Compostos voláteis e parâmetros de qualidade de diferentes genótipos de frutos de Butia odorata

Detalhes bibliográficos
Ano de defesa: 2012
Autor(a) principal: Ferrão, Tassiane dos Santos
Orientador(a): Não Informado pela instituição
Banca de defesa: Não Informado pela instituição
Tipo de documento: Dissertação
Tipo de acesso: Acesso aberto
dARK ID: ark:/26339/0013000017d14
Idioma: por
Instituição de defesa: Universidade Federal de Santa Maria
BR
Ciência e Tecnologia dos Alimentos
UFSM
Programa de Pós-Graduação em Ciência e Tecnologia dos Alimentos
Programa de Pós-Graduação: Não Informado pela instituição
Departamento: Não Informado pela instituição
País: Não Informado pela instituição
Palavras-chave em Português:
Link de acesso: http://repositorio.ufsm.br/handle/1/5718
Resumo: The Butia odorata has received special attention from the scientific community because of their nutritional and functional properties that have been revealed, in addition to its rightdown sensory characteristics. The aim of this study was to characterize different genotypes from Butia odorata fruit collected in Santa Maria - RS (SM) and Santa Rosa - RS (SR) regions during three consecutive harvests in relation to various physical and chemical properties. Many analyses were performed like: biometric, color and quality parameters, fatty acid composition in the Butia pulp. An HS-SPME method was developed for the isolation and subsequent quantification (GC-FID) and identification (GC/MS) of volatile compounds (VCs). The biometric parameters results showed pulp yields between 40.38 and 73.91%. The color of the pulp ranged between yellow and orange shades. TSS ranged between 12.39 and 15.50 °Brix, acidity between 0.69 and 2.26 g% citric acid and pH between 3.17 and 3.95. The fruit had humidity between 78.04 and 85.85 g%; ashes between 0.47 and 0.77 g%; protein between 0.57 and 0.93 g%, crude fiber between 0.84 and 4.02 g%; lipid between 0.12 and 2.27 g%. The fatty acids such as palmitic acid, linoleic and linolenic acids were found in abundance. It was possible to observe the partial discrimination between the two regions in the PCA using the physico-chemical variables. The samples from SR characterized by high scores for lipids and palmitic acid, while SM samples showed a higher humidity and TSS. The method employed use DVB/CAR/PDMS fiber for the VCs extraction of the centrifuged Butia pulp , added with 30% NaCl, and maintaining the system at a temperature of 35 °C for 45 minutes, under stirring. The volatile fraction was analyzed in GC and were identified 77 compounds among acids (5), alcohols (14), aldehydes (9), ketones (12), lactones (3), terpenes (2) and esters (34). The ethyl hexanoate compound was the major compound in almost samples. The PCA from VCs enabled to realize grouping of samples into two groups according to region of origin. The fruits from Santa Maria showed a high content of esters and the fruits from Santa Rosa had higher concentrations of alcohols and aldehydes. An exploratory analysis of the variables of physico-chemical composition and volatile of the samples was observed using PCA. In the graphs analysis also realized a partial separation of samples according to their region: the samples SM2-10 and RS1-11 distanced themselves from the other and it indicates greater particularity in their chemical compositions. Therefore the fruits (Butia odorata) showed great variability in biometric characteristics, physico-chemical and volatile profiles according to region of origin. It indicates a strong influence of soil and climatic factors. In this study, the nutritional characteristics and high yield pulp of some Butia fruits demonstrated the high potential for fresh consumption or for the manufacture of processed products
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spelling Compostos voláteis e parâmetros de qualidade de diferentes genótipos de frutos de Butia odorataVolatile compounds and quality parameters from different genotypes of Butia odorataFrutas nativasComposição centesimalÁcidos graxosSPMEGC-FIDGC/MSNative fruitsProximate compositionFatty acidsSPMECNPQ::CIENCIAS AGRARIAS::CIENCIA E TECNOLOGIA DE ALIMENTOSThe Butia odorata has received special attention from the scientific community because of their nutritional and functional properties that have been revealed, in addition to its rightdown sensory characteristics. The aim of this study was to characterize different genotypes from Butia odorata fruit collected in Santa Maria - RS (SM) and Santa Rosa - RS (SR) regions during three consecutive harvests in relation to various physical and chemical properties. Many analyses