Influ?ncia dos par?metros de secagem e formas de fracionamento na composi??o qu?mica do gengibre (zingiber officinale roscoe) desidratado

Detalhes bibliográficos
Ano de defesa: 2018
Autor(a) principal: Cristofel, Cristian Jos?
Orientador(a): Não Informado pela instituição
Banca de defesa: Não Informado pela instituição
Tipo de documento: Dissertação
Tipo de acesso: Acesso aberto
Idioma: por
Instituição de defesa: Universidade Federal da Fronteira Sul
Brasil
Campus Laranjeiras do Sul
Programa de P?s-Gradua??o em Ci?ncia e Tecnologia de Alimentos
UFFS
Programa de Pós-Graduação: Não Informado pela instituição
Departamento: Não Informado pela instituição
País: Não Informado pela instituição
Palavras-chave em Português:
Link de acesso: https://rd.uffs.edu.br/handle/prefix/2308
Resumo: Ginger, rhizome of Zingiber Officinale Roscoe, is widely marketed for use in the food, chemical and pharmaceutical industries, especially in the dried and powder form. For this, it is necessary that the raw material undergoes a drying process, which can influence significantly its characteristics, so, during drying it is necessary to take into account the most desirable conditions of the product, from the standpoint of maintenance of their constituents. This work proposes to investigate the dehydration process of gingerd under three different fractionation forms: whole, sliced and grated; and submitted to three different drying processes: heater with forced air circulation (CC) and heater without forced air circulation and (SC), both at temperatures of 50, 60, 70 and 80?C, and freeze-drying. The obtained data allowed the construction of drying curves Xbs (t): moisture content of material (kg of product - kg dry mass) / (kg dry mass)) and curves of Aw (t): activity of water versus time of dehydration. The samples dehydrated by different processes were analyzed for color, phenolic compounds, thiobarbituric acid reactive substances (TBARS), acidity index, DPPH radical sequestration capacity, and chemical composition of the essential oils obtained by hydrodistillation. The results showed that the drying time ranged from 3.7 to 30.2 hours, and was dependent on the methodology used and the process temperature, in with the highest temperatures reaching lower humidity in a shorter time, as well, as the circulation and fractionation of the sample influenced the reduction of ginger dehydration time. Fractionation of the sample also reduced the drying time for all processes. For the color analysis, the different process temperatures did not provide significant changes, however, the more fragmented the sample, the lower the luminosity (L *), the tendency for red (H *) and increase in color intensity (C *). In the freeze-drying, the fractionation of the sample did not influence the color results. In the analysis of phenolic compounds, thiobarbituric acid reactive substances, acidity index and DPPH radical sequestration capacity, it was found that the lower temperature, the lower sample fractionation and the forced air circulation generated results closer for those of the in natura sample, that is, thus preserving the bioactive compounds. The results of the best method in heater were similar to those obtained by freeze-drying. The extraction yield of ginger oil by hydrodistillation ranged from 1.53 to 1.64%. It was observed that in all the drying processes analyzed there was a change in the composition of the oil when compared to the in natura sample, and the higher temperature and the larger sample fractionation the greater was the change. There was concentration and loss of some compounds as well as the formation of others.
