Recobrimento biomimético em superfícies de titânio e aço inoxidável austenítico
| Ano de defesa: | 2013 |
|---|---|
| Autor(a) principal: | |
| Orientador(a): | |
| Banca de defesa: | , |
| Tipo de documento: | Dissertação |
| Tipo de acesso: | Acesso aberto |
| Idioma: | por |
| Instituição de defesa: |
Universidade Federal de Alfenas
|
| Programa de Pós-Graduação: |
Programa de Pós-Graduação em Ciência e Engenharia de Materiais
|
| Departamento: |
Instituto de Ciência e Tecnologia
|
| País: |
Brasil
|
| Palavras-chave em Português: | |
| Área do conhecimento CNPq: | |
| Link de acesso: | https://repositorio.unifal-mg.edu.br/handle/123456789/613 |
Resumo: | Titanium and stainless steel are examples of biomaterials widely used in dental and orthopedic implants, due to their characteristics for this application, such as corrosion resistance and excellent biocompatibility. Researches have been performed to obtain a coating in order to improve the adhesion between the bone and implant by modifying the metal surface, allowing for effective regeneration of bone tissue, osseointegration, and accelerating its growth. In this work, studied the effect of coating of biomimetic method on titanium (cp-Ti) and AISI 316L stainless steel, which consists in immersing the substrate in a solution of synthetic SBF (Simulated Body Fluid), composition, pH and temperature similar to blood plasma. The coating on both metals, was effective for obtaining hydroxyapatite, which was confirmed through the techniques of SEM, XRD and infrared. The bioactivity test showed excellent bioactive characteristics through of formation and development of hydroxyapatite on the receiving coating substrates with 1.5 SBF. For the substrates, cp-Ti and 316L austenitic stainless steel that have not received prior treatment or coating, the bioactivity test revealed only the bioactivity of cp-Ti. The polarization curves showed that the uncoated cp-Ti and 316L austenitic stainless steel with coating had better corrosion resistance at temperatures of 25ºC and 36.5°C. The uncoated cp-Ti showed as the most indicated biomaterial for implants, since it showed better bioactive characteristics and corrosion resistance. |
| id |
UNIFAL_83331a693293d5b04bfb0cbcd9c12d0b |
|---|---|
| oai_identifier_str |
oai:repositorio.unifal-mg.edu.br:123456789/613 |
| network_acronym_str |
UNIFAL |
| network_name_str |
Repositório Institucional da Universidade Federal de Alfenas - RiUnifal |
| repository_id_str |
|
| spelling |
Coelho, Mariny Fabiéle Cabralhttp://lattes.cnpq.br/0809795245116090Caraballo, Mirta MirRigo, Eliana Cristina Da SilvaMariano, Neide Aparecidahttp://lattes.cnpq.br/51703488153534582015-07-17T19:37:30Z2013-07-29COELHO, Mariny Fabiéle Cabral. Recobrimento biomimético em superfícies de titânio e aço inoxidável austenítico. 2013. 83 f. Dissertação (Mestrado em Ciência e Engenharia de Materiais) - Universidade Federal de Alfenas, Poços de Caldas, MG, 2013.https://repositorio.unifal-mg.edu.br/handle/123456789/613Titanium and stainless steel are examples of biomaterials widely used in dental and orthopedic implants, due to their characteristics for this application, such as corrosion resistance and excellent biocompatibility. Researches have been performed to obtain a coating in order to improve the adhesion between the bone and implant by modifying the metal surface, allowing for effective regeneration of bone tissue, osseointegration, and accelerating its growth. In this work, studied the effect of coating of biomimetic method on titanium (cp-Ti) and AISI 316L stainless steel, which consists in immersing the substrate in a solution of synthetic SBF (Simulated Body Fluid), composition, pH and temperature similar to blood plasma. The coating on both metals, was effective for obtaining hydroxyapatite, which was confirmed through the techniques of SEM, XRD and infrared. The bioactivity test showed excellent bioactive characteristics through of formation and development of hydroxyapatite on the receiving