were performed like: biometric, color and quality parameters, fatty acid composition in the Butia pulp. An HS-SPME method was developed for the isolation and subsequent quantification (GC-FID) and identification (GC/MS) of volatile compounds (VCs). The biometric parameters results showed pulp yields between 40.38 and 73.91%. The color of the pulp ranged between yellow and orange shades. TSS ranged between 12.39 and 15.50 °Brix, acidity between 0.69 and 2.26 g% citric acid and pH between 3.17 and 3.95. The fruit had humidity between 78.04 and 85.85 g%; ashes between 0.47 and 0.77 g%; protein between 0.57 and 0.93 g%, crude fiber between 0.84 and 4.02 g%; lipid between 0.12 and 2.27 g%. The fatty acids such as palmitic acid, linoleic and linolenic acids were found in abundance. It was possible to observe the partial discrimination between the two regions in the PCA using the physico-chemical variables. The samples from SR characterized by high scores for lipids and palmitic acid, while SM samples showed a higher humidity and TSS. The method employed use DVB/CAR/PDMS fiber for the VCs extraction of the centrifuged Butia pulp , added with 30% NaCl, and maintaining the system at a temperature of 35 °C for 45 minutes, under stirring. The volatile fraction was analyzed in GC and were identified 77 compounds among acids (5), alcohols (14), aldehydes (9), ketones (12), lactones (3), terpenes (2) and esters (34). The ethyl hexanoate compound was the major compound in almost samples. The PCA from VCs enabled to realize grouping of samples into two groups according to region of origin. The fruits from Santa Maria showed a high content of esters and the fruits from Santa Rosa had higher concentrations of alcohols and aldehydes. An exploratory analysis of the variables of physico-chemical composition and volatile of the samples was observed using PCA. In the graphs analysis also realized a partial separation of samples according to their region: the samples SM2-10 and RS1-11 distanced themselves from the other and it indicates greater particularity in their chemical compositions. Therefore the fruits (Butia odorata) showed great variability in biometric characteristics, physico-chemical and volatile profiles according to region of origin. It indicates a strong influence of soil and climatic factors. In this study, the nutritional characteristics and high yield pulp of some Butia fruits demonstrated the high potential for fresh consumption or for the manufacture of processed productsO butiá (Butia odorata) tem recebido especial atenção da comunidade científica, em virtude de suas propriedades nutritivas e funcionais que estão sendo reveladas, além das suas características sensoriais peculiares, ainda pouco exploradas. Desta forma, o objetivo do presente trabalho foi caracterizar diferentes genótipos de frutos de butiazeiros coletados nas regiões de Santa Maria RS (SM) e Santa Rosa RS (SR) em três safras consecutivas, quanto as diversas propriedades físicoquímicas. Foram realizadas análises biométricas, de cor, dos parâmetros de qualidade, composição centesimal e ácidos graxos da polpa do butiá, além do desenvolvimento de método de isolamento por SPME com posterior quantificação (GC-FID) e identificação (GC/MS) dos compostos voláteis (CVs). Os resultados dos parâmetros biométricos revelaram rendimentos de polpa, entre 40,38 e 73,91%. A cor da polpa oscilou em tons de amarelo e laranja. Os SST variaram entre 12,39 e 15,50 °Brix, a acidez entre 0,69 e 2,26 g% em ácido cítrico e o pH entre 3,17 e 3,95. As frutas apresentaram umidade entre 78,04 e 85,85 g%; cinzas entre 0,47 e 0,77 g%, proteína entre 0,57 e 0,93 g%, fibra bruta entre 0,84 e 4,02 g% e lipídios de 0,12 a 2,27 g%. Os ácidos graxos encontrados em maior abundância foram o ácido palmítico, linoléico e linolênico. Na Análise dos Componentes Principais (PCA) empregando as variáveis físico-químicas observou-se a discriminação parcial entre as duas regiões, sendo as amostras da região de SR caracterizadas por elevados escores para lipídios e ácido palmítico, enquanto que as da região de SM apresentaram, em geral, maior umidade e teor de SST. O método desenvolvido emprega o uso da fibra DVB/CAR/PDMS para a extração dos CVs da polpa de butiá centrifugada, adicionada de 30% de NaCl, e mantendo o sistema a uma temperatura de 35 ºC por 45 minutos, sob agitação. A fração volátil foi analisada em GC e nela identificados 77 compostos entre ácidos (5), alcoóis (14), aldeídos (9), cetonas (12), lactonas (3), terpenos (2) e, principalmente, ésteres (34). Entre estes se destacou o hexanoato de etila como composto majoritário. A PCA dos CVs possibilitou