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Influência da maltodextrina nas propriedades e na microestrutura da polpa de coco verde em pó

Detalhes bibliográficos
Ano de defesa: 2019
Autor(a) principal: Araújo, Tayla Maria Ramos
Orientador(a): Afonso, Marcos Rodrigues Amorim
Banca de defesa: Não Informado pela instituição
Tipo de documento: Dissertação
Tipo de acesso: Acesso aberto
Idioma: por
Instituição de defesa: Não Informado pela instituição
Programa de Pós-Graduação: Não Informado pela instituição
Departamento: Não Informado pela instituição
País: Não Informado pela instituição
Palavras-chave em Português:
Link de acesso: http://www.repositorio.ufc.br/handle/riufc/48338
Resumo: This research aimed to evaluate the influence of maltodextrin on the properties and microstructure of green coconut pulp powder obtained by lyophilization. The physicochemical characteristics of the pulp used were determined. The best drying condition was chosen by means of a complete experimental design (DCCR), varying freeze-drying time and maltodextrin concentration and the influence of these variables on humidity, hygroscopicity, solubility and color parameters ( L *, a *, b *) of the powders. The powder in the best condition was physically and chemically characterized and its stability was analyzed for 90 days. In order to evaluate the influence of maltodextrin, powders containing 5.8 to 18% maltodextrin were evaluated by scanning electron microscopy, X-ray diffraction, flow indices, apparent densities, wall friction angles and isotherms sorption. The best condition obtained was 24.7 h of lyophilization and 11.9% maltodextrin concentration (m/m). The study of coconut pulp powder stability allowed to observe the increase of humidity, hygroscopicity and b * coordinate, decrease of L * and a * coordinates and solubility. For the adsorption isotherms of powders, the best fit model was the BET model with estimated average errors below 3.5%. The results of the flow index analyzes indicated that all evaluated coconut pulp powders were cohesive, although the 18% maltodextrin powder had a lower friction angle with the wall and higher apparent density. Scanning electron microscopy showed that the powders had irregular shapes, and as the concentration of the adjuvant increased, the surfaces became smoother and less crowded. In X-ray diffraction, the completely amorphous structure of these powders was demonstrated. It can be concluded that the addition of maltodextrin up to 18% improves all characteristics of the powder studied, but the powder with 11.9% adjuvant is still considered better because it does not need more maltodextrin and is largely satisfactory in maintenance and/or improvement of the characteristics studied.
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spelling Araújo, Tayla Maria RamosEça, Kaliana SitonioAfonso, Marcos Rodrigues Amorim2019-12-11T15:36:12Z2019-12-11T15:36:12Z2019ARAÚJO, Tayla Maria Ramos. Influência da maltodextrina nas propriedades e na microestrutura da polpa de coco verde em pó. 2019. 94 f. Dissertação (Mestrado em Ciência e Tecnologia de Alimentos) - Universidade Federal do Ceará, Fortaleza, 2019.http://www.repositorio.ufc.br/handle/riufc/48338This research aimed to evaluate the influence of maltodextrin on the properties and microstructure of green coconut pulp powder obtained by lyophilization. The physicochemical characteristics of the pulp used were determined. The best drying condition was chosen by means of a complete experimental design (DCCR), varying freeze-drying time and maltodextrin concentration and the influence of these variables on humidity, hygroscopicity, solubility and color parameters ( L *, a *, b *) of the powders. The powder in the best condition was physically and chemically characterized and its stability was analyzed for 90 days. In order to evaluate the influence of maltodextrin, powders containing 5.8 to 18% maltodextrin were evaluated by scanning electron microscopy, X-ray diffraction, flow indices, apparent densities, wall friction angles and isotherms sorption. The best condition obtained was 24.7 h of lyophilization and 11.9% maltodextrin concentration (m/m). The study of coconut pulp powder stability allowed to observe the increase of humidity, hygroscopicity and b * coordinate, decrease of L * and a * coordinates and solubility. For the adsorption isotherms of powders, the best fit model was the BET model with estimated average errors below 3.5%. The