coating substrates with 1.5 SBF. For the substrates, cp-Ti and 316L austenitic stainless steel that have not received prior treatment or coating, the bioactivity test revealed only the bioactivity of cp-Ti. The polarization curves showed that the uncoated cp-Ti and 316L austenitic stainless steel with coating had better corrosion resistance at temperatures of 25ºC and 36.5°C. The uncoated cp-Ti showed as the most indicated biomaterial for implants, since it showed better bioactive characteristics and corrosion resistance.O titânio e o aço inoxidável são exemplos de biomateriais muito utilizados em implantes dentários e ortopédicos, por apresentarem características para essa aplicação, como resistência à corrosão e excelente biocompatibilidade. Pesquisas vêm sendo realizadas para a obtenção de um recobrimento, visando melhorar a adesão entre o osso e o implante, através da modificação da superfície do metal, permitindo uma eficaz regeneração do tecido ósseo, osseointegração e aceleração do seu crescimento. Neste trabalho, estudou-se o efeito do recobrimento do método biomimético sobre o titânio (Ti c.p.) e o aço inoxidável AISI 316L, que consiste na imersão do substrato, em uma solução sintética de SBF (Simulated Body Fluid), de composição, pH e temperatura semelhantes ao plasma sanguíneo. O recobrimento sobre ambos os metais, mostraram-se eficiente para obtenção de hidroxiapatita, sendo confirmada através das técnicas de MEV, DRX e infravermelho. O ensaio de bioatividade revelou ótimas características bioativas através da formação e desenvolvimento da hidroxiapatita sobre os substratos que receberam o recobrimento com 1,5 SBF. Para os substratos de Ti c.p. e aço inoxidável austenítico 316L que não receberam tratamento prévio ou recobrimento, o ensaio de bioatividade revelou a bioatividade somente do Ti c.p.. As curvas de polarização revelaram que o Ti c.p. sem recobrimento e o aço inoxidável austenítico 316L com recobrimento apresentaram melhores resistência à corrosão para as temperaturas de 25 e 36,5ºC. O titânio sem recobrimento apresentou-se como o biomaterial mais indicado para implantes, já que apresentou melhores características bioativas e resistência à corrosão.application/pdfporUniversidade Federal de AlfenasPrograma de Pós-Graduação em Ciência e Engenharia de MateriaisUNIFAL-MGBrasilInstituto de Ciência e Tecnologiainfo:eu-repo/semantics/openAccesshttp://creativecommons.org/licenses/by-nc-nd/4.0/Aço inoxidávelTitânioHidroxiapatitaENGENHARIA DE MATERIAIS E METALURGICA::METALURGIA FISICARecobrimento biomimético em superfícies de titânio e aço inoxidável austeníticoinfo:eu-repo/semantics/masterThesisinfo:eu-repo/semantics/publishedVersion-42974172594986389316006008134970431419069777reponame:Repositório Institucional da Universidade Federal de Alfenas - RiUnifalinstname:Universidade Federal de Alfenas (UNIFAL)instacron:UNIFALCoelho, Mariny Fabiéle CabralLICENSElicense.txtlicense.txttext/plain; charset=utf-81987https://repositorio.unifal-mg.edu.br/bitstreams/0a33e144-3948-411d-b049-87c15cd53032/download31555718c4fc75849dd08f27935d4f6bMD51CC-LICENSElicense_urllicense_urltext/plain; charset=utf-849https://repositorio.unifal-mg.edu.br/bitstreams/744a4866-2739-4d4d-a5ac-2d19662ea247/download4afdbb8c545fd630ea7db775da747b2fMD52license_textlicense_texttext/html; charset=utf-821326https://repositorio.unifal-mg.edu.br/bitstreams/b44ca8a4-3289-4914-af05-6d6d3ad594d4/download3ece24ca8606da559a21ffc79b7a9f85MD53license_rdflicense_rdfapplication/rdf+xml; charset=utf-823148https://repositorio.unifal-mg.edu.br/bitstreams/4bb5ba15-905a-45f3-8b5b-4604bcc8594d/download9da0b6dfac957114c6a7714714b86306MD54ORIGINALDISSERTAÇÃO Mariny Fabiele Cabral Coelho 2013.pdfDISSERTAÇÃO Mariny Fabiele Cabral Coelho 2013.pdfRecobrimento biomimético em superfícies de titânio e aço inoxidável austenítico application/pdf2314344https://repositorio.unifal-mg.edu.br/bitstreams/4acb0b5b-30b7-4194-aea1-00fe0e7bc57e/download44d8f05e7f10a7600544cead52d23304MD55TEXTDISSERTAÇÃO Mariny