Revestimentos comestíveis a base de quitosana e extrato de alecrim (rosmarinus officinalis l.) e sua aplicabilidade na carne bovina

Detalhes bibliográficos
Ano de defesa: 2019
Autor(a) principal: Lima, Allison Ferreira de
Orientador(a): Não Informado pela instituição
Banca de defesa: Não Informado pela instituição
Tipo de documento: Dissertação
Tipo de acesso: Acesso aberto
Idioma: por
Instituição de defesa: Universidade Federal Rural do Semi-Árido
Brasil
Centro de Ciências Agrárias - CCA
UFERSA
Programa de Pós-Graduação em Ciência Animal
Programa de Pós-Graduação: Não Informado pela instituição
Departamento: Não Informado pela instituição
País: Não Informado pela instituição
Palavras-chave em Português:
Link de acesso: https://doi.org/10.21708/bdtd.ppgca.dissertacao.978
https://repositorio.ufersa.edu.br/handle/prefix/978
Resumo: The objective of the research was to elaborate and evaluate edible coatings based on chitosan and rosemary extract (Rosmarinus officinalis L.) and its applicability on beef. At the beginning, the preparation of rosemary extracts at concentrations of 4% and 8%, as well as preparation of the polymer mixture and consequent immersion of the meat in this content and in distilled water (control) for the physical analyzes (pH, (coliforms at 45 ° C and the shelf life of mesophiles, psychrotrophs, Staphylococcus ssp. and detection of Salmonella spp.) and antioxidant activity (TBARS). The mechanical properties, water vapor permeability (PVA), color, transparency, solubility and moisture absorption of the films were evaluated. The results of the physical analyzes show that there was a significant effect (p <0.05) between coatings types and shelf life for pH and all color parameters studied (L, a * and b *). The highest water retention capacity occurred at the concentration of 8% of the extract. Among the treatments on weight loss in cooking, these results relate to polymer blends. The shear force also showed a difference between the treatments and the times, all the samples had a decrease in the shear force over time. In the microbiological analyzes, the absence of Salmonella spp. in 25 g of sample. As for coliforms at 45º C, values of 1100 NMP / g were found both in the treated samples and in the control at time 0 (single evaluation day). The count of aerobic mesophilic microorganisms differed significantly (p <0.05) in the coatings where the rosemary extracts were included in the other treatments, showing a tendency to reduce these microorganisms, as well as in psychrotrophic microorganisms. It was observed immediate action of the coatings against the propagation of Staphylococcus spp., Where the samples did not present statistical difference (p> 0.05) between the treatments from day 2. The coatings where there was the inclusion of rosemary extracts, demonstrated significant antioxidant capacity between treatments and over the evaluation times. Concerning the films, thickness variation was observed, however, there was no significant difference (p> 0.05) between these values. As for solubility, there was no significant difference (p> 0.05) between treatments. The moisture absorption varied significantly (p <0.05) between the control treatment and those treated with the extracts. In the PVA evaluation, there was a significant difference (p <0.05) between the control treatments and with 8% of extract, 0.41 and 0.70 g.mm/h.m².kPa, respectively, avoiding the deterioration process in food. In relation to the mechanical tests, the control requires less tension than the samples with extracts, to undergo deformation, however, there is no statistical difference (p> 0.05). Regarding the force required to break the test specimen, it was observed that the control film is more resistant than films with extracts, presenting a statistical difference (p <0.05). Thus, it was concluded that the coatings based on chitosan and rosemary extract (Rosmarinus officinalis L.) had an influence on the conservation and quality of refrigerated beef, and the coating with the lowest extract concentration (4%) was the most indicated, because it has the lowest cost of production, keeping the meat as close to the natural one
