Exchange bias perpendicular em multicamadas de IrMn/Co/Pd

Detalhes bibliográficos
Ano de defesa: 2023
Autor(a) principal: Figueiró, Bruno Monteiro lattes
Orientador(a): Oliveira, Artur Harres de lattes
Banca de defesa: Gomes, Matheus Gamino, Viegas, Alexandre da Cas
Tipo de documento: Dissertação
Tipo de acesso: Acesso aberto
Idioma: por
Instituição de defesa: Universidade Federal de Santa Maria
Centro de Ciências Naturais e Exatas
Programa de Pós-Graduação: Programa de Pós-Graduação em Física
Departamento: Física
País: Brasil
Palavras-chave em Português:
AMP
Palavras-chave em Inglês:
PMA
Área do conhecimento CNPq:
Link de acesso: http://repositorio.ufsm.br/handle/1/29238
Resumo: Magnetic skyrmions are spin textures that can arise in thin films that exhibit the Dzyaloshinskii–Moriya interaction. Such interaction emerges from symmetry breaking at the interface between a ferromagnetic material and a heavy metal. Typically, skyrmions must be subjected to an external magnetic field to be stabilized, which compromises their potential for technological applications. In this work, we aimed to use the exchange bias phenomenon to replace the role of the external field in the formation of such spin textures. Thin films composed of IrMn and Co/Pd multilayers were deposited using magnetron sputtering on glass substrates. A variable-thickness Pd spacer was inserted between IrMn and the first Co layer, with the aim of gradually reducing the interaction between the antiferromagnetic and ferromagnetic layers. To induce the exchange bias phenomenon perpendicular to the film plane, the samples were subjected to heat treatments and cooled in the presence of an external magnetic field. The samples were magnetically characterized before and after treatment using AGFM and VSM techniques. Some of the as-fabricated samples exhibited perpendicular magnetic anisotropy, and after treatment, all samples showed this anisotropy. We observed a variation in the bias field and coercive field intensity with the temperature of the heat treatment and the thickness of the spacer. Magnetic force microscopy was used to observe the magnetic domain structures present in the films under three different conditions: as-fabricated samples, after magnetically saturating out-of-plane, and after an AC demagnetization protocol. Despite the presence of perpendicular anisotropy and exchange bias in most of the films, only labyrinth and bubble-type structures were observed. It was not possible to confirm the presence of skyrmions or the influence of EB on their formation.
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spelling 2023-05-29T15:34:02Z2023-05-29T15:34:02Z2023-04-26http://repositorio.ufsm.br/handle/1/29238Magnetic skyrmions are spin textures that can arise in thin films that exhibit the Dzyaloshinskii–Moriya interaction. Such interaction emerges from symmetry breaking at the interface between a ferromagnetic material and a heavy metal. Typically, skyrmions must be subjected to an external magnetic field to be stabilized, which compromises their potential for technological applications. In this work, we aimed to use the exchange bias phenomenon to replace the role of the external field in the formation of such spin textures. Thin films composed of IrMn and Co/Pd multilayers were deposited using magnetron sputtering on glass substrates. A variable-thickness Pd spacer was inserted between IrMn and the first Co layer, with the aim of gradually reducing the interaction between the antiferromagnetic and ferromagnetic layers. To induce the exchange bias phenomenon perpendicular to the film plane, the samples were subjected to heat treatments and cooled in the presence of an external magnetic field. The samples were magnetically characterized before and after treatment using AGFM and VSM techniques. Some of the as-fabricated samples exhibited perpendicular magnetic anisotropy, and after treatment, all samples showed this anisotropy. We observed a variation in the bias field and coercive field intensity with the temperature of the heat treatment and the thickness of the spacer. Magnetic force microscopy was used to observe the magnetic domain structures present in the films under three different conditions: as-fabricated samples, after magnetically saturating out-of-plane, and after an AC