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spelling Influ?ncia dos par?metros de secagem e formas de fracionamento na composi??o qu?mica do gengibre (zingiber officinale roscoe) desidratado?leos e gorduras vegetais comest?veisInd?stria de alimentosGinger, rhizome of Zingiber Officinale Roscoe, is widely marketed for use in the food, chemical and pharmaceutical industries, especially in the dried and powder form. For this, it is necessary that the raw material undergoes a drying process, which can influence significantly its characteristics, so, during drying it is necessary to take into account the most desirable conditions of the product, from the standpoint of maintenance of their constituents. This work proposes to investigate the dehydration process of gingerd under three different fractionation forms: whole, sliced and grated; and submitted to three different drying processes: heater with forced air circulation (CC) and heater without forced air circulation and (SC), both at temperatures of 50, 60, 70 and 80?C, and freeze-drying. The obtained data allowed the construction of drying curves Xbs (t): moisture content of material (kg of product - kg dry mass) / (kg dry mass)) and curves of Aw (t): activity of water versus time of dehydration. The samples dehydrated by different processes were analyzed for color, phenolic compounds, thiobarbituric acid reactive substances (TBARS), acidity index, DPPH radical sequestration capacity, and chemical composition of the essential oils obtained by hydrodistillation. The results showed that the drying time ranged from 3.7 to 30.2 hours, and was dependent on the methodology used and the process temperature, in with the highest temperatures reaching lower humidity in a shorter time, as well, as the circulation and fractionation of the sample influenced the reduction of ginger dehydration time. Fractionation of the sample also reduced the drying time for all processes. For the color analysis, the different process temperatures did not provide significant changes, however, the more fragmented the sample, the lower the luminosity (L *), the tendency for red (H *) and increase in color intensity (C *). In the freeze-drying, the fractionation of the sample did not influence the color results. In the analysis of phenolic compounds, thiobarbituric acid reactive substances, acidity index and DPPH radical sequestration capacity, it was found that the lower temperature, the lower sample fractionation and the forced air circulation generated results closer for those of the in natura sample, that is, thus preserving the bioactive compounds. The results of the best method in heater were similar to those obtained by freeze-drying. The extraction yield of ginger oil by hydrodistillation ranged from 1.53 to 1.64%. It was observed that in all the drying processes analyzed there was a change in the composition of the oil when compared to the in natura sample, and the higher temperature and the larger sample fractionation the greater was the change. There was concentration and loss of some compounds as well as the formation of others.O gengibre, rizoma da Zingiber Officinale Roscoe, ? amplamente comercializado para uso nas ind?strias de alimentos, qu?mica e farmac?utica, principalmente na forma desidratada e em p?. Para isso, ? necess?rio que a mat?ria-prima passe por um processo de secagem, o qual pode influenciar significativamente em suas caracter?sticas, sendo assim, durante a secagem ? necess?rio levar em considera??o ?s condi??es mais desej?veis do produto, do ponto de vista de manuten??o de seus constituintes. Este trabalho prop?s investigar o processo de desidrata??o do gengibre sob tr?s diferentes m?todos de fracionamento: inteiro, fatiado e ralado; e submetido a tr?s diferentes processos de secagem: estufa com circula??o e renova??o de ar for?ado (CC) e sem circula??o e renova??o de ar for?ado (SC), ambos para as temperaturas de 50, 60, 70 e 80?C, e liofiliza??o. Os dados obtidos permitiram a constru??o das curvas de secagem Xbs (t): conte?do de umidade de um material ((kg do produto ? kg massa seca) / (kg massa seca)) e das curvas de Aw(t): atividade de ?gua em fun??o do tempo. As amostras