ver o agrupamento das amostras em dois grupos conforme a região de origem, onde, em geral, os butiás de Santa Maria apresentaram elevado teor de ésteres, enquanto os de Santa Rosa obtiveram maiores concentrações de alcoóis e aldeídos. Uma análise exploratória entre as variáveis de composição físico-química e volátil das amostras estudadas foram observadas através de uma PCA. Na visualização dos gráficos notou-se também uma parcial separação das amostras quanto à região de origem, sendo que as amostras SM2-10 e SR1-11 distanciaram-se das demais, indicando maior particularidade em suas composições químicas. Sendo assim, os butiás apresentaram grande variabilidade em suas características biométricas, físicoquímicas e nos perfis voláteis em função da região de origem e safra e, portanto, apresentou forte influência de fatores edafoclimáticos. Sobretudo, as características nutricionais e o alto rendimento de polpa de alguns frutos de butiás evidenciaram, neste estudo, o alto potencial para consumo in natura ou mesmo para a fabricação de produtos processados.Universidade Federal de Santa MariaBRCiência e Tecnologia dos AlimentosUFSMPrograma de Pós-Graduação em Ciência e Tecnologia dos AlimentosWagner, Rogerhttp://lattes.cnpq.br/4780821244553957Sautter, Cláudia Kaehlerhttp://lattes.cnpq.br/9384438325422405Barin, Juliano Smaniotohttp://lattes.cnpq.br/7545847424095994Prestes, Osmar Damianhttp://lattes.cnpq.br/9632234955509028Ferrão, Tassiane dos Santos2012-11-132012-11-132012-02-27info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/masterThesisapplication/pdfapplication/pdfFERRÃO, Tassiane dos Santos. Volatile compounds and quality parameters from different genotypes of Butia odorata. 2012. 92 f. Dissertação (Mestrado em Ciência e Tecnologia dos Alimentos) - Universidade Federal de Santa Maria, Santa Maria, 2012.http://repositorio.ufsm.br/handle/1/5718ark:/26339/0013000017d14porinfo:eu-repo/semantics/openAccessreponame:Manancial - Repositório Digital da UFSMinstname:Universidade Federal de Santa Maria (UFSM)instacron:UFSM2023-05-26T11:34:18Zoai:repositorio.ufsm.br:1/5718Biblioteca Digital de Teses e Dissertaçõeshttps://repositorio.ufsm.br/PUBhttps://repositorio.ufsm.br/oai/requestatendimento.sib@ufsm.br||tedebc@gmail.com||manancial@ufsm.bropendoar:2023-05-26T11:34:18Manancial - Repositório Digital da UFSM - Universidade Federal de Santa Maria (UFSM)false
dc.title.none.fl_str_mv Compostos voláteis e parâmetros de qualidade de diferentes genótipos de frutos de Butia odorata
Volatile compounds and quality parameters from different genotypes of Butia odorata
title Compostos voláteis e parâmetros de qualidade de diferentes genótipos de frutos de Butia odorata
spellingShingle Compostos voláteis e parâmetros de qualidade de diferentes genótipos de frutos de Butia odorata
Ferrão, Tassiane dos Santos
Frutas nativas
Composição centesimal
Ácidos graxos
SPME
GC-FID
GC/MS
Native fruits
Proximate composition
Fatty acids
SPME
CNPQ::CIENCIAS AGRARIAS::CIENCIA E TECNOLOGIA DE ALIMENTOS
title_short Compostos voláteis e parâmetros de qualidade de diferentes genótipos de frutos de Butia odorata
title_full Compostos voláteis e parâmetros de qualidade de diferentes genótipos de frutos de Butia odorata
title_fullStr Compostos voláteis e parâmetros de qualidade de diferentes genótipos de frutos de Butia odorata
title_full_unstemmed Compostos voláteis e parâmetros de qualidade de diferentes genótipos de frutos de Butia odorata
title_sort Compostos voláteis e parâmetros de qualidade de diferentes genótipos de frutos de Butia odorata
author Ferrão, Tassiane dos Santos
author_facet Ferrão, Tassiane dos Santos
author_role author
dc.contributor.none.fl_str_mv Wagner, Roger
http://lattes.cnpq.br/4780821244553957
Sautter, Cláudia Kaehler
http://lattes.cnpq.br/9384438325422405
Barin, Juliano Smanioto
http://lattes.cnpq.br/7545847424095994
Prestes, Osmar Damian
http://lattes.cnpq.br/9632234955509028
dc.contributor.author.fl_str_mv Ferrão, Tassiane dos Santos
dc.subject.por.fl_str_mv Frutas nativas
Composição centesimal
Ácidos graxos
SPME
GC-FID
GC/MS
Native fruits
Proximate composition
Fatty acids
SPME
CNPQ::CIENCIAS AGRARIAS::CIENCIA E TECNOLOGIA DE ALIMENTOS
topic Frutas nativas
Composição centesimal
Ácidos graxos
SPME
GC-FID
GC/MS
Native fruits
Proximate composition
Fatty acids
SPME
CNPQ::CIENCIAS AGRARIAS::CIENCIA E TECNOLOGIA DE ALIMENTOS
