Validation of the USAT (Universal Simple Aging Test) procedure to simulate the short and long-term aging of Brazilian asphalts
| Ano de defesa: | 2025 |
|---|---|
| Autor(a) principal: | |
| Orientador(a): | |
| Banca de defesa: | |
| Tipo de documento: | Dissertação |
| Tipo de acesso: | Acesso aberto |
| Idioma: | eng |
| Instituição de defesa: |
Biblioteca Digitais de Teses e Dissertações da USP
|
| Programa de Pós-Graduação: |
Não Informado pela instituição
|
| Departamento: |
Não Informado pela instituição
|
| País: |
Não Informado pela instituição
|
| Palavras-chave em Português: | |
| Link de acesso: | https://www.teses.usp.br/teses/disponiveis/18/18143/tde-08102025-152923/ |
Resumo: | The aging of asphalt binders is an inherent phenomenon associated with production, field application, and the service life of pavements, directly impacting their performance. However, the simulation of this aging in laboratories, especially long-term aging, is still uncommon, mainly due to the high cost of the required equipment. In the Brazilian context, this situation is further aggravated by the fact that the current specification does not include rheological performance parameters or long-term aging requirements, which discourages laboratories from adopting more robust evaluation practices. This study aims to enable alternative, more accessible, and practical procedures for simulating binder aging in Brazilian laboratories, without the need for conventional equipment such as the Rolling Thin Film Oven Test (RTFOT) and the Pressure Aging Vessel (PAV). For short-term aging, the Short-Term Universal Simple Aging Test simplified (STUSAT) was evaluated, while for long-term aging, a modified version of the Long-Term Universal Simple Aging Test (LTUSAT) was studied, reducing the procedure time from 40 to 7 hours by applying a higher temperature. Eight asphalt binders were analyzed, and the residues aged using the alternative methods were compared to those aged using the traditional ones. The comparison was based on rheological parameters such as |G*|/ sin δ, upper continuous grade, Performance Grade (PG), Multiple Stress Creep Recovery (MSCR) outputs (including J and percent recovery %R at 3.2 kPa and J<sub<nr,dif ƒ) in addition to mass change for short-term aged residues. On the other hand, for long-term residues the rheological parameters evaluated were creep stiffness S(60), relaxation rate m-value, |G*|. sin δ, complex modulus |G*|, phase angle δ, Glover-Rowe parameter, R-value, and Δ. The results showed a strong correlation between the methods, indicating that both the STUSAT and the modified LTUSAT can reliably reproduce the effects of short- and long-term aging, respectively. Therefore, this study contributes significantly to the implementation of simpler, and more cost-effective protocols, supporting the development of a Brazilian specification based on the Performance Grade system. |
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Validation of the USAT (Universal Simple Aging Test) procedure to simulate the short and long-term aging of Brazilian asphaltsValidação do ensaio universal simplificado de envelhecimento (USAT) para simular os envelhecimentos de curto e de longo prazos de asfaltos brasileirosasphalt bindersBBRBBRDSRDSRenvelhecimento de curto-prazoenvelhecimento de longo-prazoligante asfálticolong-term agingPAVPVAreologiaRTFOTRTFOTshort-term agingUSATUSATThe aging of asphalt binders is an inherent phenomenon associated with production, field application, and the service life of pavements, directly impacting their performance. However, the simulation of this aging in laboratories, especially long-term aging, is still uncommon, mainly due to the high cost of the required equipment. In the Brazilian context, this situation is further aggravated by the fact that the current specification does not include rheological performance parameters or long-term aging requirements, which discourages laboratories from adopting more robust evaluation practices. This study aims to enable alternative, more accessible, and practical procedures for simulating binder aging in Brazilian laboratories, without the need for conventional equipment such as the Rolling Thin Film Oven Test (RTFOT) and the Pressure Aging Vessel (PAV). For short-term aging, the Short-Term Universal Simple Aging Test simplified (STUSAT) was evaluated, while for long-term aging, a modified version of the Long-Term Universal Simple Aging Test (LTUSAT) was studied, reducing the procedure time from 40 to 7 hours by applying a higher temperature. Eight asphalt binders were analyzed, and the residues aged using the alternative methods were compared to those aged using the traditional ones. The comparison was based on rheological parameters such as |G*|/ sin δ, upper continuous grade, Performance Grade (PG), Multiple Stress Creep Recovery (MSCR) outputs (including J and percent recovery %R at 3.2 kPa and J<sub<nr,dif ƒ) in addition to mass change for short-term aged residues. On the other hand, for long-term residues the rheological parameters evaluated were creep