Caracteriza??o qu?mica e estrutural de ?cidos h?micos em solos de tr?s sistemas de manejo

Detalhes bibliográficos
Ano de defesa: 2016
Autor(a) principal: Gomes, Ernane Tarcisio Martins lattes
Orientador(a): Berbara, Ricardo Luiz Louro
Banca de defesa: Garc?a, Andr?s Calder?n, Pereira, Marcos Gervasio, Ara?jo, Ednaldo da Silva
Tipo de documento: Dissertação
Tipo de acesso: Acesso aberto
Idioma: por
Instituição de defesa: Universidade Federal Rural do Rio de Janeiro
Programa de Pós-Graduação: Programa de P?s-Gradua??o em Agronomia - Ci?ncia do Solo
Departamento: Instituto de Agronomia
País: Brasil
Palavras-chave em Português:
Manejo agroecol?gico
Fra??es H?micas
Caracteriza??o isot?pica
Quimiometria
Palavras-chave em Inglês:
agro-ecological management
Humic Fractions
isotopic characterization
chemometrics
Área do conhecimento CNPq:
Agronomia
Link de acesso: https://tede.ufrrj.br/jspui/handle/jspui/2098
Resumo: Soil organic matter can be derived from the decomposition of animal or vegetable. Most commercial crops show photosynthetic mechanisms C3 and C4, which set different carbon isotopes C12 or C13. Through isotopic analysis can determine the origin and prevalence of type of carbon that make up the soil organic matter (SOM) in a given area. Depending on the chemical fractionation MOS can also be divided into fractions FAF, FAH and FHU, these fractions have specific characteristics depending on their origin training and ambient conditions. The objective of this study was to evaluate the influence of plant origin C3 or C4 in the formation of the chemical and molecular structure of humic substances extracted from four areas with different vegetation cover, but submitted to agroecological management. To investigate this influence were extracted humic substances (HS) of these soils, being held chemical fractionation and chemical characterization by NMR analysis, FTIR, quantification and ?13C e ?15N isotopes in the AH fraction, 13 C-CP / MAS NMR and elemental determination. From the results obtained from these analyzes it was concluded that the plant does not influence qualitative differences, but in quantitative between the chemical components of humic substances (HS), the type of photosynthetic cycle does not seem to be a determining factor in the formation and incorporation of the types of structures in HA, but rather the quantities of these structures and their humic organizational distribution. The chemometric theoretical analyzes indicate that the development and preservation of humic these soils may be possible in intensive management systems such as rotation upon application of exogenous sources of stabilized SH, as well as favoring the humidification process in less managed systems as pasture and SAF. In this study it was demonstrated by characterization and chemometrics applied to AH of an agro-ecological system, the current state of MOS in terms of stability and structural enrichment and being proposed possible avenues for recovery and preservation of SH in mineral soils that may contribute to the increase in conditions fertility and thus agricultural production.
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spelling Berbara, Ricardo Luiz Louro483.564.257-00Garc?a, Andr?s Calder?n061.145.927-27Garc?a, Andr?s Calder?nPereira, Marcos GervasioAra?jo, Ednaldo da Silva084.577.136-12http://lattes.cnpq.br/6443805133773523Gomes, Ernane Tarcisio Martins2017-10-17T17:35:44Z2016-08-17GOMES, Ernane. Caracteriza??o qu?mica e estrutural de ?cidos h?micos em solos de tr?s sistemas de manejo. 2016. 