Remoção de sílica reativa de bauxita por flotação

Detalhes bibliográficos
Ano de defesa: 2023
Autor(a) principal: Silva, Gustavo Victor Batista E lattes
Orientador(a): Horta, Daniela Gomes lattes
Banca de defesa: Bergerman, Maurício Guimarães, Roveri, Carolina Del
Tipo de documento: Dissertação
Tipo de acesso: Acesso aberto
Idioma: por
Instituição de defesa: Universidade Federal de Alfenas
Programa de Pós-Graduação: Programa de Pós-Graduação em Engenharia Química
Departamento: Instituto de Ciência e Tecnologia
País: Brasil
Palavras-chave em Português:
Área do conhecimento CNPq:
Link de acesso: https://repositorio.unifal-mg.edu.br/handle/123456789/2370
Resumo: The objective of this work was to contribute to the development of a strategy of reverse cationic flotation of kaolinite from bauxite using several bauxite samples from Juruti- PA of the Alcoa company. The samples were characterized regarding their chemical composition by determining the content of Usable Aluminum (AA) and Reactive Silica (RS), the mineralogical composition, and the granulometric and granulochemical distributions. Flotation experiments were initially performed for the selection of collectors, depressants and dispersants. Then the most promising reagents were used in flotation tests with the samples with higher amount of fines and RS content. In the most successful conditions, the flotation reduced the RS content from 19.02% in the feed to 6.37%. The most promising reagents were the F-EDA at 200g/t (alkyl etheramine) as kaolinite collector, the corn starch (AMD) at 400g/t as gibbsite depressant, and the NO149 (polyacrylamide) at 200g/t as dispersant at pH > 9.0. The reduction in the solids content improved the flotation of bauxites with large amount of fine particles. Flotation was not efficient to reduce the RS content of the tailing sample. Compared to the physical concentration by hydrocycle that currently occurs in the plant, the concentration by flotation, still in batch, presented twice the mass recovery. The work indicates the possibility of using the flotation technique in the operation of Juruti.
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spelling Silva, Gustavo Victor Batista Ehttp://lattes.cnpq.br/4218339673249160Bergerman, Maurício GuimarãesRoveri, Carolina DelHorta, Daniela Gomeshttp://lattes.cnpq.br/99254739736405742024-01-26T14:33:57Z2023-06-26SILVA, Gustavo Victor Batista e. Remoção de sílica reativa de bauxita por flotação. 2023. 117 f. Dissertação (Mestrado em Engenharia Química) - Universidade Federal de Alfenas, Poços de Caldas, MG, 2023.https://repositorio.unifal-mg.edu.br/handle/123456789/2370The objective of this work was to contribute to the development of a strategy of reverse cationic flotation of kaolinite from bauxite using several bauxite samples from Juruti- PA of the Alcoa company. The samples were characterized regarding their chemical composition by determining the content of Usable Aluminum (AA) and Reactive Silica (RS), the mineralogical composition, and the granulometric and granulochemical distributions. Flotation experiments were initially performed for the selection of collectors, depressants and dispersants. Then the most promising reagents were used in flotation tests with the samples with higher amount of fines and RS content. In the most successful conditions, the flotation reduced the RS content from 19.02% in the feed to 6.37%. The most promising reagents were the F-EDA at 200g/t (alkyl etheramine) as kaolinite collector, the corn starch (AMD) at 400g/t as gibbsite depressant, and the NO149 (polyacrylamide) at 200g/t as dispersant at pH > 9.0. The reduction in the solids content improved the flotation of bauxites with large amount of fine particles. Flotation was not efficient to reduce the RS content of the tailing sample. Compared to the physical concentration by hydrocycle that currently occurs in the plant, the concentration by flotation, still in batch, presented twice the mass