results of the flow index analyzes indicated that all evaluated coconut pulp powders were cohesive, although the 18% maltodextrin powder had a lower friction angle with the wall and higher apparent density. Scanning electron microscopy showed that the powders had irregular shapes, and as the concentration of the adjuvant increased, the surfaces became smoother and less crowded. In X-ray diffraction, the completely amorphous structure of these powders was demonstrated. It can be concluded that the addition of maltodextrin up to 18% improves all characteristics of the powder studied, but the powder with 11.9% adjuvant is still considered better because it does not need more maltodextrin and is largely satisfactory in maintenance and/or improvement of the characteristics studied.Esta pesquisa teve como objetivo avaliar a influência da maltodextrina nas propriedades e na microestrutura do pó da polpa de coco verde obtido por liofilização. As características físico-químicas da polpa utilizada foram determinadas. A melhor condição de secagem foi escolhida por meio de um planejamento experimental completo (DCCR), variando-se tempo de liofilização e a concentração de maltodextrina e verificou-se a influência dessas variáveis sobre a umidade, higroscopicidade, solubilidade e os parâmetros de cor (L*, a*, b*) dos pós. O pó na melhor condição foi caracterizado físico-quimicamente e sua estabilidade foi analisada por 90 dias. A fim de avaliar a influência da maltodextrina, pós contendo de 5,8 a 18% de maltodextrina foram avaliados através de microscopia eletrônica de varredura, difração de raios-X, índices de fluxo, densidades aparentes, ângulos de fricção com a parede e isotermas de sorção. A melhor condição obtida foi com 24,7 h de liofilização e 11,9% de concentração de maltodextrina (m/m). O estudo da estabilidade do pó da polpa de coco permitiu observar o aumento da umidade, higroscopicidade e da coordenada b*, a diminuição das coordenadas L* e a* e da solubilidade. Para as isotermas de adsorção dos pós, o modelo de melhor ajuste foi o de BET com erros médios estimados abaixo de 3,5%. Os resultados das análises dos índices de fluxo indicaram que todos os pós de polpa coco avaliados se apresentaram coesos, embora o pó com 18% de maltodextrina tenha obtido um menor ângulo de atrito com a parede e maior densidade aparente. Na microscopia eletrônica de varredura verificou-se que os pós tinham formatos irregulares, e a medida em que a concentração do adjuvante aumentava, as superfícies se tornavam mais lisas e menos aglomeradas. Já na difração de raios-X, demonstrou-se a estrutura completamente amorfa desses pós. Pode-se concluir que a adição da maltodextrina até 18% melhora todas as características estudadas do pó, porém o pó com 11,9% de adjuvante ainda é considerado melhor, por não precisar de maior quantidade de maltodextrina e se apresentar amplamente satisfatório na manutenção e/ou melhoria das características estudadas.DesidrataçãoLiofilizaçãoMaltodextrinaCoco verdeInfluência da maltodextrina nas propriedades e na microestrutura da polpa de coco verde em póInfluence of maltodextrin on the properties and microstructure of green coconut powder pulpinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/masterThesisporreponame:Repositório Institucional da Universidade Federal do Ceará (UFC)instname:Universidade Federal do Ceará (UFC)instacron:UFCinfo:eu-repo/semantics/openAccessORIGINAL2019_dis_tmraraujo.pdf2019_dis_tmraraujo.pdfapplication/pdf2121041http://repositorio.ufc.br/bitstream/riufc/48338/3/2019_dis_tmraraujo.pdfcdcb45ebb9849bc889ce853c535095d4MD53LICENSElicense.txtlicense.txttext/plain; charset=utf-81748http://repositorio.ufc.br/bitstream/riufc/48338/4/license.txt8a4605be74aa9ea9d79846c1fba20a33MD54riufc/483382020-04-28 15:06:30.163oai:repositorio.ufc.br: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Repositório InstitucionalPUBhttp://www.repositorio.ufc.br/ri-oai/requestbu@ufc.br || repositorio@ufc.bropendoar:2020-04-28T18:06:30Repositório Institucional da Universidade Federal do Ceará (UFC) - Universidade Federal do Ceará (UFC)false
dc.title.pt_BR.fl_str_mv Influência da maltodextrina nas propriedades e na microestrutura da polpa de coco verde em pó
dc.title.en.pt_BR.fl_str_mv Influence of maltodextrin on the properties and microstructure of green coconut powder pulp
title Influência da maltodextrina nas propriedades e na microestrutura da polpa de coco verde em pó