description The Butia odorata has received special attention from the scientific community because of their nutritional and functional properties that have been revealed, in addition to its rightdown sensory characteristics. The aim of this study was to characterize different genotypes from Butia odorata fruit collected in Santa Maria - RS (SM) and Santa Rosa - RS (SR) regions during three consecutive harvests in relation to various physical and chemical properties. Many analyses were performed like: biometric, color and quality parameters, fatty acid composition in the Butia pulp. An HS-SPME method was developed for the isolation and subsequent quantification (GC-FID) and identification (GC/MS) of volatile compounds (VCs). The biometric parameters results showed pulp yields between 40.38 and 73.91%. The color of the pulp ranged between yellow and orange shades. TSS ranged between 12.39 and 15.50 °Brix, acidity between 0.69 and 2.26 g% citric acid and pH between 3.17 and 3.95. The fruit had humidity between 78.04 and 85.85 g%; ashes between 0.47 and 0.77 g%; protein between 0.57 and 0.93 g%, crude fiber between 0.84 and 4.02 g%; lipid between 0.12 and 2.27 g%. The fatty acids such as palmitic acid, linoleic and linolenic acids were found in abundance. It was possible to observe the partial discrimination between the two regions in the PCA using the physico-chemical variables. The samples from SR characterized by high scores for lipids and palmitic acid, while SM samples showed a higher humidity and TSS. The method employed use DVB/CAR/PDMS fiber for the VCs extraction of the centrifuged Butia pulp , added with 30% NaCl, and maintaining the system at a temperature of 35 °C for 45 minutes, under stirring. The volatile fraction was analyzed in GC and were identified 77 compounds among acids (5), alcohols (14), aldehydes (9), ketones (12), lactones (3), terpenes (2) and esters (34). The ethyl hexanoate compound was the major compound in almost samples. The PCA from VCs enabled to realize grouping of samples into two groups according to region of origin. The fruits from Santa Maria showed a high content of esters and the fruits from Santa Rosa had higher concentrations of alcohols and aldehydes. An exploratory analysis of the variables of physico-chemical composition and volatile of the samples was observed using PCA. In the graphs analysis also realized a partial separation of samples according to their region: the samples SM2-10 and RS1-11 distanced themselves from the other and it indicates greater particularity in their chemical compositions. Therefore the fruits (Butia odorata) showed great variability in biometric characteristics, physico-chemical and volatile profiles according to region of origin. It indicates a strong influence of soil and climatic factors. In this study, the nutritional characteristics and high yield pulp of some Butia fruits demonstrated the high potential for fresh consumption or for the manufacture of processed products
publishDate 2012
dc.date.none.fl_str_mv 2012-11-13
2012-11-13
2012-02-27
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/masterThesis
format masterThesis
status_str publishedVersion
dc.identifier.uri.fl_str_mv FERRÃO, Tassiane dos Santos. Volatile compounds and quality parameters from different genotypes of Butia odorata. 2012. 92 f. Dissertação (Mestrado em Ciência e Tecnologia dos Alimentos) - Universidade Federal de Santa Maria, Santa Maria, 2012.
http://repositorio.ufsm.br/handle/1/5718
dc.identifier.dark.fl_str_mv ark:/26339/0013000017d14
identifier_str_mv FERRÃO, Tassiane dos Santos. Volatile compounds and quality parameters from different genotypes of Butia odorata. 2012. 92 f. Dissertação (Mestrado em Ciência e Tecnologia dos Alimentos) - Universidade Federal de Santa Maria, Santa Maria, 2012.
ark:/26339/0013000017d14
url http://repositorio.ufsm.br/handle/1/5718
dc.language.iso.fl_str_mv por
language por
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
application/pdf
dc.publisher.none.fl_str_mv Universidade Federal de Santa Maria
BR
Ciência e Tecnologia dos Alimentos
UFSM
Programa de Pós-Graduação em Ciência e Tecnologia dos Alimentos
publisher.none.fl_str_mv Universidade Federal de Santa Maria
BR
Ciência e Tecnologia dos Alimentos
UFSM
Programa de Pós-Graduação em Ciência e Tecnologia dos Alimentos
dc.source.none.fl_str_mv reponame:Manancial - Repositório Digital da UFSM
instname:Universidade Federal de Santa Maria (UFSM)
instacron:UFSM
instname_str Universidade Federal de Santa Maria (UFSM)
instacron_str UFSM
institution UFSM
reponame_str Manancial - Repositório Digital da UFSM
collection Manancial - Repositório Digital da UFSM
repository.name.fl_str_mv Manancial - Repositório Digital da UFSM - Universidade Federal de Santa Maria (UFSM)
repository.mail.fl_str_mv atendimento.sib@ufsm.br||tedebc@gmail.com||manancial@ufsm.br
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