recovery. The work indicates the possibility of using the flotation technique in the operation of Juruti.O objetivo do trabalho foi contribuir para o desenvolvimento de uma estratégia de flotação catiônica reversa de caulinita usando diversas amostras de bauxita de Juruti- PA da empresa Alcoa. As amostras foram caracterizadas quanto a sua composição química por meio da determinação dos teores de Alumínio Aproveitável (AA) e Sílica Reativa (SR), da composição mineralógica e das distribuições granulométrica e granuloquímica. Os ensaios de flotação foram realizados, inicialmente, para a seleção de coletores, depressores e dispersantes. Em seguida, os reagentes mais promissores foram empregados em ensaios de flotação com as amostras com maior quantidade de finos e teores de SR. Nas condições mais satisfatórias, a flotação reduziu o teor de SR de 19,02% na alimentação para 6,37%. Os reagentes mais promissores foram o coletor de caulinita F-EDA na dosagem de 200g/t (alquil eteramina), o depressor de gibbsita amido de milho (AMD) na dosagem de 400g/t, e o dispersante NO149 (poliacrilamida) na dosagem de 200g/t em pH > 9,0. A redução da concentração de sólidos aprimorou a flotação de bauxitas com grande quantidade de partículas finas. A flotação não foi eficiente para reduzir o teor de SR da amostra de rejeito. Em comparação à concentração física por hidrociclonagem, que ocorre atualmente na planta, a concentração por flotação, ainda em batelada, apresentou o dobro de recuperação mássica. O trabalho indica a possibilidade de emprego da técnica de flotação na operação de Juruti.Fundação de Amparo à Pesquisa do Estado de Minas Gerais - FAPEMIGapplication/pdfporUniversidade Federal de AlfenasPrograma de Pós-Graduação em Engenharia QuímicaUNIFAL-MGBrasilInstituto de Ciência e Tecnologiainfo:eu-repo/semantics/openAccessBauxita.Beneficiamento.Flotação.Caulinita.Sílica reativa.ENGENHARIAS::ENGENHARIA QUIMICARemoção de sílica reativa de bauxita por flotaçãoinfo:eu-repo/semantics/masterThesisinfo:eu-repo/semantics/publishedVersion-4297417259498638931600600600-1848640261096870878-1527361517405938873reponame:Biblioteca Digital de Teses e Dissertações da UNIFALinstname:Universidade Federal de Alfenas (UNIFAL)instacron:UNIFALSilva, Gustavo Victor Batista EORIGINALDissertacao_Gustavo Victor Batista e Silva_2023_PPGEQ.pdfDissertacao_Gustavo Victor Batista e Silva_2023_PPGEQ.pdfapplication/pdf5919497https://repositorio.unifal-mg.edu.br/bitstreams/acbf19fb-ef80-465d-b29e-d9952376470d/download4b12f8ef0dcbcef11506b775d7c90369MD52LICENSElicense.txtlicense.txttext/plain; charset=utf-81987https://repositorio.unifal-mg.edu.br/bitstreams/bbececd5-e92b-4abf-9299-2645b5f5264a/download31555718c4fc75849dd08f27935d4f6bMD51TEXTDissertacao_Gustavo Victor Batista e Silva_2023_PPGEQ.pdf.txtDissertacao_Gustavo Victor Batista e Silva_2023_PPGEQ.pdf.txtExtracted texttext/plain102836https://repositorio.unifal-mg.edu.br/bitstreams/1e8e2e4b-8315-4b4c-b6f9-e80fa9aba39f/download559a273972265b018b61131319331a20MD55THUMBNAILDissertacao_Gustavo Victor Batista e Silva_2023_PPGEQ.pdf.jpgDissertacao_Gustavo Victor Batista e Silva_2023_PPGEQ.pdf.jpgGenerated Thumbnailimage/jpeg2486https://repositorio.unifal-mg.edu.br/bitstreams/2a6c5439-de1b-45c0-88cf-259558b8e9f5/download14a192742726a4f960d0f6aaeef4a05aMD56123456789/23702025-04-14 09:54:55.29open.accessoai:repositorio.unifal-mg.edu.br:123456789/2370https://repositorio.unifal-mg.edu.brBiblioteca Digital de Teses e DissertaçõesPUBhttps://bdtd.unifal-mg.edu.br:8443/oai/requestbdtd@unifal-mg.edu.br || bdtd@unifal-mg.edu.bropendoar:2025-04-14T12:54:55Biblioteca Digital de Teses e Dissertações da UNIFAL - Universidade Federal de Alfenas (UNIFAL)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
dc.title.pt-BR.fl_str_mv Remoção de sílica reativa de bauxita por flotação
title Remoção de sílica reativa de bauxita por flotação
spellingShingle Remoção de sílica reativa de bauxita por flotação
Silva, Gustavo Victor Batista E
Bauxita.