demagnetization protocol. Despite the presence of perpendicular anisotropy and exchange bias in most of the films, only labyrinth and bubble-type structures were observed. It was not possible to confirm the presence of skyrmions or the influence of EB on their formation.Skyrmions magnéticos são texturas de spins que podem surgir em filmes finos que apresentam a interação de Dzyaloshinskii–Moriya. Tal interação emerge da quebra de simetria na interface entre um material ferromagnético e um metal pesado. Tipicamente, os skyrmions necessitam de um campo magnético externo para serem estabilizados, o que compromete o seu potencial para aplicações tecnológicas. No presente trabalho, tínhamos como objetivo utilizar o fenômeno de exchange bias para substituir o papel do campo externo na formação de tais texturas de spin. Filmes finos compostos por IrMn e multicamadas de Co/Pd foram depositadas via magnetron sputtering sobre substratos de vidro. Entre o IrMn e a primeira camada de Co foi inserido um espaçador de Pd com espessura variável, com o intuito de diminuir gradualmente a interação entre as camadas antiferromagnética e ferromagnética. Afim de induzir o fenômeno de exchange bias em uma direção perpendicular ao plano dos filmes, as amostras foram submetidas a tratamentos térmicos e resfriados na presença de um campo externo. As amostras foram caracterizadas magneticamente como feitas e após tratadas utilizando as técnicas de AGFM e VSM. Algumas amostras como feitas apresentaram anisotropia magnética perpendicular, e após tratadas todas apresentaram esta anisotropia. Observamos uma variação na intensidade do campo de bias e campo coercivo com a temperatura de tratamento térmico utilizado e a espessura do espaçador. Microscopia de força magnética foi utilizada para observar as estruturas de domínios magnéticos presentes nos filmes em três diferentes situações: amostras como feitas, após saturadas magneticamente fora do plano e após a realização de um protocolo de desmagnetização AC. Apesar da existência de anisotropia perpendicular e exchange bias em grande parte dos filmes, somente foi possível observar estruturas do tipo labirinto e bolhas. Não sendo possível confirmar a presença de skyrmions e a influência do EB na formação destes.Coordenação de Aperfeiçoamento de Pessoal de Nível Superior - CAPESporUniversidade Federal de Santa MariaCentro de Ciências Naturais e ExatasPrograma de Pós-Graduação em FísicaUFSMBrasilFísicaAttribution-NonCommercial-NoDerivatives 4.0 Internationalhttp://creativecommons.org/licenses/by-nc-nd/4.0/info:eu-repo/semantics/openAccessSkyrmions magneticosExchange bias perpendicularAMPFilmes finosMagnetic skyrmionsPerpendicular exchange biasPMAThin filmsCNPQ::CIENCIAS EXATAS E DA TERRA::FISICAExchange bias perpendicular em multicamadas de IrMn/Co/PdPerpendicular exchange bias in IrMn/Co/Pd multilayersinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/masterThesisOliveira, Artur Harres dehttp://lattes.cnpq.br/5413344891000141Gomes, Matheus GaminoViegas, Alexandre da Cashttp://lattes.cnpq.br/4064426626269342Figueiró, Bruno Monteiro100500000006600600600600600415298f1-dc82-4dc9-8d55-f7adec36681028ee22f1-a385-4963-a790-08555a0b283bba4ed109-f8a1-416d-838a-27987cc53aafddcbbe6a-39da-488d-bfd2-af3fc2a9c937reponame:Manancial - Repositório Digital da UFSMinstname:Universidade Federal de Santa Maria (UFSM)instacron:UFSMCC-LICENSElicense_rdflicense_rdfapplication/rdf+xml; charset=utf-8805http://repositorio.ufsm.br/bitstream/1/29238/2/license_rdf4460e5956bc1d1639be9ae6146a50347MD52LICENSElicense.txtlicense.txttext/plain; charset=utf-81956http://repositorio.ufsm.br/bitstream/1/29238/3/license.txt2f0571ecee68693bd5cd3f17c1e075dfMD53ORIGINALDIS_PPGFÍSICA_2023_FIGUEIRÓ_BRUNO.pdfDIS_PPGFÍSICA_2023_FIGUEIRÓ_BRUNO.pdfDissertação de mestradoapplication/pdf18480282http://repositorio.ufsm.br/bitstream/1/29238/1/DIS_PPGF%c3%8dSICA_2023_FIGUEIR%c3%93_BRUNO.pdf35a8cb0b212c1e39f948f1bea0b94dd2MD511/292382023-05-29 12:34:02.414oai:repositorio.ufsm.br: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ório Institucionalhttp://repositorio.ufsm.br/PUBhttp://repositorio.ufsm.br/oai/requestopendoar:39132023-05-29T15:34:02Manancial - Repositório Digital da UFSM - Universidade Federal de Santa Maria (UFSM)false
dc.title.por.fl_str_mv Exchange bias perpendicular em multicamadas de IrMn/Co/Pd
