Roten?ides de Derris longifolia
Ano de defesa: | 1980 |
---|---|
Autor(a) principal: | |
Orientador(a): | |
Banca de defesa: | |
Tipo de documento: | Dissertação |
Tipo de acesso: | Acesso aberto |
Idioma: | por |
Instituição de defesa: |
Universidade Federal Rural do Rio de Janeiro
|
Programa de Pós-Graduação: |
Programa de P?s-Gradua??o em Qu?mica
|
Departamento: |
Instituto de Ci?ncias Exatas
|
País: |
Brasil
|
Palavras-chave em Português: | |
Área do conhecimento CNPq: | |
Link de acesso: | https://tede.ufrrj.br/jspui/handle/jspui/4344 |
Resumo: | The benzene and petroleum ether extracts from the roots of Derris longifolia were prepared at Instituto Nacional de Pesquisas da Amaz?nia (INPA). Fractionation by chromatographia method resulted in the isolation of five rotenoids: rotenone, deguelin, 12a-hydroxyrotenone, tephrosin and 6a, 12a-dehidrorotenone and one steroid: sitosterol. The structure of the compounds were formulated on the basis of the interpretation of their spectral data. A review of spectral data of the rotenoids was described and used for the structural determinations of the compounds isolate. Verification of the chemical characteristics of the flavonoids of Derris revealed systematics interest. |
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Braz Filho, RaimundoBraz Filho, Raimundohttp://lattes.cnpq.br/7605529873093547Figueiredo, Uir Santana de2021-01-26T01:03:46Z1980-03-07FIGUEIREDO, Uir Santana de. Roten?ides de Derris longifolia. 1980. 148 f. Disserta??o (Mestrado em Qu?mica) - Instituo de Ci?ncias Exatas, Universidade Federal Rural do Rio de Janeiro, Serop?dica - RJ, 1980.https://tede.ufrrj.br/jspui/handle/jspui/4344The benzene and petroleum ether extracts from the roots of Derris longifolia were prepared at Instituto Nacional de Pesquisas da Amaz?nia (INPA). Fractionation by chromatographia method resulted in the isolation of five rotenoids: rotenone, deguelin, 12a-hydroxyrotenone, tephrosin and 6a, 12a-dehidrorotenone and one steroid: sitosterol. The structure of the compounds were formulated on the basis of the interpretation of their spectral data. A review of spectral data of the rotenoids was described and used for the structural determinations of the compounds isolate. Verification of the chemical characteristics of the flavonoids of Derris revealed systematics interest.Os extratos ?ter de petr?leo e benz?nico (da raiz) de Derris longifolia foram preparados no Instituto Nacional de Pesquisas da Amaz?nia (INPA) e fracionamento por m?todos cromatogr?ficos levou ao isolamento de cinco rotenoides: rotenona, deguelina, 12a-hidroxirotenona, tefrosina e 6a, 12a-desidrorotenona; e um esteroide: sitosterol. As estruturas das subst?ncias foram deduzidas com base na interpreta??o de seus dados espectrais. Uma revis?o de dados espectrais de rotenoides serviu de apoio para o estabelecimento das estruturas das subst?ncias isoladas. Um levantamento das caracter?sticas qu?micas de flavonoides de Derris revelou significado sistem?tico.Submitted by Jorge Silva (jorgelmsilva@ufrrj.br) on 2021-01-26T01:03:46Z No. of bitstreams: 1 1980 - Uir Santana de Figueiredo.pdf: 2486575 bytes, checksum: 5b37caf4ec23251ef1d00342bfe7b8ec (MD5)Made available in DSpace on 2021-01-26T01:03:46Z (GMT). No. of bitstreams: 1 1980 - Uir Santana de Figueiredo.pdf: 2486575 bytes, checksum: 5b37caf4ec23251ef1d00342bfe7b8ec (MD5) Previous issue date: 1980-03-07Coordena??o de Aperfei?oamento de Pessoal de N?vel Superior (CAPES)application/pdfhttps://tede.ufrrj.br/retrieve/63835/1980%20-%20Uir%20Santana%20de%20Figueiredo.pdf.jpgporUniversidade Federal Rural do Rio de JaneiroPrograma de P?s-Gradua??o em Qu?micaUFRRJBrasilInstituto de Ci?ncias ExatasDerris longifoliarotenoidesesteroideQu?micaRoten?ides de Derris longifoliainfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/masterThesisinfo:eu-repo/semantics/openAccessreponame:Biblioteca Digital de Teses e Dissertações da UFRRJinstname:Universidade Federal Rural do Rio de Janeiro (UFRRJ)instacron:UFRRJTHUMBNAIL1980 - Uir Santana de Figueiredo.pdf.jpg1980 - Uir Santana de Figueiredo.pdf.jpgimage/jpeg2007http://localhost:8080/tede/bitstream/jspui/4344/4/1980+-+Uir+Santana+de+Figueiredo.pdf.jpg25c0eb9e25245b2987bc87fd16a9490cMD54TEXT1980 - Uir Santana de Figueiredo.pdf.txt1980 - Uir Santana de Figueiredo.pdf.txttext/plain59728http://localhost:8080/tede/bitstream/jspui/4344/3/1980+-+Uir+Santana+de+Figueiredo.pdf.txt26418bb66676a5c10a8be3c4d44152cbMD53ORIGINAL1980 - Uir Santana de Figueiredo.pdf1980 - Uir Santana de Figueiredo.pdfapplication/pdf2486575http://localhost:8080/tede/bitstream/jspui/4344/2/1980+-+Uir+Santana+de+Figueiredo.pdf5b37caf4ec23251ef1d00342bfe7b8ecMD52LICENSElicense.txtlicense.txttext/plain; charset=utf-82089http://localhost:8080/tede/bitstream/jspui/4344/1/license.txt7b5ba3d2445355f386edab96125d42b7MD51jspui/43442022-06-07 11:17:25.948oai:localhost: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Biblioteca Digital de Teses e Dissertaçõeshttps://tede.ufrrj.br/PUBhttps://tede.ufrrj.br/oai/requestbibliot@ufrrj.br||bibliot@ufrrj.bropendoar:2022-06-07T14:17:25Biblioteca Digital de Teses e Dissertações da UFRRJ - Universidade Federal Rural do Rio de Janeiro (UFRRJ)false |
dc.title.por.fl_str_mv |
Roten?ides de Derris longifolia |
title |
Roten?ides de Derris longifolia |
spellingShingle |
Roten?ides de Derris longifolia Figueiredo, Uir Santana de Derris longifolia rotenoides esteroide Qu?mica |
title_short |
Roten?ides de Derris longifolia |
title_full |
Roten?ides de Derris longifolia |
title_fullStr |
Roten?ides de Derris longifolia |
title_full_unstemmed |
Roten?ides de Derris longifolia |
title_sort |
Roten?ides de Derris longifolia |
author |
Figueiredo, Uir Santana de |
author_facet |
Figueiredo, Uir Santana de |
author_role |
author |
dc.contributor.advisor1.fl_str_mv |
Braz Filho, Raimundo |
dc.contributor.referee1.fl_str_mv |
Braz Filho, Raimundo |
dc.contributor.authorLattes.fl_str_mv |
http://lattes.cnpq.br/7605529873093547 |
dc.contributor.author.fl_str_mv |
Figueiredo, Uir Santana de |
contributor_str_mv |
Braz Filho, Raimundo Braz Filho, Raimundo |
dc.subject.por.fl_str_mv |
Derris longifolia rotenoides esteroide |
topic |
Derris longifolia rotenoides esteroide Qu?mica |
dc.subject.cnpq.fl_str_mv |
Qu?mica |
description |
The benzene and petroleum ether extracts from the roots of Derris longifolia were prepared at Instituto Nacional de Pesquisas da Amaz?nia (INPA). Fractionation by chromatographia method resulted in the isolation of five rotenoids: rotenone, deguelin, 12a-hydroxyrotenone, tephrosin and 6a, 12a-dehidrorotenone and one steroid: sitosterol. The structure of the compounds were formulated on the basis of the interpretation of their spectral data. A review of spectral data of the rotenoids was described and used for the structural determinations of the compounds isolate. Verification of the chemical characteristics of the flavonoids of Derris revealed systematics interest. |
publishDate |
1980 |
dc.date.issued.fl_str_mv |
1980-03-07 |
dc.date.accessioned.fl_str_mv |
2021-01-26T01:03:46Z |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/masterThesis |
format |
masterThesis |
status_str |
publishedVersion |
dc.identifier.citation.fl_str_mv |
FIGUEIREDO, Uir Santana de. Roten?ides de Derris longifolia. 1980. 148 f. Disserta??o (Mestrado em Qu?mica) - Instituo de Ci?ncias Exatas, Universidade Federal Rural do Rio de Janeiro, Serop?dica - RJ, 1980. |
dc.identifier.uri.fl_str_mv |
https://tede.ufrrj.br/jspui/handle/jspui/4344 |
identifier_str_mv |
FIGUEIREDO, Uir Santana de. Roten?ides de Derris longifolia. 1980. 148 f. Disserta??o (Mestrado em Qu?mica) - Instituo de Ci?ncias Exatas, Universidade Federal Rural do Rio de Janeiro, Serop?dica - RJ, 1980. |
url |
https://tede.ufrrj.br/jspui/handle/jspui/4344 |
dc.language.iso.fl_str_mv |
por |
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por |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
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openAccess |
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application/pdf |
dc.publisher.none.fl_str_mv |
Universidade Federal Rural do Rio de Janeiro |
dc.publisher.program.fl_str_mv |
Programa de P?s-Gradua??o em Qu?mica |
dc.publisher.initials.fl_str_mv |
UFRRJ |
dc.publisher.country.fl_str_mv |
Brasil |
dc.publisher.department.fl_str_mv |
Instituto de Ci?ncias Exatas |
publisher.none.fl_str_mv |
Universidade Federal Rural do Rio de Janeiro |
dc.source.none.fl_str_mv |
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