desidratadas pelos diferentes processos e in natura foram analisadas quanto ? cor, compostos fen?licos, subst?ncias reativas ao ?cido tiobarbit?rico (TBARS), acidez titul?vel, capacidade de sequestro do radical DPPH, e composi??o qu?mica dos ?leos essenciais, obtidos por hidrodestila??o. Os resultados mostraram que o tempo de secagem variou de 3,7 a 30,2 horas, e foi dependente da metodologia utilizada e da temperatura de processo, em que as mais altas atingindo umidades mais baixas em menor tempo, como tamb?m, que a circula??o de ar e o fracionamento da amostra influenciaram na redu??o do tempo de desidrata??o do gengibre. O fracionamento da amostra tamb?m reduziu o tempo de secagem para todos os processos. Para a an?lise de cor, as diferentes temperaturas do processo n?o proporcionaram altera??es significativas, entretanto, quanto mais fracionada a amostra, menor a luminosidade (L*), tend?ncia para a colora??o vermelha (H*) e aumento da intensidade da cor (C*). J? na liofiliza??o, o fracionamento da amostra n?o influenciou na cor. Nas an?lises de compostos fen?licos, subst?ncias reativas ao ?cido tiobarbit?rico, acidez titul?vel e capacidade de sequestro do radical DPPH, verificou-se que quanto menor a temperatura, menor o fracionamento da amostra e com circula??o de ar for?ado, geraram resultados mais pr?ximos aos obtidos para a amostra in natura, preservando os compostos bioativos. Os resultados do melhor m?todo em estufa foram semelhantes aos obtidos por liofiliza??o. O rendimento na extra??o dos ?leos ess?ncias do gengibre por hidrodestila??o variou de 1,53 a 1,64%. Observou-se que em todos os processos de secagem analisados houve altera??o na composi??o do ?leo, quando comparado com a amostra in natura, sendo que quanto maior a temperatura e maior o fracionamento da amostra, maior foi a altera??o. Houve a concentra??o e a perda de alguns compostos bem como a forma??o de outros.Universidade Federal da Fronteira SulBrasilCampus Laranjeiras do SulPrograma de P?s-Gradua??o em Ci?ncia e Tecnologia de AlimentosUFFSTormen, LucianoCristofel, Cristian Jos?20182019-01-28T13:06:23Z2019-01-282019-01-28T13:06:23Z2018info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/masterThesishttps://rd.uffs.edu.br/handle/prefix/2308porinfo:eu-repo/semantics/openAccessreponame:Repositório Institucional da UFFS (Repositório Digital da UFFS)instname:Universidade Federal Fronteira do Sul (UFFS)instacron:UFFS2021-09-29T13:20:01Zoai:rd.uffs.edu.br:prefix/2308Repositório InstitucionalPUBhttps://rd.uffs.edu.br/oai/requestfranciele.cruz@uffs.edu.bropendoar:39242021-09-29T13:20:01Repositório Institucional da UFFS (Repositório Digital da UFFS) - Universidade Federal Fronteira do Sul (UFFS)false
dc.title.none.fl_str_mv Influ?ncia dos par?metros de secagem e formas de fracionamento na composi??o qu?mica do gengibre (zingiber officinale roscoe) desidratado
title Influ?ncia dos par?metros de secagem e formas de fracionamento na composi??o qu?mica do gengibre (zingiber officinale roscoe) desidratado
spellingShingle Influ?ncia dos par?metros de secagem e formas de fracionamento na composi??o qu?mica do gengibre (zingiber officinale roscoe) desidratado
Cristofel, Cristian Jos?
?leos e gorduras vegetais comest?veis
Ind?stria de alimentos
title_short Influ?ncia dos par?metros de secagem e formas de fracionamento na composi??o qu?mica do gengibre (zingiber officinale roscoe) desidratado
title_full Influ?ncia dos par?metros de secagem e formas de fracionamento na composi??o qu?mica do gengibre (zingiber officinale roscoe) desidratado
title_fullStr Influ?ncia dos par?metros de secagem e formas de fracionamento na composi??o qu?mica do gengibre (zingiber officinale roscoe) desidratado
title_full_unstemmed Influ?ncia dos par?metros de secagem e formas de fracionamento na composi??o qu?mica do gengibre (zingiber officinale roscoe) desidratado
title_sort Influ?ncia dos par?metros de secagem e formas de fracionamento na composi??o qu?mica do gengibre (zingiber officinale roscoe) desidratado
author Cristofel, Cristian Jos?
author_facet Cristofel, Cristian Jos?
author_role author
dc.contributor.none.fl_str_mv Tormen, Luciano
dc.contributor.author.fl_str_mv Cristofel, Cristian Jos?