dc.title.alternative.eng.fl_str_mv Perpendicular exchange bias in IrMn/Co/Pd multilayers
title Exchange bias perpendicular em multicamadas de IrMn/Co/Pd
spellingShingle Exchange bias perpendicular em multicamadas de IrMn/Co/Pd
Figueiró, Bruno Monteiro
Skyrmions magneticos
Exchange bias perpendicular
AMP
Filmes finos
Magnetic skyrmions
Perpendicular exchange bias
PMA
Thin films
CNPQ::CIENCIAS EXATAS E DA TERRA::FISICA
title_short Exchange bias perpendicular em multicamadas de IrMn/Co/Pd
title_full Exchange bias perpendicular em multicamadas de IrMn/Co/Pd
title_fullStr Exchange bias perpendicular em multicamadas de IrMn/Co/Pd
title_full_unstemmed Exchange bias perpendicular em multicamadas de IrMn/Co/Pd
title_sort Exchange bias perpendicular em multicamadas de IrMn/Co/Pd
author Figueiró, Bruno Monteiro
author_facet Figueiró, Bruno Monteiro
author_role author
dc.contributor.advisor1.fl_str_mv Oliveira, Artur Harres de
dc.contributor.advisor1Lattes.fl_str_mv http://lattes.cnpq.br/5413344891000141
dc.contributor.referee1.fl_str_mv Gomes, Matheus Gamino
dc.contributor.referee2.fl_str_mv Viegas, Alexandre da Cas
dc.contributor.authorLattes.fl_str_mv http://lattes.cnpq.br/4064426626269342
dc.contributor.author.fl_str_mv Figueiró, Bruno Monteiro
contributor_str_mv Oliveira, Artur Harres de
Gomes, Matheus Gamino
Viegas, Alexandre da Cas
dc.subject.por.fl_str_mv Skyrmions magneticos
Exchange bias perpendicular
AMP
Filmes finos
topic Skyrmions magneticos
Exchange bias perpendicular
AMP
Filmes finos
Magnetic skyrmions
Perpendicular exchange bias
PMA
Thin films
CNPQ::CIENCIAS EXATAS E DA TERRA::FISICA
dc.subject.eng.fl_str_mv Magnetic skyrmions
Perpendicular exchange bias
PMA
Thin films
dc.subject.cnpq.fl_str_mv CNPQ::CIENCIAS EXATAS E DA TERRA::FISICA
description Magnetic skyrmions are spin textures that can arise in thin films that exhibit the Dzyaloshinskii–Moriya interaction. Such interaction emerges from symmetry breaking at the interface between a ferromagnetic material and a heavy metal. Typically, skyrmions must be subjected to an external magnetic field to be stabilized, which compromises their potential for technological applications. In this work, we aimed to use the exchange bias phenomenon to replace the role of the external field in the formation of such spin textures. Thin films composed of IrMn and Co/Pd multilayers were deposited using magnetron sputtering on glass substrates. A variable-thickness Pd spacer was inserted between IrMn and the first Co layer, with the aim of gradually reducing the interaction between the antiferromagnetic and ferromagnetic layers. To induce the exchange bias phenomenon perpendicular to the film plane, the samples were subjected to heat treatments and cooled in the presence of an external magnetic field. The samples were magnetically characterized before and after treatment using AGFM and VSM techniques. Some of the as-fabricated samples exhibited perpendicular magnetic anisotropy, and after treatment, all samples showed this anisotropy. We observed a variation in the bias field and coercive field intensity with the temperature of the heat treatment and the thickness of the spacer. Magnetic force microscopy was used to observe the magnetic domain structures present in the films under three different conditions: as-fabricated samples, after magnetically saturating out-of-plane, and after an AC demagnetization protocol. Despite the presence of perpendicular anisotropy and exchange bias in most of the films, only labyrinth and bubble-type structures were observed. It was not possible to confirm the presence of skyrmions or the influence of EB on their formation.
publishDate 2023
dc.date.accessioned.fl_str_mv 2023-05-29T15:34:02Z
dc.date.available.fl_str_mv 2023-05-29T15:34:02Z
dc.date.issued.fl_str_mv 2023-04-26
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
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url http://repositorio.ufsm.br/handle/1/29238
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Centro de Ciências Naturais e Exatas
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dc.publisher.department.fl_str_mv Física
publisher.none.fl_str_mv Universidade Federal de Santa Maria
Centro de Ciências Naturais e Exatas
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