33 f. Disserta??o (Mestrado em Agronomia - Ci?ncia do Solo) - Instituto de Agronomia, Departamento de Solos, Universidade Federal Rural do Rio de Janeiro, Serop?dica, 2016.https://tede.ufrrj.br/jspui/handle/jspui/2098Soil organic matter can be derived from the decomposition of animal or vegetable. Most commercial crops show photosynthetic mechanisms C3 and C4, which set different carbon isotopes C12 or C13. Through isotopic analysis can determine the origin and prevalence of type of carbon that make up the soil organic matter (SOM) in a given area. Depending on the chemical fractionation MOS can also be divided into fractions FAF, FAH and FHU, these fractions have specific characteristics depending on their origin training and ambient conditions. The objective of this study was to evaluate the influence of plant origin C3 or C4 in the formation of the chemical and molecular structure of humic substances extracted from four areas with different vegetation cover, but submitted to agroecological management. To investigate this influence were extracted humic substances (HS) of these soils, being held chemical fractionation and chemical characterization by NMR analysis, FTIR, quantification and ?13C e ?15N isotopes in the AH fraction, 13 C-CP / MAS NMR and elemental determination. From the results obtained from these analyzes it was concluded that the plant does not influence qualitative differences, but in quantitative between the chemical components of humic substances (HS), the type of photosynthetic cycle does not seem to be a determining factor in the formation and incorporation of the types of structures in HA, but rather the quantities of these structures and their humic organizational distribution. The chemometric theoretical analyzes indicate that the development and preservation of humic these soils may be possible in intensive management systems such as rotation upon application of exogenous sources of stabilized SH, as well as favoring the humidification process in less managed systems as pasture and SAF. In this study it was demonstrated by characterization and chemometrics applied to AH of an agro-ecological system, the current state of MOS in terms of stability and structural enrichment and being proposed possible avenues for recovery and preservation of SH in mineral soils that may contribute to the increase in conditions fertility and thus agricultural production.A mat?ria org?nica do solo pode ser oriunda da decomposi??o de animais ou vegetais. A maioria das culturas comerciais apresentam mecanismos fotossint?ticos C3 ou C4, que fixam diferentes is?topos de carbono C12 ou C13. Atrav?s de an?lises isot?picas ? poss?vel determinar a origem e predomin?ncia do tipo de carbono que comp?em a mat?ria org?nica do solo (MOS) em determinada ?rea. Em fun??o do fracionamento qu?mico a MOS ainda pode ser dividida nas fra??es FAF, FAH e FHU, estas fra??es apresentam caracter?sticas especificas em fun??o da sua origem de forma??o e condi??es ambientes. O objetivo deste trabalho foi avaliar a influ?ncia da origem vegetal C3 ou C4 na forma??o da estrutura qu?mica e molecular das substancias h?micas extra?das de quatro ?reas com cobertura diferentes vegetais, por?m submetidas ao manejo agroecol?gico. Para averiguar esta influ?ncia foram extra?das as substancias h?micas (SH) destes solos, sendo realizado o fracionamento qu?mico e caracteriza??o qu?mica atrav?s de an?lises de RMN, FTIR, quantifica??o de is?topos ?13C e?15N na fra??o de AH, 13C-CP/MAS NMR e a determina??o elementar. A partir dos resultados obtidos a partir dessas an?lises foi poss?vel concluir que a origem vegetal n?o influencia em diferen?as qualitativas e sim em quantitativas entre os componentes qu?micos das substancias h?micas (SH), o tipo de ciclo fotossint?tico n?o parece ser um fator determinante na forma??o e incorpora??o dos tipos de estruturas nos AH, mas sim nas quantidades destas estruturas e na sua distribui??o organizacional h?mica. As an?lises te?ricas quimiom?tricas indicam que a incorpora??o e preserva??o de MO humificada nestes solos pode ser poss?vel em sistemas de manejo intensivo como a rota??o, mediante aplica??es de fontes ex?genas de SH estabilizada, assim como tamb?m o favorecimento dos processos de humifica??o em sistemas menos manejados como pastagem e SAF. Neste estudo foi comprovado mediante carateriza??o e quimiometria aplicadas aos AH de um sistema agroecol?gico, o estado atual da MOS em termos de estabilidade e enriquecimento estrutural e sendo propostas poss?veis vias para a recupera??o e preserva??o das SH em solos minerais que possam contribuir ao aumento