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spelling Revestimentos comestíveis a base de quitosana e extrato de alecrim (rosmarinus officinalis l.) e sua aplicabilidade na carne bovinaCoberturaConservaçãoQualidade da carneTecnologia de alimentosVida útilConservationFood technologyMeat qualityRoofShelf lifeCNPQ::CIENCIAS AGRARIAS::MEDICINA VETERINARIAThe objective of the research was to elaborate and evaluate edible coatings based on chitosan and rosemary extract (Rosmarinus officinalis L.) and its applicability on beef. At the beginning, the preparation of rosemary extracts at concentrations of 4% and 8%, as well as preparation of the polymer mixture and consequent immersion of the meat in this content and in distilled water (control) for the physical analyzes (pH, (coliforms at 45 ° C and the shelf life of mesophiles, psychrotrophs, Staphylococcus ssp. and detection of Salmonella spp.) and antioxidant activity (TBARS). The mechanical properties, water vapor permeability (PVA), color, transparency, solubility and moisture absorption of the films were evaluated. The results of the physical analyzes show that there was a significant effect (p <0.05) between coatings types and shelf life for pH and all color parameters studied (L, a * and b *). The highest water retention capacity occurred at the concentration of 8% of the extract. Among the treatments on weight loss in cooking, these results relate to polymer blends. The shear force also showed a difference between the treatments and the times, all the samples had a decrease in the shear force over time. In the microbiological analyzes, the absence of Salmonella spp. in 25 g of sample. As for coliforms at 45º C, values of 1100 NMP / g were found both in the treated samples and in the control at time 0 (single evaluation day). The count of aerobic mesophilic microorganisms differed significantly (p <0.05) in the coatings where the rosemary extracts were included in the other treatments, showing a tendency to reduce these microorganisms, as well as in psychrotrophic microorganisms. It was observed immediate action of the coatings against the propagation of Staphylococcus spp., Where the samples did not present statistical difference (p> 0.05) between the treatments from day 2. The coatings where there was the inclusion of rosemary extracts, demonstrated significant antioxidant capacity between treatments and over the evaluation times. Concerning the films, thickness variation was observed, however, there was no significant difference (p> 0.05) between these values. As for solubility, there was no significant difference (p> 0.05) between treatments. The moisture absorption varied significantly (p <0.05) between the control treatment and those treated with the extracts. In the PVA evaluation, there was a significant difference (p <0.05) between the control treatments and with 8% of extract, 0.41 and 0.70 g.mm/h.m².kPa, respectively, avoiding the deterioration process in food. In relation to the mechanical tests, the control requires less tension than the samples with extracts, to undergo deformation, however, there is no statistical difference (p> 0.05). Regarding the force required to break the test specimen, it was observed that the control film is more resistant than films with extracts, presenting a statistical difference (p <0.05). Thus, it was concluded that the coatings based on chitosan and rosemary extract (Rosmarinus officinalis L.) had an influence on the conservation and quality of refrigerated beef, and the coating with the lowest extract concentration (4%) was the most indicated, because it has the lowest cost of production, keeping the meat as close to the natural oneO objetivo da pesquisa foi elaborar e avaliar revestimentos comestíveis a base de quitosana e extrato de alecrim (Rosmarinus officinalis L.) e sua aplicabilidade na carne bovina. A princípio o estudo contou com a preparação dos extratos de alecrim nas concentrações de 4% e 8%, além do preparo da mistura polimérica e, consequente imersão da carne nesse conteúdo e em água destilada (controle) para as análises: físicas (pH, cor, capacidade de retenção de água, perda de peso na