Beneficiamento.
Flotação.
Caulinita.
Sílica reativa.
ENGENHARIAS::ENGENHARIA QUIMICA
title_short Remoção de sílica reativa de bauxita por flotação
title_full Remoção de sílica reativa de bauxita por flotação
title_fullStr Remoção de sílica reativa de bauxita por flotação
title_full_unstemmed Remoção de sílica reativa de bauxita por flotação
title_sort Remoção de sílica reativa de bauxita por flotação
author Silva, Gustavo Victor Batista E
author_facet Silva, Gustavo Victor Batista E
author_role author
dc.contributor.author.fl_str_mv Silva, Gustavo Victor Batista E
dc.contributor.advisor1Lattes.fl_str_mv http://lattes.cnpq.br/4218339673249160
dc.contributor.referee1.fl_str_mv Bergerman, Maurício Guimarães
dc.contributor.referee2.fl_str_mv Roveri, Carolina Del
dc.contributor.advisor1.fl_str_mv Horta, Daniela Gomes
dc.contributor.authorLattes.fl_str_mv http://lattes.cnpq.br/9925473973640574
contributor_str_mv Bergerman, Maurício Guimarães
Roveri, Carolina Del
Horta, Daniela Gomes
dc.subject.por.fl_str_mv Bauxita.
Beneficiamento.
Flotação.
Caulinita.
Sílica reativa.
topic Bauxita.
Beneficiamento.
Flotação.
Caulinita.
Sílica reativa.
ENGENHARIAS::ENGENHARIA QUIMICA
dc.subject.cnpq.fl_str_mv ENGENHARIAS::ENGENHARIA QUIMICA
description The objective of this work was to contribute to the development of a strategy of reverse cationic flotation of kaolinite from bauxite using several bauxite samples from Juruti- PA of the Alcoa company. The samples were characterized regarding their chemical composition by determining the content of Usable Aluminum (AA) and Reactive Silica (RS), the mineralogical composition, and the granulometric and granulochemical distributions. Flotation experiments were initially performed for the selection of collectors, depressants and dispersants. Then the most promising reagents were used in flotation tests with the samples with higher amount of fines and RS content. In the most successful conditions, the flotation reduced the RS content from 19.02% in the feed to 6.37%. The most promising reagents were the F-EDA at 200g/t (alkyl etheramine) as kaolinite collector, the corn starch (AMD) at 400g/t as gibbsite depressant, and the NO149 (polyacrylamide) at 200g/t as dispersant at pH > 9.0. The reduction in the solids content improved the flotation of bauxites with large amount of fine particles. Flotation was not efficient to reduce the RS content of the tailing sample. Compared to the physical concentration by hydrocycle that currently occurs in the plant, the concentration by flotation, still in batch, presented twice the mass recovery. The work indicates the possibility of using the flotation technique in the operation of Juruti.
publishDate 2023
dc.date.issued.fl_str_mv 2023-06-26
dc.date.accessioned.fl_str_mv 2024-01-26T14:33:57Z
dc.type.driver.fl_str_mv info:eu-repo/semantics/masterThesis
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dc.identifier.citation.fl_str_mv SILVA, Gustavo Victor Batista e. Remoção de sílica reativa de bauxita por flotação. 2023. 117 f. Dissertação (Mestrado em Engenharia Química) - Universidade Federal de Alfenas, Poços de Caldas, MG, 2023.
dc.identifier.uri.fl_str_mv https://repositorio.unifal-mg.edu.br/handle/123456789/2370
identifier_str_mv SILVA, Gustavo Victor Batista e. Remoção de sílica reativa de bauxita por flotação. 2023. 117 f. Dissertação (Mestrado em Engenharia Química) - Universidade Federal de Alfenas, Poços de Caldas, MG, 2023.
url https://repositorio.unifal-mg.edu.br/handle/123456789/2370
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