das condi??es de fertilidade e consequentemente da produ??o agr?cola.Submitted by Jorge Silva (jorgelmsilva@ufrrj.br) on 2017-10-17T17:35:44Z No. of bitstreams: 1 2016 - Ernane Tarcisio Martins Gomes.pdf: 1573845 bytes, checksum: 78069c6459bd2b6aba951ba371ae74fd (MD5)Made available in DSpace on 2017-10-17T17:35:44Z (GMT). No. of bitstreams: 1 2016 - Ernane Tarcisio Martins Gomes.pdf: 1573845 bytes, checksum: 78069c6459bd2b6aba951ba371ae74fd (MD5) Previous issue date: 2016-08-17CNPq - Conselho Nacional de Desenvolvimento Cient?fico e Tecnol?gicoapplication/pdfhttps://tede.ufrrj.br/retrieve/6133/2016%20-%20Ernane%20Tarcisio%20Martins%20Gomes.pdf.jpghttps://tede.ufrrj.br/retrieve/20940/2016%20-%20Ernane%20Tarcisio%20Martins%20Gomes.pdf.jpghttps://tede.ufrrj.br/retrieve/27257/2016%20-%20Ernane%20Tarcisio%20Martins%20Gomes.pdf.jpghttps://tede.ufrrj.br/retrieve/33704/2016%20-%20Ernane%20Tarcisio%20Martins%20Gomes.pdf.jpghttps://tede.ufrrj.br/retrieve/40050/2016%20-%20Ernane%20Tarcisio%20Martins%20Gomes.pdf.jpghttps://tede.ufrrj.br/retrieve/46466/2016%20-%20Ernane%20Tarcisio%20Martins%20Gomes.pdf.jpghttps://tede.ufrrj.br/retrieve/52848/2016%20-%20Ernane%20Tarcisio%20Martins%20Gomes.pdf.jpghttps://tede.ufrrj.br/retrieve/59322/2016%20-%20Ernane%20Tarcisio%20Martins%20Gomes.pdf.jpgporUniversidade Federal Rural do Rio de JaneiroPrograma de P?s-Gradua??o em Agronomia - Ci?ncia do SoloUFRRJBrasilInstituto de AgronomiaALVES, B.J.R.; CAMPOS, D. 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dc.title.por.fl_str_mv Caracteriza??o qu?mica e estrutural de ?cidos h?micos em solos de tr?s sistemas de manejo
dc.title.alternative.eng.fl_str_mv Chemical and structural characterization of humic acids in soils of three management systems
title Caracteriza??o qu?mica e estrutural de ?cidos h?micos em solos de tr?s sistemas de manejo
spellingShingle Caracteriza??o qu?mica e estrutural de ?cidos h?micos em solos de tr?s sistemas de manejo
Gomes, Ernane Tarcisio Martins
agro-ecological management
Humic Fractions
isotopic characterization
chemometrics
Manejo agroecol?gico
Fra??es H?micas
Caracteriza??o isot?pica
Quimiometria
Agronomia
title_short Caracteriza??o qu?mica e estrutural de ?cidos h?micos em solos de tr?s sistemas de manejo
title_full Caracteriza??o qu?mica e estrutural de ?cidos h?micos em solos de tr?s sistemas de manejo
title_fullStr Caracteriza??o qu?mica e estrutural de ?cidos h?micos em solos de tr?s sistemas de manejo
title_full_unstemmed Caracteriza??o qu?mica e estrutural de ?cidos h?micos em solos de tr?s sistemas de manejo
title_sort Caracteriza??o qu?mica e estrutural de ?cidos h?micos em solos de tr?s sistemas de manejo
author Gomes, Ernane Tarcisio Martins
author_facet Gomes, Ernane Tarcisio Martins
author_role author
dc.contributor.advisor1.fl_str_mv Berbara, Ricardo Luiz Louro
dc.contributor.advisor1ID.fl_str_mv 483.564.257-00
dc.contributor.advisor-co1.fl_str_mv Garc?a, Andr?s Calder?n
dc.contributor.advisor-co1ID.fl_str_mv 061.145.927-27
dc.contributor.referee1.fl_str_mv Garc?a, Andr?s Calder?n
dc.contributor.referee2.fl_str_mv Pereira, Marcos Gervasio
dc.contributor.referee3.fl_str_mv Ara?jo, Ednaldo da Silva
dc.contributor.authorID.fl_str_mv 084.577.136-12
dc.contributor.authorLattes.fl_str_mv http://lattes.cnpq.br/6443805133773523
dc.contributor.author.fl_str_mv Gomes, Ernane Tarcisio Martins
contributor_str_mv Berbara, Ricardo Luiz Louro
Garc?a, Andr?s Calder?n
Garc?a, Andr?s Calder?n
Pereira, Marcos Gervasio
Ara?jo, Ednaldo da Silva
dc.subject.eng.fl_str_mv agro-ecological management
Humic Fractions
isotopic characterization
chemometrics
topic agro-ecological management
Humic Fractions
isotopic characterization
chemometrics
Manejo agroecol?gico
Fra??es H?micas
Caracteriza??o isot?pica
Quimiometria
Agronomia
dc.subject.por.fl_str_mv Manejo agroecol?gico
Fra??es H?micas
Caracteriza??o isot?pica
Quimiometria
dc.subject.cnpq.fl_str_mv Agronomia