dc.subject.por.fl_str_mv ?leos e gorduras vegetais comest?veis
Ind?stria de alimentos
topic ?leos e gorduras vegetais comest?veis
Ind?stria de alimentos
description Ginger, rhizome of Zingiber Officinale Roscoe, is widely marketed for use in the food, chemical and pharmaceutical industries, especially in the dried and powder form. For this, it is necessary that the raw material undergoes a drying process, which can influence significantly its characteristics, so, during drying it is necessary to take into account the most desirable conditions of the product, from the standpoint of maintenance of their constituents. This work proposes to investigate the dehydration process of gingerd under three different fractionation forms: whole, sliced and grated; and submitted to three different drying processes: heater with forced air circulation (CC) and heater without forced air circulation and (SC), both at temperatures of 50, 60, 70 and 80?C, and freeze-drying. The obtained data allowed the construction of drying curves Xbs (t): moisture content of material (kg of product - kg dry mass) / (kg dry mass)) and curves of Aw (t): activity of water versus time of dehydration. The samples dehydrated by different processes were analyzed for color, phenolic compounds, thiobarbituric acid reactive substances (TBARS), acidity index, DPPH radical sequestration capacity, and chemical composition of the essential oils obtained by hydrodistillation. The results showed that the drying time ranged from 3.7 to 30.2 hours, and was dependent on the methodology used and the process temperature, in with the highest temperatures reaching lower humidity in a shorter time, as well, as the circulation and fractionation of the sample influenced the reduction of ginger dehydration time. Fractionation of the sample also reduced the drying time for all processes. For the color analysis, the different process temperatures did not provide significant changes, however, the more fragmented the sample, the lower the luminosity (L *), the tendency for red (H *) and increase in color intensity (C *). In the freeze-drying, the fractionation of the sample did not influence the color results. In the analysis of phenolic compounds, thiobarbituric acid reactive substances, acidity index and DPPH radical sequestration capacity, it was found that the lower temperature, the lower sample fractionation and the forced air circulation generated results closer for those of the in natura sample, that is, thus preserving the bioactive compounds. The results of the best method in heater were similar to those obtained by freeze-drying. The extraction yield of ginger oil by hydrodistillation ranged from 1.53 to 1.64%. It was observed that in all the drying processes analyzed there was a change in the composition of the oil when compared to the in natura sample, and the higher temperature and the larger sample fractionation the greater was the change. There was concentration and loss of some compounds as well as the formation of others.
publishDate 2018
dc.date.none.fl_str_mv 2018
2018
2019-01-28T13:06:23Z
2019-01-28
2019-01-28T13:06:23Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/masterThesis
format masterThesis
status_str publishedVersion
dc.identifier.uri.fl_str_mv https://rd.uffs.edu.br/handle/prefix/2308
url https://rd.uffs.edu.br/handle/prefix/2308
dc.language.iso.fl_str_mv por
language por
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.publisher.none.fl_str_mv Universidade Federal da Fronteira Sul
Brasil
Campus Laranjeiras do Sul
Programa de P?s-Gradua??o em Ci?ncia e Tecnologia de Alimentos
UFFS
publisher.none.fl_str_mv Universidade Federal da Fronteira Sul
Brasil
Campus Laranjeiras do Sul
Programa de P?s-Gradua??o em Ci?ncia e Tecnologia de Alimentos
UFFS
dc.source.none.fl_str_mv reponame:Repositório Institucional da UFFS (Repositório Digital da UFFS)
instname:Universidade Federal Fronteira do Sul (UFFS)
instacron:UFFS
instname_str Universidade Federal Fronteira do Sul (UFFS)
instacron_str UFFS
institution UFFS
reponame_str Repositório Institucional da UFFS (Repositório Digital da UFFS)
collection Repositório Institucional da UFFS (Repositório Digital da UFFS)
repository.name.fl_str_mv Repositório Institucional da UFFS (Repositório Digital da UFFS) - Universidade Federal Fronteira do Sul (UFFS)
repository.mail.fl_str_mv franciele.cruz@uffs.edu.br
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