Validation of the USAT (Universal Simple Aging Test) procedure to simulate the short and long-term aging of Brazilian asphalts

Detalhes bibliográficos
Ano de defesa: 2025
Autor(a) principal: Carvalho, Talita de Souza
Orientador(a): Não Informado pela instituição
Banca de defesa: Não Informado pela instituição
Tipo de documento: Dissertação
Tipo de acesso: Acesso aberto
Idioma: eng
Instituição de defesa: Biblioteca Digitais de Teses e Dissertações da USP
Programa de Pós-Graduação: Não Informado pela instituição
Departamento: Não Informado pela instituição
País: Não Informado pela instituição
Palavras-chave em Português:
BBR
DSR
PAV
PVA
Link de acesso: https://www.teses.usp.br/teses/disponiveis/18/18143/tde-08102025-152923/
Resumo: The aging of asphalt binders is an inherent phenomenon associated with production, field application, and the service life of pavements, directly impacting their performance. However, the simulation of this aging in laboratories, especially long-term aging, is still uncommon, mainly due to the high cost of the required equipment. In the Brazilian context, this situation is further aggravated by the fact that the current specification does not include rheological performance parameters or long-term aging requirements, which discourages laboratories from adopting more robust evaluation practices. This study aims to enable alternative, more accessible, and practical procedures for simulating binder aging in Brazilian laboratories, without the need for conventional equipment such as the Rolling Thin Film Oven Test (RTFOT) and the Pressure Aging Vessel (PAV). For short-term aging, the Short-Term Universal Simple Aging Test simplified (STUSAT) was evaluated, while for long-term aging, a modified version of the Long-Term Universal Simple Aging Test (LTUSAT) was studied, reducing the procedure time from 40 to 7 hours by applying a higher temperature. Eight asphalt binders were analyzed, and the residues aged using the alternative methods were compared to those aged using the traditional ones. The comparison was based on rheological parameters such as |G*|/ sin &delta;, upper continuous grade, Performance Grade (PG), Multiple Stress Creep Recovery (MSCR) outputs (including J and percent recovery %R at 3.2 kPa and J<sub<nr,dif &fnof;) in addition to mass change for short-term aged residues. On the other hand, for long-term residues the rheological parameters evaluated were creep stiffness S(60), relaxation rate m-value, |G*|. sin &delta;, complex modulus |G*|, phase angle &delta;, Glover-Rowe parameter, R-value, and &Delta;. The results showed a strong correlation between the methods, indicating that both the STUSAT and the modified LTUSAT can reliably reproduce the effects of short- and long-term aging, respectively. Therefore, this study contributes significantly to the implementation of simpler, and more cost-effective protocols, supporting the development of a Brazilian specification based on the Performance Grade system.
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spelling Validation of the USAT (Universal Simple Aging Test) procedure to simulate the short and long-term aging of Brazilian asphaltsValidação do ensaio universal simplificado de envelhecimento (USAT) para simular os envelhecimentos de curto e de longo prazos de asfaltos brasileirosasphalt bindersBBRBBRDSRDSRenvelhecimento de curto-prazoenvelhecimento de longo-prazoligante asfálticolong-term agingPAVPVAreologiaRTFOTRTFOTshort-term agingUSATUSATThe aging of asphalt binders is an inherent phenomenon associated with production, field application, and the service life of pavements, directly impacting their performance. However, the simulation of this aging in laboratories, especially long-term aging, is still uncommon, mainly due to the high cost of the required equipment. In the Brazilian context, this situation is further aggravated by the fact that the current specification does not include rheological performance parameters or long-term aging requirements, which discourages laboratories from adopting more robust evaluation practices. This study aims to enable alternative, more accessible, and practical procedures for simulating binder aging in Brazilian laboratories, without the need for conventional equipment such as the Rolling Thin Film Oven Test (RTFOT) and the Pressure Aging Vessel (PAV). For short-term aging, the Short-Term Universal Simple Aging Test simplified (STUSAT) was evaluated, while for long-term aging, a modified version of the Long-Term Universal Simple Aging Test (LTUSAT) was studied, reducing the procedure time from 40 to 7 hours by applying a higher temperature. Eight asphalt binders were analyzed, and the residues aged using the alternative methods were compared to those aged using the traditional ones. The comparison was based on rheological parameters such as |G*|/ sin &delta;, upper continuous grade, Performance Grade (PG), Multiple Stress Creep Recovery (MSCR) outputs (including J and percent recovery %R at 3.2 kPa and J<sub<nr,dif &fnof;) in addition to mass change for short-term aged residues. On the other hand, for long-term residues the rheological parameters evaluated were creep stiffness S(60), relaxation rate m-value, |G*|. sin &delta;, complex modulus |G*|, phase angle &delta;, Glover-Rowe parameter, R-value, and &Delta;. The results showed a strong correlation between the methods, indicating that both the STUSAT and the modified LTUSAT can reliably reproduce the effects of short- and long-term aging, respectively. Therefore, this study contributes significantly to the implementation of simpler, and more cost-effective protocols, supporting the development of a Brazilian specification based on the Performance Grade system.O envelhecimento dos ligantes asfálticos é um fenômeno inerente aos processos de produção, aplicação em campo e à própria vida útil do pavimento, impactando diretamente seu de- sempenho. Contudo, a simulação desse envelhecimento em laboratório, especialmente de longo prazo, ainda é pouco praticada, principalmente devido ao alto custo dos equipamentos necessários. No contexto brasileiro, esse cenário se agrava, uma vez que a especificação vigente não contempla parâmetros reológicos de desempenho nem requisitos relacionados ao envel- hecimento de longo prazo, o que desestimula a adoção de práticas de avaliação mais robustas pelos laboratórios. Este trabalho tem como objetivo propor procedimentos alternativos, mais acessíveis e viáveis, para a simulação do envelhecimento de ligantes em laboratórios nacionais, sem a necessidade de equipamentos convencionais, como o Rolling Thin Film Oven Test (RT- FOT) e o Pressure Aging Vessel (PAV). Para o envelhecimento de curto prazo, foi avaliado o método Short-Term Universal Simple Aging Test (STUSAT), enquanto, para o envelhecimento de longo prazo, foi analisada uma versão modificada do Long-Term Universal Simple Aging Test (LTUSAT), com redução do tempo de envelhecimento de 40 para 7 horas, mediante o uso de uma temperatura mais elevada. Foram analisados oito ligantes asfálticos, cujos resíduos envelhecidos pelos métodos alternativos foram comparados àqueles obtidos pelos métodos tradicionais. A análise foi realizada com base em parâmetros reológicos, como |G*|/ sin &delta;, grau contínuo superior, Performance Grade (PG) e resultados do ensaio Multiple Stress Creep Re- covery (MSCR), incluindo Jnr, recuperação percentual (%R) a 3,2 kPa e Jnr, dif &fnof;, além da variação de massa para os resíduos de curto prazo. Para os resíduos envelhecidos a longo prazo, foram avaliados os parâmetros rigidez à fluência S(60), taxa de relaxação (m-value), |G|. sin &delta;, módulo complexo (G), ângulo de fase (&delta;), parâmetro Glover-Rowe, R-value e &Delta; . Os resultados demonstraram forte correlação entre os métodos, indicando que tanto o STUSAT quanto o LTUSAT modificado são capazes de reproduzir os efeitos do envelhecimento de curto e longo prazo, respectivamente. Dessa forma, este estudo contribui significativamente para a imple- mentação de protocolos mais simples, econômicos e robustos, apoiando o desenvolvimento de uma especificação brasileira baseada no conceito de Performance Grade.Biblioteca Digitais de Teses e Dissertações da USPFaxina, Adalberto LeandroCarvalho, Talita de Souza2025-08-01info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/masterThesisapplication/pdfhttps://www.teses.usp.br/teses/disponiveis/18/18143/tde-08102025-152923/reponame:Biblioteca Digital de Teses e Dissertações da USPinstname:Universidade de São Paulo (USP)instacron:USPLiberar o conteúdo para acesso público.info:eu-repo/semantics/openAccesseng2025-10-10T12:53:01Zoai:teses.usp.br:tde-08102025-152923Biblioteca Digital de Teses e Dissertaçõeshttp://www.teses.usp.br/PUBhttp://www.teses.usp.br/cgi-bin/mtd2br.plvirginia@if.usp.br|| atendimento@aguia.usp.br||virginia@if.usp.bropendoar:27212025-10-10T12:53:01Biblioteca Digital de Teses e Dissertações da USP - Universidade de São Paulo (USP)false
dc.title.none.fl_str_mv Validation of the USAT (Universal Simple Aging Test) procedure to simulate the short and long-term aging of Brazilian asphalts
Validação do ensaio universal simplificado de envelhecimento (USAT) para simular os envelhecimentos de curto e de longo prazos de asfaltos brasileiros
title Validation of the USAT (Universal Simple Aging Test) procedure to simulate the short and long-term aging of Brazilian asphalts
spellingShingle Validation of the USAT (Universal Simple Aging Test) procedure to simulate the short and long-term aging of Brazilian asphalts
Carvalho, Talita de Souza
asphalt binders
BBR
BBR
DSR
DSR
envelhecimento de curto-prazo
envelhecimento de longo-prazo
ligante asfáltico
long-term aging
PAV
PVA
reologia
RTFOT
RTFOT
short-term aging
USAT
USAT
