Micronização como alternativa para valorização do bagaço de uva: caracterização e aplicação em snack extrusado

Detalhes bibliográficos
Ano de defesa: 2020
Autor(a) principal: Bender, Ana Betine Beutinger
Orientador(a): Não Informado pela instituição
Banca de defesa: Não Informado pela instituição
Tipo de documento: Tese
Tipo de acesso: Acesso aberto
dARK ID: ark:/26339/0013000010xzt
Idioma: por
Instituição de defesa: Universidade Federal de Santa Maria
Brasil
Ciência e Tecnologia dos Alimentos
UFSM
Programa de Pós-Graduação em Ciência e Tecnologia dos Alimentos
Centro de Ciências Rurais
Programa de Pós-Graduação: Não Informado pela instituição
Departamento: Não Informado pela instituição
País: Não Informado pela instituição
Palavras-chave em Português:
Link de acesso: http://repositorio.ufsm.br/handle/1/20765
Resumo: Grape pomace, the winemaking by-product, is characterized by a significant amount of dietary fiber and phenolic compounds. Most of these compounds are associated with the fibrous matrix. Physical modifications, such as micronization, have been used to modify the functionality of dietary fiber by caused by the breakdown of its polymeric constituents. Because it is underused by the wine industry, there is growing interest in its use. Few studies evaluate the effect of incorporation of micronized ingredients in food products as well as their influence on in vitro digestibility. Therefore, the aim of the present study was to evaluate the effect of micronization on the physicochemical properties of dietary fiber from grape pomace in order to enhance the functional properties of an extruded product. The effects of micronization of grape pomace and its fiber concentrate on dietary fiber fractions, physicochemical properties, phenolic compounds, and antioxidant capacity were evaluated. Factorial design with two independent variables (22) – speed and time – was used to determine the best milling conditions to increase the soluble fiber content. The insoluble fiber constituents, such as cellulose and lignin, were partially degraded and the content decreased after milling, resulting in higher soluble fiber content, which demonstrates the compound redistribution. Micronization had a significant effect on reducing the particle size, as evidenced by scanning electron microscopy. FT-IR spectra revealed changes in typical absorption bands of polysaccharides. After milling, powder solubility increased and water holding, oil and cation binding capacities decreased. Furthermore, micronization enhanced phenolic compound extraction, mainly catechin and epicatechin, and the antioxidant capacity evaluated by ABTS and ORAC assays. The results obtained indicate that micronization modifies the dietary fiber composition of grape pomace, increasing possibilities for use as a functional ingredient in the food industry. In this way grape pomace and micronized grape pomace were added to an extruded product. Physicochemical, technological and sensory characteristics, including phenolic and anthocyanin content, antioxidant capacity, and in vitro starch digestibility, were evaluated. The addition of grape pomace influenced the expansion ration, bulk density, and water absorption and solubility indexes. Regarding the composition, total, insoluble and soluble fiber content increased in fortified formulations. The inclusion of grape pomace and micronized grape pomace increased the total phenolic content, total monomeric anthocyanin and, consequently, the antioxidant capacity (ABTS and ORAC assays). The color and flavor attributes had the highest scores at the sensory analysis. The in vitro starch digestibility showed an increased in resistant starch fraction with addition of grape pomace and micronized grape pomace, which had lower glycemic index. The results demonstrate that the extruded products fortified with grape pomace and micronized grape pomace have interesting technological and functional characteristics, and could be considered as promising ingredients for using in the food industry.