spellingShingle Influência da maltodextrina nas propriedades e na microestrutura da polpa de coco verde em pó
Araújo, Tayla Maria Ramos
Desidratação
Liofilização
Maltodextrina
Coco verde
title_short Influência da maltodextrina nas propriedades e na microestrutura da polpa de coco verde em pó
title_full Influência da maltodextrina nas propriedades e na microestrutura da polpa de coco verde em pó
title_fullStr Influência da maltodextrina nas propriedades e na microestrutura da polpa de coco verde em pó
title_full_unstemmed Influência da maltodextrina nas propriedades e na microestrutura da polpa de coco verde em pó
title_sort Influência da maltodextrina nas propriedades e na microestrutura da polpa de coco verde em pó
author Araújo, Tayla Maria Ramos
author_facet Araújo, Tayla Maria Ramos
author_role author
dc.contributor.co-advisor.none.fl_str_mv Eça, Kaliana Sitonio
dc.contributor.author.fl_str_mv Araújo, Tayla Maria Ramos
dc.contributor.advisor1.fl_str_mv Afonso, Marcos Rodrigues Amorim
contributor_str_mv Afonso, Marcos Rodrigues Amorim
dc.subject.por.fl_str_mv Desidratação
Liofilização
Maltodextrina
Coco verde
topic Desidratação
Liofilização
Maltodextrina
Coco verde
description This research aimed to evaluate the influence of maltodextrin on the properties and microstructure of green coconut pulp powder obtained by lyophilization. The physicochemical characteristics of the pulp used were determined. The best drying condition was chosen by means of a complete experimental design (DCCR), varying freeze-drying time and maltodextrin concentration and the influence of these variables on humidity, hygroscopicity, solubility and color parameters ( L *, a *, b *) of the powders. The powder in the best condition was physically and chemically characterized and its stability was analyzed for 90 days. In order to evaluate the influence of maltodextrin, powders containing 5.8 to 18% maltodextrin were evaluated by scanning electron microscopy, X-ray diffraction, flow indices, apparent densities, wall friction angles and isotherms sorption. The best condition obtained was 24.7 h of lyophilization and 11.9% maltodextrin concentration (m/m). The study of coconut pulp powder stability allowed to observe the increase of humidity, hygroscopicity and b * coordinate, decrease of L * and a * coordinates and solubility. For the adsorption isotherms of powders, the best fit model was the BET model with estimated average errors below 3.5%. The results of the flow index analyzes indicated that all evaluated coconut pulp powders were cohesive, although the 18% maltodextrin powder had a lower friction angle with the wall and higher apparent density. Scanning electron microscopy showed that the powders had irregular shapes, and as the concentration of the adjuvant increased, the surfaces became smoother and less crowded. In X-ray diffraction, the completely amorphous structure of these powders was demonstrated. It can be concluded that the addition of maltodextrin up to 18% improves all characteristics of the powder studied, but the powder with 11.9% adjuvant is still considered better because it does not need more maltodextrin and is largely satisfactory in maintenance and/or improvement of the characteristics studied.
publishDate 2019
dc.date.accessioned.fl_str_mv 2019-12-11T15:36:12Z
dc.date.available.fl_str_mv 2019-12-11T15:36:12Z
dc.date.issued.fl_str_mv 2019
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/masterThesis
format masterThesis
status_str publishedVersion
dc.identifier.citation.fl_str_mv ARAÚJO, Tayla Maria Ramos. Influência da maltodextrina nas propriedades e na microestrutura da polpa de coco verde em pó. 2019. 94 f. Dissertação (Mestrado em Ciência e Tecnologia de Alimentos) - Universidade Federal do Ceará, Fortaleza, 2019.
dc.identifier.uri.fl_str_mv http://www.repositorio.ufc.br/handle/riufc/48338
identifier_str_mv ARAÚJO, Tayla Maria Ramos. Influência da maltodextrina nas propriedades e na microestrutura da polpa de coco verde em pó. 2019. 94 f. Dissertação (Mestrado em Ciência e Tecnologia de Alimentos) - Universidade Federal do Ceará, Fortaleza, 2019.
url http://www.repositorio.ufc.br/handle/riufc/48338
dc.language.iso.fl_str_mv por
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dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
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dc.source.none.fl_str_mv reponame:Repositório Institucional da Universidade Federal do Ceará (UFC)
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