Fabiele Cabral Coelho 2013.pdf.txtDISSERTAÇÃO Mariny Fabiele Cabral Coelho 2013.pdf.txtExtracted texttext/plain102959https://repositorio.unifal-mg.edu.br/bitstreams/1f46e907-985e-43ac-ab90-d9434d820642/download3a5b89c72df44fd3264bed57acf69ff1MD510THUMBNAILDISSERTAÇÃO Mariny Fabiele Cabral Coelho 2013.pdf.jpgDISSERTAÇÃO Mariny Fabiele Cabral Coelho 2013.pdf.jpgGenerated Thumbnailimage/jpeg3282https://repositorio.unifal-mg.edu.br/bitstreams/7e938975-513f-48ee-a318-26a4f2343e02/downloadfe0ebdf2b4ac875a6a84dc16313e54baMD59123456789/6132026-01-07 14:32:46.804http://creativecommons.org/licenses/by-nc-nd/4.0/open.accessoai:repositorio.unifal-mg.edu.br:123456789/613https://repositorio.unifal-mg.edu.brRepositório InstitucionalPUBhttps://bdtd.unifal-mg.edu.br:8443/oai/requestrepositorio@unifal-mg.edu.bropendoar:2026-01-07T17:32:46Repositório Institucional da Universidade Federal de Alfenas - RiUnifal - Universidade Federal de Alfenas (UNIFAL)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 |
| dc.title.pt-BR.fl_str_mv |
Recobrimento biomimético em superfícies de titânio e aço inoxidável austenítico |
| title |
Recobrimento biomimético em superfícies de titânio e aço inoxidável austenítico |
| spellingShingle |
Recobrimento biomimético em superfícies de titânio e aço inoxidável austenítico Coelho, Mariny Fabiéle Cabral Aço inoxidável Titânio Hidroxiapatita ENGENHARIA DE MATERIAIS E METALURGICA::METALURGIA FISICA |
| title_short |
Recobrimento biomimético em superfícies de titânio e aço inoxidável austenítico |
| title_full |
Recobrimento biomimético em superfícies de titânio e aço inoxidável austenítico |
| title_fullStr |
Recobrimento biomimético em superfícies de titânio e aço inoxidável austenítico |
| title_full_unstemmed |
Recobrimento biomimético em superfícies de titânio e aço inoxidável austenítico |
| title_sort |
Recobrimento biomimético em superfícies de titânio e aço inoxidável austenítico |
| author |
Coelho, Mariny Fabiéle Cabral |
| author_facet |
Coelho, Mariny Fabiéle Cabral |
| author_role |
author |
| dc.contributor.author.fl_str_mv |
Coelho, Mariny Fabiéle Cabral |
| dc.contributor.advisor1Lattes.fl_str_mv |
http://lattes.cnpq.br/0809795245116090 |
| dc.contributor.referee1.fl_str_mv |
Caraballo, Mirta Mir |
| dc.contributor.referee2.fl_str_mv |
Rigo, Eliana Cristina Da Silva |
| dc.contributor.advisor1.fl_str_mv |
Mariano, Neide Aparecida |
| dc.contributor.authorLattes.fl_str_mv |
http://lattes.cnpq.br/5170348815353458 |
| contributor_str_mv |
Caraballo, Mirta Mir Rigo, Eliana Cristina Da Silva Mariano, Neide Aparecida |
| dc.subject.por.fl_str_mv |
Aço inoxidável Titânio Hidroxiapatita |
| topic |
Aço inoxidável Titânio Hidroxiapatita ENGENHARIA DE MATERIAIS E METALURGICA::METALURGIA FISICA |
| dc.subject.cnpq.fl_str_mv |
ENGENHARIA DE MATERIAIS E METALURGICA::METALURGIA FISICA |
| description |
Titanium and stainless steel are examples of biomaterials widely used in dental and orthopedic implants, due to their characteristics for this application, such as corrosion resistance and excellent biocompatibility. Researches have been performed to obtain a coating in order to improve the adhesion between the bone and implant by modifying the metal surface, allowing for effective regeneration of bone tissue, osseointegration, and accelerating its growth. In this work, studied the effect of coating of biomimetic method on titanium (cp-Ti) and AISI 316L stainless steel, which consists in immersing the substrate in a solution of synthetic SBF (Simulated Body Fluid), composition, pH and temperature similar to blood plasma. The coating on both metals, was effective for obtaining hydroxyapatite, which was confirmed through the techniques of SEM, XRD and infrared. The bioactivity test showed excellent bioactive characteristics through of formation and development of hydroxyapatite on the receiving coating substrates with 1.5 SBF. For the substrates, cp-Ti and 316L austenitic stainless steel that have not received prior treatment or coating, the bioactivity test revealed only the bioactivity of cp-Ti. The polarization curves showed that the uncoated cp-Ti and 316L austenitic stainless steel with coating had better corrosion resistance at temperatures of 25ºC and 36.5°C. The uncoated cp-Ti showed as the most indicated biomaterial for implants, since it showed better bioactive characteristics and corrosion resistance. |