stiffness S(60), relaxation rate m-value, |G*|. sin δ, complex modulus |G*|, phase angle δ, Glover-Rowe parameter, R-value, and Δ. The results showed a strong correlation between the methods, indicating that both the STUSAT and the modified LTUSAT can reliably reproduce the effects of short- and long-term aging, respectively. Therefore, this study contributes significantly to the implementation of simpler, and more cost-effective protocols, supporting the development of a Brazilian specification based on the Performance Grade system.O envelhecimento dos ligantes asfálticos é um fenômeno inerente aos processos de produção, aplicação em campo e à própria vida útil do pavimento, impactando diretamente seu de- sempenho. Contudo, a simulação desse envelhecimento em laboratório, especialmente de longo prazo, ainda é pouco praticada, principalmente devido ao alto custo dos equipamentos necessários. No contexto brasileiro, esse cenário se agrava, uma vez que a especificação vigente não contempla parâmetros reológicos de desempenho nem requisitos relacionados ao envel- hecimento de longo prazo, o que desestimula a adoção de práticas de avaliação mais robustas pelos laboratórios. Este trabalho tem como objetivo propor procedimentos alternativos, mais acessíveis e viáveis, para a simulação do envelhecimento de ligantes em laboratórios nacionais, sem a necessidade de equipamentos convencionais, como o Rolling Thin Film Oven Test (RT- FOT) e o Pressure Aging Vessel (PAV). Para o envelhecimento de curto prazo, foi avaliado o método Short-Term Universal Simple Aging Test (STUSAT), enquanto, para o envelhecimento de longo prazo, foi analisada uma versão modificada do Long-Term Universal Simple Aging Test (LTUSAT), com redução do tempo de envelhecimento de 40 para 7 horas, mediante o uso de uma temperatura mais elevada. Foram analisados oito ligantes asfálticos, cujos resíduos envelhecidos pelos métodos alternativos foram comparados àqueles obtidos pelos métodos tradicionais. A análise foi realizada com base em parâmetros reológicos, como |G*|/ sin δ, grau contínuo superior, Performance Grade (PG) e resultados do ensaio Multiple Stress Creep Re- covery (MSCR), incluindo Jnr, recuperação percentual (%R) a 3,2 kPa e Jnr, dif ƒ, além da variação de massa para os resíduos de curto prazo. Para os resíduos envelhecidos a longo prazo, foram avaliados os parâmetros rigidez à fluência S(60), taxa de relaxação (m-value), |G|. sin δ, módulo complexo (G), ângulo de fase (δ), parâmetro Glover-Rowe, R-value e Δ . Os resultados demonstraram forte correlação entre os métodos, indicando que tanto o STUSAT quanto o LTUSAT modificado são capazes de reproduzir os efeitos do envelhecimento de curto e longo prazo, respectivamente. Dessa forma, este estudo contribui significativamente para a imple- mentação de protocolos mais simples, econômicos e robustos, apoiando o desenvolvimento de uma especificação brasileira baseada no conceito de Performance Grade.Biblioteca Digitais de Teses e Dissertações da USPFaxina, Adalberto LeandroCarvalho, Talita de Souza2025-08-01info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/masterThesisapplication/pdfhttps://www.teses.usp.br/teses/disponiveis/18/18143/tde-08102025-152923/reponame:Biblioteca Digital de Teses e Dissertações da USPinstname:Universidade de São Paulo (USP)instacron:USPLiberar o conteúdo para acesso público.info:eu-repo/semantics/openAccesseng2025-10-10T12:53:01Zoai:teses.usp.br:tde-08102025-152923Biblioteca Digital de Teses e Dissertaçõeshttp://www.teses.usp.br/PUBhttp://www.teses.usp.br/cgi-bin/mtd2br.plvirginia@if.usp.br|| atendimento@aguia.usp.br||virginia@if.usp.bropendoar:27212025-10-10T12:53:01Biblioteca Digital de Teses e Dissertações da USP - Universidade de São Paulo (USP)false |
| dc.title.none.fl_str_mv |
Validation of the USAT (Universal Simple Aging Test) procedure to simulate the short and long-term aging of Brazilian asphalts Validação do ensaio universal simplificado de envelhecimento (USAT) para simular os envelhecimentos de curto e de longo prazos de asfaltos brasileiros |
| title |
Validation of the USAT (Universal Simple Aging Test) procedure to simulate the short and long-term aging of Brazilian asphalts |
| spellingShingle |
Validation of the USAT (Universal Simple Aging Test) procedure to simulate the short and long-term aging of Brazilian asphalts Carvalho, Talita de Souza asphalt binders BBR BBR DSR DSR envelhecimento de curto-prazo envelhecimento de longo-prazo ligante asfáltico long-term aging PAV PVA reologia RTFOT RTFOT short-term aging USAT USAT |
| title_short |
Validation of the USAT (Universal Simple Aging Test) procedure to simulate the short and long-term aging of Brazilian asphalts |
| title_full |
Validation of the USAT (Universal Simple Aging Test) procedure to simulate the short and long-term aging of Brazilian asphalts |
| title_fullStr |
Validation of the USAT (Universal Simple Aging Test) procedure to simulate the short and long-term aging of Brazilian asphalts |
| title_full_unstemmed |
Validation of the USAT (Universal Simple Aging Test) procedure to simulate the short and long-term aging of Brazilian asphalts |