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spelling Micronização como alternativa para valorização do bagaço de uva: caracterização e aplicação em snack extrusadoMicronization as an alternative for valuation of grape pomace: characterization and application in extruded productExtrusãoMoagem ultrafinaResíduo agroindustrialVitiviniculturaExtrusionUltrafine grindingAgro-industrial by-productsVitivinicultureCNPQ::CIENCIAS AGRARIAS::CIENCIA E TECNOLOGIA DE ALIMENTOSGrape pomace, the winemaking by-product, is characterized by a significant amount of dietary fiber and phenolic compounds. Most of these compounds are associated with the fibrous matrix. Physical modifications, such as micronization, have been used to modify the functionality of dietary fiber by caused by the breakdown of its polymeric constituents. Because it is underused by the wine industry, there is growing interest in its use. Few studies evaluate the effect of incorporation of micronized ingredients in food products as well as their influence on in vitro digestibility. Therefore, the aim of the present study was to evaluate the effect of micronization on the physicochemical properties of dietary fiber from grape pomace in order to enhance the functional properties of an extruded product. The effects of micronization of grape pomace and its fiber concentrate on dietary fiber fractions, physicochemical properties, phenolic compounds, and antioxidant capacity were evaluated. Factorial design with two independent variables (22) – speed and time – was used to determine the best milling conditions to increase the soluble fiber content. The insoluble fiber constituents, such as cellulose and lignin, were partially degraded and the content decreased after milling, resulting in higher soluble fiber content, which demonstrates the compound redistribution. Micronization had a significant effect on reducing the particle size, as evidenced by scanning electron microscopy. FT-IR spectra revealed changes in typical absorption bands of polysaccharides. After milling, powder solubility increased and water holding, oil and cation binding capacities decreased. Furthermore, micronization enhanced phenolic compound extraction, mainly catechin and epicatechin, and the antioxidant capacity evaluated by ABTS and ORAC assays. The results obtained indicate that micronization modifies the dietary fiber composition of grape pomace, increasing possibilities for use as a functional ingredient in the food industry. In this way grape pomace and micronized grape pomace were added to an extruded product. Physicochemical, technological and sensory characteristics, including phenolic and anthocyanin content, antioxidant capacity, and in vitro starch digestibility, were evaluated. The addition of grape pomace influenced the expansion ration, bulk density, and water absorption and solubility indexes. Regarding the composition, total, insoluble and soluble fiber content increased in fortified formulations. The inclusion of grape pomace and micronized grape pomace increased the total phenolic content, total monomeric anthocyanin and, consequently, the antioxidant capacity (ABTS and ORAC assays). The color and flavor attributes had the highest scores at the sensory analysis. The in vitro starch digestibility showed an increased in resistant starch fraction with addition of grape pomace and micronized grape pomace, which had lower glycemic index. The results demonstrate that the extruded products fortified with grape pomace and micronized grape pomace have interesting technological and functional characteristics, and could be considered as promising ingredients for using in the food industry.Coordenação de Aperfeiçoamento de Pessoal de Nível Superior - CAPESO bagaço de uva, resíduo da vinificação, caracteriza-se por apresentar quantidade significativa de fibra alimentar e compostos fenólicos. Grande parte destes compostos encontra-se associada à matriz fibrosa. Modificações físicas, como a micronização, vêm sendo utilizadas para alterar a funcionalidade da fibra alimentar, através da quebra de seus constituintes poliméricos. Por tratar-se de material subutilizado pela indústria vinícola, há crescente interesse pelo seu aproveitamento. Poucos estudos avaliam o efeito da incorporação dos ingredientes micronizados em produtos alimentícios bem como a influência destes na digestibilidade in vitro. Diante disto, o objetivo do presente estudo foi avaliar o efeito da micronização sobre as características físico-químicas da fibra do bagaço de uva com o intuito de potencializar as propriedades funcionais de um produto extrusado. Foram avaliados os efeitos da micronização do bagaço de uva e do seu concentrado de fibra nas frações de fibra alimentar, propriedades físico-químicas, compostos fenólicos e capacidade antioxidante. Delineamento fatorial com duas variáveis independentes (22) - rotação e tempo - foi utilizado para determinar as melhores condições de moagem para aumentar o teor de fibra solúvel. Os constituintes da fibra insolúvel, como celulose e lignina, foram degradados parcialmente e os teores diminuíram