cocção e força de cisalhamento), microbiológicas (coliformes a 45°C e o tempo de prateleira de mesófilos, psicrotróficos, Staphylococcus ssp. e detecção de Salmonella spp.) e atividade antioxidante (TBARS). Avaliou-se as propriedades mecânicas, permeabilidade ao vapor de água (PVA), cor, transparência, solubilidade e absorção de umidade dos filmes. Os resultados das análises físicas, demonstram que houve efeito significativo (p<0,05) entre os tipos de revestimentos e tempo de prateleira para pH e todos os parâmetros de cor estudados (L, a* e b*). A capacidade de retenção de água mais elevada, ocorreu na concentração de 8% do extrato. Entre os tratamentos na perda de peso na cocção, relacionado esses resultados as misturas poliméricas. A força de cisalhamento também apresentou diferença entre os tratamentos e os tempos, todas as amostras tiveram uma diminuição na força de cisalhamento ao longo do tempo. Nas análises microbiológicas, verificou-se a conformidade da ausência de Salmonella spp. em 25g de amostra. Quanto a coliformes a 45º C, foram encontrados valores de 1100 NMP/ g tanto nas amostras tratadas, como no controle no tempo 0 (único dia de avaliação). A contagem de microrganismos aeróbios mesófilos diferiu significativamente (p<0,05) nos revestimentos onde havia a inclusão dos extratos de alecrim, dos demais tratamentos, apresentando uma tendência de redução desses microrganismos, assim como nos microrganismos psicrotróficos. Observou-se ação imediata dos revestimentos contra a propagação de Staphylococcus spp., onde as amostras não apresentaram diferença estatística (p>0,05) entre os tratamentos a partir do dia 2. Os revestimentos onde havia a inclusão dos extratos de alecrim, demonstraram capacidade antioxidante significativa entre os tratamentos e ao longo dos tempos de avaliação. Concernente aos filmes, observou-se variação da espessura, entretanto, não houve diferença significativa (p>0,05) entre esses valores. Tratando-se da solubilidade, não houve diferença significativa (p>0,05) entre os tratamentos. A absorção de umidade variou significativamente (p<0,05) entre o tratamento controle e os tratados com os extratos. Na avaliação de PVA, há diferença significativa (p<0,05) entre os tratamentos controle e com 8% de extrato, 0,41 e 0,70 g.mm/h.m².kPa, respectivamente, evitando o processo de deterioração em alimentos. Em relação aos testes mecânicos, o controle, requer menor tensão que as amostras com extratos, para sofrer a deformação, no entanto, não há diferença estatística (p>0,05). Com relação à força necessária para romper o corpo de prova, observou-se que o filme controle, apresenta-se mais resistente que os filmes com extratos, apresentando diferença estatística (p<0,05). Assim, conclui-se que os revestimentos à base de quitosana e extrato de alecrim (Rosmarinus officinalis L.), apresentaram influência na conservação e qualidade da carne bovina refrigerada, sendo o revestimento com menor concentração do extrato (4%) o mais indicado, pois possui o menor custo de produção, mantendo a carne o mais próximo do naturalCoordenação de Aperfeiçoamento de Pessoal de Nível Superior - CAPESUniversidade Federal Rural do Semi-ÁridoBrasilCentro de Ciências Agrárias - CCAUFERSAPrograma de Pós-Graduação em Ciência AnimalLeite, Ricardo Henrique de Lima52264343400http://lattes.cnpq.br/3801476460958779Lima, Patrícia de Oliveira76517780491http://lattes.cnpq.br/5491095039598621Abrantes, Maria Rociene05476448411http://lattes.cnpq.br/8581676690083096Lima, Allison Ferreira de2019-03-14T19:26:15Z2019-03-142019-03-14T19:26:15Z2019-02-22info:eu-repo/semantics/masterThesisinfo:eu-repo/semantics/publishedVersionapplication/pdfCitação com autor incluído no texto: Lima (2019) Citação com autor não incluído no texto: (LIMA, 2019)https://doi.org/10.21708/bdtd.ppgca.dissertacao.978https://repositorio.ufersa.edu.br/handle/prefix/978porLIMA, Allison Ferreira de. Revestimentos comestíveis a base de quitosana e extrato de alecrim (rosmarinus officinalis l.) e sua aplicabilidade na carne bovina. 2019. 54 f. Dissertação (Mestrado em Ciência Animal), Universidade Federal Rural do Semi-Árido, Mossoró, 2019.info:eu-repo/semantics/openAccessCC-BY-SAreponame:Repositório Digital da Universidade Federal Rural do Semiárido (RDU)instname:Universidade Federal Rural do Semi-Árido (UFERSA)instacron:UFERSA2025-02-05T04:59:15Zoai:repositorio.ufersa.edu.br:prefix/978Repositório Institucionalhttps://repositorio.ufersa.edu.br/PUBhttps://repositorio.ufersa.edu.br/server/oai/requestrepositorio@ufersa.edu.br || admrepositorio@ufersa.edu.bropendoar:2025-02-05T04:59:15Repositório Digital da Universidade Federal Rural do Semiárido (RDU) - Universidade Federal Rural do Semi-Árido (UFERSA)false