| title_sort |
Validation of the USAT (Universal Simple Aging Test) procedure to simulate the short and long-term aging of Brazilian asphalts |
| author |
Carvalho, Talita de Souza |
| author_facet |
Carvalho, Talita de Souza |
| author_role |
author |
| dc.contributor.none.fl_str_mv |
Faxina, Adalberto Leandro |
| dc.contributor.author.fl_str_mv |
Carvalho, Talita de Souza |
| dc.subject.por.fl_str_mv |
asphalt binders BBR BBR DSR DSR envelhecimento de curto-prazo envelhecimento de longo-prazo ligante asfáltico long-term aging PAV PVA reologia RTFOT RTFOT short-term aging USAT USAT |
| topic |
asphalt binders BBR BBR DSR DSR envelhecimento de curto-prazo envelhecimento de longo-prazo ligante asfáltico long-term aging PAV PVA reologia RTFOT RTFOT short-term aging USAT USAT |
| description |
The aging of asphalt binders is an inherent phenomenon associated with production, field application, and the service life of pavements, directly impacting their performance. However, the simulation of this aging in laboratories, especially long-term aging, is still uncommon, mainly due to the high cost of the required equipment. In the Brazilian context, this situation is further aggravated by the fact that the current specification does not include rheological performance parameters or long-term aging requirements, which discourages laboratories from adopting more robust evaluation practices. This study aims to enable alternative, more accessible, and practical procedures for simulating binder aging in Brazilian laboratories, without the need for conventional equipment such as the Rolling Thin Film Oven Test (RTFOT) and the Pressure Aging Vessel (PAV). For short-term aging, the Short-Term Universal Simple Aging Test simplified (STUSAT) was evaluated, while for long-term aging, a modified version of the Long-Term Universal Simple Aging Test (LTUSAT) was studied, reducing the procedure time from 40 to 7 hours by applying a higher temperature. Eight asphalt binders were analyzed, and the residues aged using the alternative methods were compared to those aged using the traditional ones. The comparison was based on rheological parameters such as |G*|/ sin δ, upper continuous grade, Performance Grade (PG), Multiple Stress Creep Recovery (MSCR) outputs (including J and percent recovery %R at 3.2 kPa and J<sub<nr,dif ƒ) in addition to mass change for short-term aged residues. On the other hand, for long-term residues the rheological parameters evaluated were creep stiffness S(60), relaxation rate m-value, |G*|. sin δ, complex modulus |G*|, phase angle δ, Glover-Rowe parameter, R-value, and Δ. The results showed a strong correlation between the methods, indicating that both the STUSAT and the modified LTUSAT can reliably reproduce the effects of short- and long-term aging, respectively. Therefore, this study contributes significantly to the implementation of simpler, and more cost-effective protocols, supporting the development of a Brazilian specification based on the Performance Grade system. |
| publishDate |
2025 |
| dc.date.none.fl_str_mv |
2025-08-01 |
| dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
| dc.type.driver.fl_str_mv |
info:eu-repo/semantics/masterThesis |
| format |
masterThesis |
| status_str |
publishedVersion |
| dc.identifier.uri.fl_str_mv |
https://www.teses.usp.br/teses/disponiveis/18/18143/tde-08102025-152923/ |
| url |
https://www.teses.usp.br/teses/disponiveis/18/18143/tde-08102025-152923/ |
| dc.language.iso.fl_str_mv |
eng |
| language |
eng |
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|
| dc.rights.driver.fl_str_mv |
Liberar o conteúdo para acesso público. info:eu-repo/semantics/openAccess |
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Liberar o conteúdo para acesso público. |
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openAccess |
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application/pdf |
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|
| dc.publisher.none.fl_str_mv |
Biblioteca Digitais de Teses e Dissertações da USP |
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Biblioteca Digitais de Teses e Dissertações da USP |
| dc.source.none.fl_str_mv |
reponame:Biblioteca Digital de Teses e Dissertações da USP instname:Universidade de São Paulo (USP) instacron:USP |
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Universidade de São Paulo (USP) |
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USP |
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USP |
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Biblioteca Digital de Teses e Dissertações da USP |
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Biblioteca Digital de Teses e Dissertações da USP |
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Biblioteca Digital de Teses e Dissertações da USP - Universidade de São Paulo (USP) |
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virginia@if.usp.br|| atendimento@aguia.usp.br||virginia@if.usp.br |
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1848370472198078464 |