após a moagem, resultando em maior teor de fibra solúvel, o que demonstra a redistribuição dos compostos. A micronização teve efeito significativo na redução do tamanho de partícula, como evidenciado pela microscopia eletrônica de varredura. Os espectros de FT-IR revelaram alterações nas bandas de absorção típicas de polissacarídeos. Após a moagem, a solubilidade dos pós aumentou e as capacidades de retenção de água, ligação ao óleo e a cátions diminuíram. Além disso, a micronização melhorou a extração de compostos fenólicos, principalmente catequina e epicatequina, e a capacidade antioxidante avaliada pelos métodos ABTS e ORAC. Os resultados obtidos indicam que a micronização modifica a composição da fibra alimentar do bagaço de uva, aumentando as possibilidades de uso como ingrediente funcional na indústria de alimentos. Desta forma, o bagaço de uva e o bagaço de uva micronizado foram adicionados a um produto extrusado. Foram avaliadas as características físico-químicas, tecnológicas e sensoriais, incluindo o conteúdo de fenólicos e antocianinas, a capacidade antioxidante e a digestibilidade do amido in vitro. A adição de bagaço influenciou a taxa de expansão, densidade aparente e os índices de absorção e solubilidade em água. Quanto à composição, o teor de fibra alimentar total, insolúvel e solúvel aumentou nas formulações fortificadas. A inclusão de bagaço de uva e bagaço de uva micronizado aumentou o conteúdo de fenólicos totais, antocianinas monoméricas totais e, consequentemente, a capacidade antioxidante (métodos ABTS e ORAC). Os atributos cor e sabor apresentaram os maiores escores na análise sensorial. A digestibilidade do amido in vitro revelou aumento no teor de amido resistente nas formulações contendo bagaço de uva, que apresentaram menor índice glicêmico. Os resultados demonstram que os produtos extrusados fortificados com bagaço de uva e bagaço de uva micronizado apresentam características tecnológicas e funcionais interessantes e mostram-se como ingredientes promissores para utilização na indústria de alimentos.Universidade Federal de Santa MariaBrasilCiência e Tecnologia dos AlimentosUFSMPrograma de Pós-Graduação em Ciência e Tecnologia dos AlimentosCentro de Ciências RuraisPenna, Neidi Garciahttp://lattes.cnpq.br/8386196315488275Silva, Leila Picolli daFerrigolo, Fernanda Rodrigues GoulartMonteiro, Sabrina SauthierEmanuelli, TatianaBallus, Cristiano AugustoBender, Ana Betine Beutinger2021-05-04T13:21:31Z2021-05-04T13:21:31Z2020-01-20info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/doctoralThesisapplication/pdfhttp://repositorio.ufsm.br/handle/1/20765ark:/26339/0013000010xztporAttribution-NonCommercial-NoDerivatives 4.0 Internationalinfo:eu-repo/semantics/openAccessreponame:Manancial - Repositório Digital da UFSMinstname:Universidade Federal de Santa Maria (UFSM)instacron:UFSM2025-03-10T12:55:57Zoai:repositorio.ufsm.br:1/20765Biblioteca Digital de Teses e Dissertaçõeshttps://repositorio.ufsm.br/PUBhttps://repositorio.ufsm.br/oai/requestatendimento.sib@ufsm.br||tedebc@gmail.com||manancial@ufsm.bropendoar:2025-03-10T12:55:57Manancial - Repositório Digital da UFSM - Universidade Federal de Santa Maria (UFSM)false
dc.title.none.fl_str_mv Micronização como alternativa para valorização do bagaço de uva: caracterização e aplicação em snack extrusado
Micronization as an alternative for valuation of grape pomace: characterization and application in extruded product
title Micronização como alternativa para valorização do bagaço de uva: caracterização e aplicação em snack extrusado
spellingShingle Micronização como alternativa para valorização do bagaço de uva: caracterização e aplicação em snack extrusado
Bender, Ana Betine Beutinger
Extrusão
Moagem ultrafina
Resíduo agroindustrial
Vitivinicultura
Extrusion
Ultrafine grinding
Agro-industrial by-products
Vitiviniculture
CNPQ::CIENCIAS AGRARIAS::CIENCIA E TECNOLOGIA DE ALIMENTOS
title_short Micronização como alternativa para valorização do bagaço de uva: caracterização e aplicação em snack extrusado
title_full Micronização como alternativa para valorização do bagaço de uva: caracterização e aplicação em snack extrusado
title_fullStr Micronização como alternativa para valorização do bagaço de uva: caracterização e aplicação em snack extrusado
title_full_unstemmed Micronização como alternativa para valorização do bagaço de uva: caracterização e aplicação em snack extrusado
title_sort Micronização como alternativa para valorização do bagaço de uva: caracterização e aplicação em snack extrusado
author Bender, Ana Betine Beutinger
author_facet Bender, Ana Betine Beutinger
author_role author
dc.contributor.none.fl_str_mv Penna, Neidi Garcia
http://lattes.cnpq.br/8386196315488275
Silva, Leila Picolli da
Ferrigolo, Fernanda Rodrigues Goulart
Monteiro, Sabrina Sauthier
Emanuelli, Tatiana
Ballus, Cristiano Augusto
dc.contributor.author.fl_str_mv Bender, Ana Betine Beutinger
dc.subject.por.fl_str_mv Extrusão
Moagem ultrafina
Resíduo agroindustrial
Vitivinicultura
Extrusion
Ultrafine grinding
Agro-industrial by-products
Vitiviniculture
CNPQ::CIENCIAS AGRARIAS::CIENCIA E TECNOLOGIA DE ALIMENTOS