| publishDate |
2013 |
| dc.date.issued.fl_str_mv |
2013-07-29 |
| dc.date.accessioned.fl_str_mv |
2015-07-17T19:37:30Z |
| dc.type.driver.fl_str_mv |
info:eu-repo/semantics/masterThesis |
| dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
| format |
masterThesis |
| status_str |
publishedVersion |
| dc.identifier.citation.fl_str_mv |
COELHO, Mariny Fabiéle Cabral. Recobrimento biomimético em superfícies de titânio e aço inoxidável austenítico. 2013. 83 f. Dissertação (Mestrado em Ciência e Engenharia de Materiais) - Universidade Federal de Alfenas, Poços de Caldas, MG, 2013. |
| dc.identifier.uri.fl_str_mv |
https://repositorio.unifal-mg.edu.br/handle/123456789/613 |
| identifier_str_mv |
COELHO, Mariny Fabiéle Cabral. Recobrimento biomimético em superfícies de titânio e aço inoxidável austenítico. 2013. 83 f. Dissertação (Mestrado em Ciência e Engenharia de Materiais) - Universidade Federal de Alfenas, Poços de Caldas, MG, 2013. |
| url |
https://repositorio.unifal-mg.edu.br/handle/123456789/613 |
| dc.language.iso.fl_str_mv |
por |
| language |
por |
| dc.relation.department.fl_str_mv |
-4297417259498638931 |
| dc.relation.confidence.fl_str_mv |
600 600 |
| dc.relation.cnpq.fl_str_mv |
8134970431419069777 |
| dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess http://creativecommons.org/licenses/by-nc-nd/4.0/ |
| eu_rights_str_mv |
openAccess |
| rights_invalid_str_mv |
http://creativecommons.org/licenses/by-nc-nd/4.0/ |
| dc.format.none.fl_str_mv |
application/pdf |
| dc.publisher.none.fl_str_mv |
Universidade Federal de Alfenas |
| dc.publisher.program.fl_str_mv |
Programa de Pós-Graduação em Ciência e Engenharia de Materiais |
| dc.publisher.initials.fl_str_mv |
UNIFAL-MG |
| dc.publisher.country.fl_str_mv |
Brasil |
| dc.publisher.department.fl_str_mv |
Instituto de Ciência e Tecnologia |
| publisher.none.fl_str_mv |
Universidade Federal de Alfenas |
| dc.source.none.fl_str_mv |
reponame:Repositório Institucional da Universidade Federal de Alfenas - RiUnifal instname:Universidade Federal de Alfenas (UNIFAL) instacron:UNIFAL |
| instname_str |
Universidade Federal de Alfenas (UNIFAL) |
| instacron_str |
UNIFAL |
| institution |
UNIFAL |
| reponame_str |
Repositório Institucional da Universidade Federal de Alfenas - RiUnifal |
| collection |
Repositório Institucional da Universidade Federal de Alfenas - RiUnifal |
| bitstream.url.fl_str_mv |
https://repositorio.unifal-mg.edu.br/bitstreams/0a33e144-3948-411d-b049-87c15cd53032/download https://repositorio.unifal-mg.edu.br/bitstreams/744a4866-2739-4d4d-a5ac-2d19662ea247/download https://repositorio.unifal-mg.edu.br/bitstreams/b44ca8a4-3289-4914-af05-6d6d3ad594d4/download https://repositorio.unifal-mg.edu.br/bitstreams/4bb5ba15-905a-45f3-8b5b-4604bcc8594d/download https://repositorio.unifal-mg.edu.br/bitstreams/4acb0b5b-30b7-4194-aea1-00fe0e7bc57e/download https://repositorio.unifal-mg.edu.br/bitstreams/1f46e907-985e-43ac-ab90-d9434d820642/download https://repositorio.unifal-mg.edu.br/bitstreams/7e938975-513f-48ee-a318-26a4f2343e02/download |
| bitstream.checksum.fl_str_mv |
31555718c4fc75849dd08f27935d4f6b 4afdbb8c545fd630ea7db775da747b2f 3ece24ca8606da559a21ffc79b7a9f85 9da0b6dfac957114c6a7714714b86306 44d8f05e7f10a7600544cead52d23304 3a5b89c72df44fd3264bed57acf69ff1 fe0ebdf2b4ac875a6a84dc16313e54ba |
| bitstream.checksumAlgorithm.fl_str_mv |
MD5 MD5 MD5 MD5 MD5 MD5 MD5 |
| repository.name.fl_str_mv |
Repositório Institucional da Universidade Federal de Alfenas - RiUnifal - Universidade Federal de Alfenas (UNIFAL) |
| repository.mail.fl_str_mv |
repositorio@unifal-mg.edu.br |
| _version_ |
1859830882506899456 |