dc.title.none.fl_str_mv Revestimentos comestíveis a base de quitosana e extrato de alecrim (rosmarinus officinalis l.) e sua aplicabilidade na carne bovina
title Revestimentos comestíveis a base de quitosana e extrato de alecrim (rosmarinus officinalis l.) e sua aplicabilidade na carne bovina
spellingShingle Revestimentos comestíveis a base de quitosana e extrato de alecrim (rosmarinus officinalis l.) e sua aplicabilidade na carne bovina
Lima, Allison Ferreira de
Cobertura
Conservação
Qualidade da carne
Tecnologia de alimentos
Vida útil
Conservation
Food technology
Meat quality
Roof
Shelf life
CNPQ::CIENCIAS AGRARIAS::MEDICINA VETERINARIA
title_short Revestimentos comestíveis a base de quitosana e extrato de alecrim (rosmarinus officinalis l.) e sua aplicabilidade na carne bovina
title_full Revestimentos comestíveis a base de quitosana e extrato de alecrim (rosmarinus officinalis l.) e sua aplicabilidade na carne bovina
title_fullStr Revestimentos comestíveis a base de quitosana e extrato de alecrim (rosmarinus officinalis l.) e sua aplicabilidade na carne bovina
title_full_unstemmed Revestimentos comestíveis a base de quitosana e extrato de alecrim (rosmarinus officinalis l.) e sua aplicabilidade na carne bovina
title_sort Revestimentos comestíveis a base de quitosana e extrato de alecrim (rosmarinus officinalis l.) e sua aplicabilidade na carne bovina
author Lima, Allison Ferreira de
author_facet Lima, Allison Ferreira de
author_role author
dc.contributor.none.fl_str_mv Leite, Ricardo Henrique de Lima
52264343400
http://lattes.cnpq.br/3801476460958779
Lima, Patrícia de Oliveira
76517780491
http://lattes.cnpq.br/5491095039598621
Abrantes, Maria Rociene
05476448411
http://lattes.cnpq.br/8581676690083096
dc.contributor.author.fl_str_mv Lima, Allison Ferreira de
dc.subject.por.fl_str_mv Cobertura
Conservação
Qualidade da carne
Tecnologia de alimentos
Vida útil
Conservation
Food technology
Meat quality
Roof
Shelf life
CNPQ::CIENCIAS AGRARIAS::MEDICINA VETERINARIA
topic Cobertura
Conservação
Qualidade da carne
Tecnologia de alimentos
Vida útil
Conservation
Food technology
Meat quality
Roof
Shelf life
CNPQ::CIENCIAS AGRARIAS::MEDICINA VETERINARIA
description The objective of the research was to elaborate and evaluate edible coatings based on chitosan and rosemary extract (Rosmarinus officinalis L.) and its applicability on beef. At the beginning, the preparation of rosemary extracts at concentrations of 4% and 8%, as well as preparation of the polymer mixture and consequent immersion of the meat in this content and in distilled water (control) for the physical analyzes (pH, (coliforms at 45 ° C and the shelf life of mesophiles, psychrotrophs, Staphylococcus ssp. and detection of Salmonella spp.) and antioxidant activity (TBARS). The mechanical properties, water vapor permeability (PVA), color, transparency, solubility and moisture absorption of the films were evaluated. The results of the physical analyzes show that there was a significant effect (p <0.05) between coatings types and shelf life for pH and all color parameters studied (L, a * and b *). The highest water retention capacity occurred at the concentration of 8% of the extract. Among the treatments on weight loss in cooking, these results relate to polymer blends. The shear force also showed a difference between the treatments and the times, all the samples had a decrease in the shear force over time. In the microbiological analyzes, the absence of Salmonella spp. in 25 g of sample. As for coliforms at 45º C, values of 1100 NMP / g were found both in the treated samples and in the control at time 0 (single