topic Extrusão
Moagem ultrafina
Resíduo agroindustrial
Vitivinicultura
Extrusion
Ultrafine grinding
Agro-industrial by-products
Vitiviniculture
CNPQ::CIENCIAS AGRARIAS::CIENCIA E TECNOLOGIA DE ALIMENTOS
description Grape pomace, the winemaking by-product, is characterized by a significant amount of dietary fiber and phenolic compounds. Most of these compounds are associated with the fibrous matrix. Physical modifications, such as micronization, have been used to modify the functionality of dietary fiber by caused by the breakdown of its polymeric constituents. Because it is underused by the wine industry, there is growing interest in its use. Few studies evaluate the effect of incorporation of micronized ingredients in food products as well as their influence on in vitro digestibility. Therefore, the aim of the present study was to evaluate the effect of micronization on the physicochemical properties of dietary fiber from grape pomace in order to enhance the functional properties of an extruded product. The effects of micronization of grape pomace and its fiber concentrate on dietary fiber fractions, physicochemical properties, phenolic compounds, and antioxidant capacity were evaluated. Factorial design with two independent variables (22) – speed and time – was used to determine the best milling conditions to increase the soluble fiber content. The insoluble fiber constituents, such as cellulose and lignin, were partially degraded and the content decreased after milling, resulting in higher soluble fiber content, which demonstrates the compound redistribution. Micronization had a significant effect on reducing the particle size, as evidenced by scanning electron microscopy. FT-IR spectra revealed changes in typical absorption bands of polysaccharides. After milling, powder solubility increased and water holding, oil and cation binding capacities decreased. Furthermore, micronization enhanced phenolic compound extraction, mainly catechin and epicatechin, and the antioxidant capacity evaluated by ABTS and ORAC assays. The results obtained indicate that micronization modifies the dietary fiber composition of grape pomace, increasing possibilities for use as a functional ingredient in the food industry. In this way grape pomace and micronized grape pomace were added to an extruded product. Physicochemical, technological and sensory characteristics, including phenolic and anthocyanin content, antioxidant capacity, and in vitro starch digestibility, were evaluated. The addition of grape pomace influenced the expansion ration, bulk density, and water absorption and solubility indexes. Regarding the composition, total, insoluble and soluble fiber content increased in fortified formulations. The inclusion of grape pomace and micronized grape pomace increased the total phenolic content, total monomeric anthocyanin and, consequently, the antioxidant capacity (ABTS and ORAC assays). The color and flavor attributes had the highest scores at the sensory analysis. The in vitro starch digestibility showed an increased in resistant starch fraction with addition of grape pomace and micronized grape pomace, which had lower glycemic index. The results demonstrate that the extruded products fortified with grape pomace and micronized grape pomace have interesting technological and functional characteristics, and could be considered as promising ingredients for using in the food industry.
publishDate 2020
dc.date.none.fl_str_mv 2020-01-20
2021-05-04T13:21:31Z
2021-05-04T13:21:31Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/doctoralThesis
format doctoralThesis
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://repositorio.ufsm.br/handle/1/20765
dc.identifier.dark.fl_str_mv ark:/26339/0013000010xzt
url http://repositorio.ufsm.br/handle/1/20765
identifier_str_mv ark:/26339/0013000010xzt
dc.language.iso.fl_str_mv por
language por
dc.rights.driver.fl_str_mv Attribution-NonCommercial-NoDerivatives 4.0 International
info:eu-repo/semantics/openAccess
rights_invalid_str_mv Attribution-NonCommercial-NoDerivatives 4.0 International
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.publisher.none.fl_str_mv Universidade Federal de Santa Maria
Brasil
Ciência e Tecnologia dos Alimentos
UFSM
Programa de Pós-Graduação em Ciência e Tecnologia dos Alimentos
Centro de Ciências Rurais
publisher.none.fl_str_mv Universidade Federal de Santa Maria
Brasil
Ciência e Tecnologia dos Alimentos
UFSM
Programa de Pós-Graduação em Ciência e Tecnologia dos Alimentos
Centro de Ciências Rurais
dc.source.none.fl_str_mv reponame:Manancial - Repositório Digital da UFSM
instname:Universidade Federal de Santa Maria (UFSM)
instacron:UFSM
instname_str Universidade Federal de Santa Maria (UFSM)
instacron_str UFSM
institution UFSM
reponame_str Manancial - Repositório Digital da UFSM
collection Manancial - Repositório Digital da UFSM
repository.name.fl_str_mv Manancial - Repositório Digital da UFSM - Universidade Federal de Santa Maria (UFSM)
repository.mail.fl_str_mv atendimento.sib@ufsm.br||tedebc@gmail.com||manancial@ufsm.br
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