description Soil organic matter can be derived from the decomposition of animal or vegetable. Most commercial crops show photosynthetic mechanisms C3 and C4, which set different carbon isotopes C12 or C13. Through isotopic analysis can determine the origin and prevalence of type of carbon that make up the soil organic matter (SOM) in a given area. Depending on the chemical fractionation MOS can also be divided into fractions FAF, FAH and FHU, these fractions have specific characteristics depending on their origin training and ambient conditions. The objective of this study was to evaluate the influence of plant origin C3 or C4 in the formation of the chemical and molecular structure of humic substances extracted from four areas with different vegetation cover, but submitted to agroecological management. To investigate this influence were extracted humic substances (HS) of these soils, being held chemical fractionation and chemical characterization by NMR analysis, FTIR, quantification and ?13C e ?15N isotopes in the AH fraction, 13 C-CP / MAS NMR and elemental determination. From the results obtained from these analyzes it was concluded that the plant does not influence qualitative differences, but in quantitative between the chemical components of humic substances (HS), the type of photosynthetic cycle does not seem to be a determining factor in the formation and incorporation of the types of structures in HA, but rather the quantities of these structures and their humic organizational distribution. The chemometric theoretical analyzes indicate that the development and preservation of humic these soils may be possible in intensive management systems such as rotation upon application of exogenous sources of stabilized SH, as well as favoring the humidification process in less managed systems as pasture and SAF. In this study it was demonstrated by characterization and chemometrics applied to AH of an agro-ecological system, the current state of MOS in terms of stability and structural enrichment and being proposed possible avenues for recovery and preservation of SH in mineral soils that may contribute to the increase in conditions fertility and thus agricultural production.
publishDate 2016
dc.date.issued.fl_str_mv 2016-08-17
dc.date.accessioned.fl_str_mv 2017-10-17T17:35:44Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/masterThesis
format masterThesis
status_str publishedVersion
dc.identifier.citation.fl_str_mv GOMES, Ernane. Caracteriza??o qu?mica e estrutural de ?cidos h?micos em solos de tr?s sistemas de manejo. 2016. 33 f. Disserta??o (Mestrado em Agronomia - Ci?ncia do Solo) - Instituto de Agronomia, Departamento de Solos, Universidade Federal Rural do Rio de Janeiro, Serop?dica, 2016.
dc.identifier.uri.fl_str_mv https://tede.ufrrj.br/jspui/handle/jspui/2098
identifier_str_mv GOMES, Ernane. Caracteriza??o qu?mica e estrutural de ?cidos h?micos em solos de tr?s sistemas de manejo. 2016. 33 f. Disserta??o (Mestrado em Agronomia - Ci?ncia do Solo) - Instituto de Agronomia, Departamento de Solos, Universidade Federal Rural do Rio de Janeiro, Serop?dica, 2016.
url https://tede.ufrrj.br/jspui/handle/jspui/2098
dc.language.iso.fl_str_mv por
language por
dc.relation.references.por.fl_str_mv ALVES, B.J.R.; CAMPOS, D. V. B. de; P.; S.; M. Emprego do is?topo est?vel 13 C para o estudo da din?mica da mat?ria org?nica do solo. In: Renato Roscoe, F?bio Martins Mercante, J?lio Cesar Salton. (Org.). Din?mica da mat?ria org?nica do solo em sistemas conservacionais (Modelagem matem?tica e m?todos auxiliares. Dourados - MS: Embrapa Agropecu?ria Oeste, v., p. 133-161, (2006). ALVES, B. J. R, ZOTARELLIL, JANTALIA CP, BODDEY RM, URQUIAGA S Emprego de is?topos est?veis para o estudo do carbono e do nitrog?nio no sistema solo planta. In: Aquino, A.M.& Assis, R.L., eds. Processos biol?gicos no sistema solo-planta: Ferramentas para uma agricultura sustent?vel. Bras?lia, Embrapa-SCT, 2005.p.343-350. (2005). AMIR S, JOURAIPHY A, MEDDICH A, GHAROUS M, WINTERTO P, HAFIDI M Structural study of humic acids during composting of activated sludge-green waste: elemental analysis, FTIR and 13C NMR. J Hazard Mater 177:524-529. doi:10.1016/j.jhazmat.2009.12.064. 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