title_short Validation of the USAT (Universal Simple Aging Test) procedure to simulate the short and long-term aging of Brazilian asphalts
title_full Validation of the USAT (Universal Simple Aging Test) procedure to simulate the short and long-term aging of Brazilian asphalts
title_fullStr Validation of the USAT (Universal Simple Aging Test) procedure to simulate the short and long-term aging of Brazilian asphalts
title_full_unstemmed Validation of the USAT (Universal Simple Aging Test) procedure to simulate the short and long-term aging of Brazilian asphalts
title_sort Validation of the USAT (Universal Simple Aging Test) procedure to simulate the short and long-term aging of Brazilian asphalts
author Carvalho, Talita de Souza
author_facet Carvalho, Talita de Souza
author_role author
dc.contributor.none.fl_str_mv Faxina, Adalberto Leandro
dc.contributor.author.fl_str_mv Carvalho, Talita de Souza
dc.subject.por.fl_str_mv asphalt binders
BBR
BBR
DSR
DSR
envelhecimento de curto-prazo
envelhecimento de longo-prazo
ligante asfáltico
long-term aging
PAV
PVA
reologia
RTFOT
RTFOT
short-term aging
USAT
USAT
topic asphalt binders
BBR
BBR
DSR
DSR
envelhecimento de curto-prazo
envelhecimento de longo-prazo
ligante asfáltico
long-term aging
PAV
PVA
reologia
RTFOT
RTFOT
short-term aging
USAT
USAT
description The aging of asphalt binders is an inherent phenomenon associated with production, field application, and the service life of pavements, directly impacting their performance. However, the simulation of this aging in laboratories, especially long-term aging, is still uncommon, mainly due to the high cost of the required equipment. In the Brazilian context, this situation is further aggravated by the fact that the current specification does not include rheological performance parameters or long-term aging requirements, which discourages laboratories from adopting more robust evaluation practices. This study aims to enable alternative, more accessible, and practical procedures for simulating binder aging in Brazilian laboratories, without the need for conventional equipment such as the Rolling Thin Film Oven Test (RTFOT) and the Pressure Aging Vessel (PAV). For short-term aging, the Short-Term Universal Simple Aging Test simplified (STUSAT) was evaluated, while for long-term aging, a modified version of the Long-Term Universal Simple Aging Test (LTUSAT) was studied, reducing the procedure time from 40 to 7 hours by applying a higher temperature. Eight asphalt binders were analyzed, and the residues aged using the alternative methods were compared to those aged using the traditional ones. The comparison was based on rheological parameters such as |G*|/ sin &delta;, upper continuous grade, Performance Grade (PG), Multiple Stress Creep Recovery (MSCR) outputs (including J and percent recovery %R at 3.2 kPa and J<sub<nr,dif &fnof;) in addition to mass change for short-term aged residues. On the other hand, for long-term residues the rheological parameters evaluated were creep stiffness S(60), relaxation rate m-value, |G*|. sin &delta;, complex modulus |G*|, phase angle &delta;, Glover-Rowe parameter, R-value, and &Delta;. The results showed a strong correlation between the methods, indicating that both the STUSAT and the modified LTUSAT can reliably reproduce the effects of short- and long-term aging, respectively. Therefore, this study contributes significantly to the implementation of simpler, and more cost-effective protocols, supporting the development of a Brazilian specification based on the Performance Grade system.
publishDate 2025
dc.date.none.fl_str_mv 2025-08-01
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/masterThesis
format masterThesis
status_str publishedVersion
dc.identifier.uri.fl_str_mv https://www.teses.usp.br/teses/disponiveis/18/18143/tde-08102025-152923/
url https://www.teses.usp.br/teses/disponiveis/18/18143/tde-08102025-152923/
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv
dc.rights.driver.fl_str_mv Liberar o conteúdo para acesso público.
info:eu-repo/semantics/openAccess
rights_invalid_str_mv Liberar o conteúdo para acesso público.
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.coverage.none.fl_str_mv
dc.publisher.none.fl_str_mv Biblioteca Digitais de Teses e Dissertações da USP
publisher.none.fl_str_mv Biblioteca Digitais de Teses e Dissertações da USP
dc.source.none.fl_str_mv
reponame:Biblioteca Digital de Teses e Dissertações da USP
instname:Universidade de São Paulo (USP)
instacron:USP
instname_str Universidade de São Paulo (USP)
instacron_str USP
institution USP
reponame_str Biblioteca Digital de Teses e Dissertações da USP
collection Biblioteca Digital de Teses e Dissertações da USP
repository.name.fl_str_mv Biblioteca Digital de Teses e Dissertações da USP - Universidade de São Paulo (USP)
repository.mail.fl_str_mv virginia@if.usp.br|| atendimento@aguia.usp.br||virginia@if.usp.br
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