ufpb.br||bdtd@biblioteca.ufpb.bropendoar:25462022-10-25T12:21:07Repositório Institucional da UFPB - Universidade Federal da Paraíba (UFPB)false
dc.title.none.fl_str_mv Uso do pó das folhas do melão de São Caetano (Momordica charantia l.), obtido por secagem em camada de espuma, em formulações cosméticas capilares
title Uso do pó das folhas do melão de São Caetano (Momordica charantia l.), obtido por secagem em camada de espuma, em formulações cosméticas capilares
spellingShingle Uso do pó das folhas do melão de São Caetano (Momordica charantia l.), obtido por secagem em camada de espuma, em formulações cosméticas capilares
Almeida, Elaine Cristina Castro
Isotermas
Xampu
Condicionador
Cosméticos
Isotherms
Shampoo
Conditioner
Cosmetics
CNPQ::ENGENHARIAS::ENGENHARIA QUIMICA
title_short Uso do pó das folhas do melão de São Caetano (Momordica charantia l.), obtido por secagem em camada de espuma, em formulações cosméticas capilares
title_full Uso do pó das folhas do melão de São Caetano (Momordica charantia l.), obtido por secagem em camada de espuma, em formulações cosméticas capilares
title_fullStr Uso do pó das folhas do melão de São Caetano (Momordica charantia l.), obtido por secagem em camada de espuma, em formulações cosméticas capilares
title_full_unstemmed Uso do pó das folhas do melão de São Caetano (Momordica charantia l.), obtido por secagem em camada de espuma, em formulações cosméticas capilares
title_sort Uso do pó das folhas do melão de São Caetano (Momordica charantia l.), obtido por secagem em camada de espuma, em formulações cosméticas capilares
author Almeida, Elaine Cristina Castro
author_facet Almeida, Elaine Cristina Castro
author_role author
dc.contributor.none.fl_str_mv Cavalcante, Josilene de Assis
http://lattes.cnpq.br/5620795941510888
Cornélio, Melânia Lopes
http://lattes.cnpq.br/9470334173934601
dc.contributor.author.fl_str_mv Almeida, Elaine Cristina Castro
dc.subject.por.fl_str_mv Isotermas
Xampu
Condicionador
Cosméticos
Isotherms
Shampoo
Conditioner
Cosmetics
CNPQ::ENGENHARIAS::ENGENHARIA QUIMICA
topic Isotermas
Xampu
Condicionador
Cosméticos
Isotherms
Shampoo
Conditioner
Cosmetics
CNPQ::ENGENHARIAS::ENGENHARIA QUIMICA
description The São Caetano melon (Momordica charantia L.) is a plant belonging to the cucurbitaceae family. It originated in Asia and is currently considered an invasive plant in tropical and subtropical countries, due to its rapid adaptation in these regions. Leaves, flowers and fruits have significant chemical and nutritional composition and activities such as antioxidant, antimicrobial and anti-inflammatory have already been proven in several parts of this plant. Global demand for natural cosmetics has been growing considerably in recent years, driven by sustainability and wellness trends. Consumers become interested in raw materials of natural origin that add value to the final product. The drying process is of great importance to ensure the quality and stability of plant species, reducing the risk of proliferation of microorganisms, since there is a reduction in water present in the material. Among the various drying techniques, the foam layer has been widely studied due to its low cost and high efficiency in removing moisture. The objective of this work was to obtain powder from the leaves of São Caetano melon, from drying in a foam layer, for later use in hair cosmetic formulations. For physicochemical characterization of the obtained powder, analyzes of pH, ash, moisture, solubility, total titratable acidity, measurement of brix and lipids, in addition to determinations of ascorbic acid, phenolic compounds and granulometry were performed. Adsorption isotherms were developed following an adaptation of the method proposed by Spiess and Wolf (1987). Samples were weighed with 0.5 g and taken for water activity reading, at the initial time and at regular time intervals. The temperatures in this study were 15; 30 and 45°C. For the development of shampoo and conditioner, concentrations of 0.5; 1.5 and 2.0% of the powder. The isotherms showed statistically significant values and were adjusted for the linear, Oswin and Peleg BET models, when analyzed individually and in groups. The obtained powder presented an average of 10.15% of humidity and a very low solubility rate, when compared with other materials. The content of lipids, vitamin C and phenolic compounds showed better results than some found in the literature for other studies. To compare the effects of the foaming agent used, a lyophilization drying was performed. The efficiency of the formulations was evaluated by means of foam and surface tension tests, for shampoos, and by combability tests and strands of different hair types. The foams and surface tensions of the formulations developed were equivalent to market products. For combing, concentrations of 1.5 and 2.0% obtained the best results. When analyzing the brightness, all the concentrations used proved to be efficient. In the accelerated stability study, the shampoo proved to be unstable over the weeks, requiring a formula adjustment. The conditioner was stable, with no change in viscosity, just a slight change in pH. From what has been observed, the powder of São Caetano melon leaves can be an alternative for use as an active in cosmetic formulations.
publishDate 2022
dc.date.none.fl_str_mv 2022-10-19T18:33:46Z
2022-06-13
2022-10-19T18:33:46Z
2022-03-28
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/masterThesis
format masterThesis
status_str publishedVersion
dc.identifier.uri.fl_str_mv https://repositorio.ufpb.br/jspui/handle/123456789/25145
url https://repositorio.ufpb.br/jspui/handle/123456789/25145
dc.language.iso.fl_str_mv por
language por
dc.rights.driver.fl_str_mv http://creativecommons.org/licenses/by-nd/3.0/br/
info:eu-repo/semantics/openAccess
rights_invalid_str_mv http://creativecommons.org/licenses/by-nd/3.0/br/
eu_rights_str_mv openAccess
dc.publisher.none.fl_str_mv Universidade Federal da Paraíba
Brasil
Engenharia Química
Programa de Pós-Graduação em Engenharia Química
UFPB
publisher.none.fl_str_mv Universidade Federal da Paraíba
Brasil
Engenharia Química
Programa de Pós-Graduação em Engenharia Química
UFPB
dc.source.none.fl_str_mv reponame:Repositório Institucional da UFPB
instname:Universidade Federal da Paraíba (UFPB)
instacron:UFPB
instname_str Universidade Federal da Paraíba (UFPB)
instacron_str UFPB
institution UFPB
reponame_str Repositório Institucional da UFPB
collection Repositório Institucional da UFPB
repository.name.fl_str_mv Repositório Institucional da UFPB - Universidade Federal da Paraíba (UFPB)
repository.mail.fl_str_mv diretoria@ufpb.br||bdtd@biblioteca.ufpb.br
_version_ 1863379053920124928