evaluation day). The count of aerobic mesophilic microorganisms differed significantly (p <0.05) in the coatings where the rosemary extracts were included in the other treatments, showing a tendency to reduce these microorganisms, as well as in psychrotrophic microorganisms. It was observed immediate action of the coatings against the propagation of Staphylococcus spp., Where the samples did not present statistical difference (p> 0.05) between the treatments from day 2. The coatings where there was the inclusion of rosemary extracts, demonstrated significant antioxidant capacity between treatments and over the evaluation times. Concerning the films, thickness variation was observed, however, there was no significant difference (p> 0.05) between these values. As for solubility, there was no significant difference (p> 0.05) between treatments. The moisture absorption varied significantly (p <0.05) between the control treatment and those treated with the extracts. In the PVA evaluation, there was a significant difference (p <0.05) between the control treatments and with 8% of extract, 0.41 and 0.70 g.mm/h.m².kPa, respectively, avoiding the deterioration process in food. In relation to the mechanical tests, the control requires less tension than the samples with extracts, to undergo deformation, however, there is no statistical difference (p> 0.05). Regarding the force required to break the test specimen, it was observed that the control film is more resistant than films with extracts, presenting a statistical difference (p <0.05). Thus, it was concluded that the coatings based on chitosan and rosemary extract (Rosmarinus officinalis L.) had an influence on the conservation and quality of refrigerated beef, and the coating with the lowest extract concentration (4%) was the most indicated, because it has the lowest cost of production, keeping the meat as close to the natural one
publishDate 2019
dc.date.none.fl_str_mv 2019-03-14T19:26:15Z
2019-03-14
2019-03-14T19:26:15Z
2019-02-22
dc.type.driver.fl_str_mv info:eu-repo/semantics/masterThesis
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
format masterThesis
status_str publishedVersion
dc.identifier.uri.fl_str_mv Citação com autor incluído no texto: Lima (2019) Citação com autor não incluído no texto: (LIMA, 2019)
https://doi.org/10.21708/bdtd.ppgca.dissertacao.978
https://repositorio.ufersa.edu.br/handle/prefix/978
identifier_str_mv Citação com autor incluído no texto: Lima (2019) Citação com autor não incluído no texto: (LIMA, 2019)
url https://doi.org/10.21708/bdtd.ppgca.dissertacao.978
https://repositorio.ufersa.edu.br/handle/prefix/978
dc.language.iso.fl_str_mv por
language por
dc.relation.none.fl_str_mv LIMA, Allison Ferreira de. Revestimentos comestíveis a base de quitosana e extrato de alecrim (rosmarinus officinalis l.) e sua aplicabilidade na carne bovina. 2019. 54 f. Dissertação (Mestrado em Ciência Animal), Universidade Federal Rural do Semi-Árido, Mossoró, 2019.
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
CC-BY-SA
eu_rights_str_mv openAccess
rights_invalid_str_mv CC-BY-SA
dc.format.none.fl_str_mv application/pdf
dc.publisher.none.fl_str_mv Universidade Federal Rural do Semi-Árido
Brasil
Centro de Ciências Agrárias - CCA
UFERSA
Programa de Pós-Graduação em Ciência Animal
publisher.none.fl_str_mv Universidade Federal Rural do Semi-Árido
Brasil
Centro de Ciências Agrárias - CCA
UFERSA
Programa de Pós-Graduação em Ciência Animal
dc.source.none.fl_str_mv reponame:Repositório Digital da Universidade Federal Rural do Semiárido (RDU)
instname:Universidade Federal Rural do Semi-Árido (UFERSA)
instacron:UFERSA
instname_str Universidade Federal Rural do Semi-Árido (UFERSA)
instacron_str UFERSA
institution UFERSA
reponame_str Repositório Digital da Universidade Federal Rural do Semiárido (RDU)
collection Repositório Digital da Universidade Federal Rural do Semiárido (RDU)
repository.name.fl_str_mv Repositório Digital da Universidade Federal Rural do Semiárido (RDU) - Universidade Federal Rural do Semi-Árido (UFERSA)
repository.mail.fl_str_mv repositorio@ufersa.edu.br || admrepositorio@ufersa.edu.br
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